KR101972389B1 - Gas supply module for atomic layer deposition - Google Patents
Gas supply module for atomic layer deposition Download PDFInfo
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- KR101972389B1 KR101972389B1 KR1020170048384A KR20170048384A KR101972389B1 KR 101972389 B1 KR101972389 B1 KR 101972389B1 KR 1020170048384 A KR1020170048384 A KR 1020170048384A KR 20170048384 A KR20170048384 A KR 20170048384A KR 101972389 B1 KR101972389 B1 KR 101972389B1
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- gas
- gas supply
- supply unit
- diffusion region
- diffusion
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- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C16/00—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes
- C23C16/44—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating
- C23C16/455—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating characterised by the method used for introducing gases into reaction chamber or for modifying gas flows in reaction chamber
- C23C16/45523—Pulsed gas flow or change of composition over time
- C23C16/45525—Atomic layer deposition [ALD]
- C23C16/45544—Atomic layer deposition [ALD] characterized by the apparatus
- C23C16/45548—Atomic layer deposition [ALD] characterized by the apparatus having arrangements for gas injection at different locations of the reactor for each ALD half-reaction
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- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C16/00—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes
- C23C16/44—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating
- C23C16/455—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating characterised by the method used for introducing gases into reaction chamber or for modifying gas flows in reaction chamber
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C16/00—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes
- C23C16/44—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating
- C23C16/455—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating characterised by the method used for introducing gases into reaction chamber or for modifying gas flows in reaction chamber
- C23C16/45559—Diffusion of reactive gas to substrate
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- Chemical & Material Sciences (AREA)
- General Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Chemical Vapour Deposition (AREA)
Abstract
The gas supply module for atomic layer deposition according to an embodiment of the present invention includes a case and an atomic layer deposition gas including a source gas, a purge gas, and a reactive gas, provided inside the case, And the gas supply unit is formed in a multi-stage shape with respect to the height direction of the case, and the atomic layer deposition gas is diffused from one side to the other side through diffusion holes provided for each stage .
Description
The present invention relates to atomic layer deposition techniques used in semiconductor or display device fabrication, and more particularly to a gas supply module for atomic layer deposition.
In general, a method of depositing a thin film having a predetermined thickness on a substrate such as a semiconductor substrate or a glass substrate includes physical vapor deposition (PVD) using physical collision such as sputtering, And chemical vapor deposition (CVD).
In recent years, as the design rule of a semiconductor device becomes very minute, a thin film of a fine pattern is required and a step of a region where a thin film is formed is greatly increased, so that a fine pattern of atomic layer thickness can be formed very uniformly There is an increasing use of atomic layer deposition (ALD) as well as excellent step coverage.
This atomic layer deposition method is similar to the general chemical vapor deposition method in that it utilizes a chemical reaction between gas molecules. However, unlike conventional CVD in which a plurality of gaseous molecules are injected into a process chamber at the same time and the resulting reaction product is deposited on the substrate, the atomic layer deposition method injects a gas containing one source material into the process chamber, There is a difference in that a product by chemical reaction between the source material on the substrate surface is deposited by adsorbing on the substrate and then injecting a gas containing another source material into the process chamber.
However, the atomic layer deposition method currently being investigated has a problem that the productivity is low because the atomic layer deposition method can not be uniformly performed in spraying the deposition gas onto the substrate. Therefore, a gas supply module capable of uniformly spraying the deposition gas to maintain the high quality of the atomic layer deposition thin film but improve the productivity is proposed.
An embodiment of the present invention provides a gas supply module for atomic layer deposition capable of uniformly injecting gas into a substrate used for semiconductor or display device manufacture through a plurality of holes through which gas is passed stepwise.
Also, in one embodiment of the present invention, a gas supply module for atomic layer deposition capable of preventing introduction of a gas to be injected by forming a gas barrier using a gas when the gas is injected into the substrate is provided.
The problems to be solved by the present invention are not limited to the above-mentioned problem (s), and another problem (s) not mentioned can be clearly understood by those skilled in the art from the following description.
The gas supply module for atomic layer deposition according to an embodiment of the present invention includes a case and an atomic layer deposition gas provided inside the case and including a source gas, a purge gas, and a reaction gas, And the gas supply unit is formed in a multi-stage shape with respect to a height direction of the case, and the atomic layer deposition gas is diffused from one side to the other side through diffusion holes provided for each stage, .
Further, the gas supply unit according to an embodiment of the present invention includes a source gas supply unit for injecting the source gas, a purge gas supply unit for supplying the purge gas, and a reaction gas supply unit for injecting the reaction gas, The supply part, the purge gas supply part, and the reaction gas supply part may be arranged side by side at regular intervals along the longitudinal direction of the case.
According to an embodiment of the present invention, the gas supply unit may include a first gas diffusion region, which is a space formed on the gas supply unit, a source gas supply unit, and a reactive gas supply unit, And a third gas diffusion region formed in the source gas supply unit and the reaction gas supply unit, the third gas diffusion region being a space connected to the second gas diffusion region.
According to an embodiment of the present invention, the first to third gas diffusion regions may include a first gas diffusion region, a second gas diffusion region, and a second gas diffusion region provided between the first gas diffusion region and the second gas diffusion region, A second gas barrier layer provided between the third gas diffusion regions and a third barrier rib provided below the third gas diffusion region, wherein the diffusion holes are formed in a plurality of .
In addition, the diffusion holes may be formed at regular intervals along the longitudinal direction of the first to third barrier ribs according to an embodiment of the present invention.
In addition, the diffusion holes according to the embodiment of the present invention may be formed to face each other at corresponding positions of one side surface and the other side surface of each partition wall.
In addition, the number of the diffusion holes according to an embodiment of the present invention can satisfy the following expression.
[Equation]
The number of diffusion holes formed in the first bank, the number of diffusion holes formed in the second bank, and the number of diffusion holes formed in the third bank.
The number of diffusion holes formed in the first bank is 3 to 5, the number of diffusion holes formed in the second bank is 8 to 12, and the number of diffusion holes formed in the third bank is 240 to 260 pieces.
In addition, the gas supply module for atomic layer deposition according to an embodiment of the present invention may further include an outer purge gas supply unit disposed on the outer periphery so as to surround the gas supply unit, the outer purge gas supply unit being communicated with each other.
The distance between the purge gas supply unit and the deposition target substrate may be set to a distance between the reaction gas supply unit and the deposition target substrate, The distance between the source gas supply unit and the deposition target substrate may be smaller than the distance between the source gas supply unit and the deposition target substrate.
The details of other embodiments are included in the detailed description and the accompanying drawings.
According to an embodiment of the present invention, gas can be uniformly injected into a substrate used for manufacturing a semiconductor or a display device through a plurality of holes through which gas is passed stepwise.
Further, according to an embodiment of the present invention, when the gas is injected into the substrate, a gas barrier made of a gas is formed, thereby preventing the introduction of the injected gas.
1 is a perspective view of a gas supply module for atomic layer deposition according to an embodiment of the present invention, showing a top cross-section of a gas supply module.
FIG. 2 is a plan view of a gas supply module for atomic layer deposition according to an embodiment of the present invention, showing a lower section of a gas supply module. FIG.
3 is a plan view showing a cross-section AA 'of the gas supply module of FIG.
4 is a plan view showing an internal structure of a gas supply module in an embodiment of the present invention.
FIGS. 5A through 5C are graphs showing experimental results on the flow of a fluid according to a separation distance between a purge gas supply unit and a substrate to be deposited, in an embodiment of the present invention. FIG.
FIG. 6 is a view illustrating a process of spraying a deposition gas through a gas diffusion region of a gas supply unit according to an embodiment of the present invention. Referring to FIG.
BRIEF DESCRIPTION OF THE DRAWINGS The advantages and / or features of the present invention, and how to accomplish them, will become apparent with reference to the embodiments described in detail below with reference to the accompanying drawings. It should be understood, however, that the invention is not limited to the disclosed embodiments, but is capable of many different forms and should not be construed as limited to the embodiments set forth herein. Rather, these embodiments are provided so that this disclosure will be thorough and complete, To fully disclose the scope of the invention to those skilled in the art, and the invention is only defined by the scope of the claims. Like reference numerals refer to like elements throughout the specification.
Hereinafter, embodiments of the present invention will be described in detail with reference to the accompanying drawings.
The atomic layer deposition equipment gas module according to an embodiment of the present invention can form various thin film layers. For example, at least one thin film layer of a metal thin film layer, an oxide thin film layer, a nitride thin film layer, a carbide thin film layer, and a sulfide thin film layer can be formed. According to one embodiment, the source gas for forming the metal thin film layer is one of TMA (TriMethyl Aluminum), TEA (Tri Ethyl Aluminum) and DMACl (Di Methyl Aluminum Chloride), and the reactive gas is oxygen gas and ozone gas ≪ / RTI > At this time, the purge gas may be any one of argon (Ar), nitrogen (N2), and helium (He) or a mixture of two or more gases. According to another embodiment, the source gas for forming the silicon thin film layer may be one of silane (SiH4), disilane (Si2H6) and silicon tetrafluoride (SiF4) containing ricons, May be one of an oxygen gas and an ozone gas. At this time, the purge gas may be any one of argon (Ar), nitrogen (N2), and helium (He), or a mixture of two or more gases. At this time, the source gas, the purge gas, and the reaction gas are not limited to these, and may be changed according to the needs of those skilled in the art.
A gas supply module for atomic layer deposition according to an embodiment of the present invention is a module for injecting gas into a substrate to be deposited for depositing an atomic layer thin film and includes a case and a gas supply unit provided inside the case, . A suction module (not shown) for suctioning the gas may be mounted on the upper portion of the case. In this embodiment, five suction modules may be mounted. The gas supply unit injects an atomic layer deposition gas containing a source gas, a purge gas, and a reactive gas into another region of the substrate to be deposited. Hereinafter, with reference to Figs. 1 to 4, the gas supply unit will be described in more detail.
FIG. 1 is a perspective view illustrating a gas supply module for atomic layer deposition according to an embodiment of the present invention, and FIG. 2 is a cross- FIG. 3 is a plan view showing a cross-section taken along the line AA 'of the gas supply module of FIG. 1, and FIG. 4 is a cross- Fig. 7 is a plan view showing the internal structure of the supply module.
1 and 2, the
Meanwhile, in the present embodiment, the outer purge
For reference, the outer purge
Referring to FIG. 3, the
A
The
The first and second source
According to the present embodiment, each
An exhaust port 122c for exhausting the source gas injected from the first source
The exhaust ports 122c and 126d can communicate with a bar dry pump (not shown). By the driving of the bar dry pump, the source gas and / or the reactive gas out of the corresponding region of the substrate among the source gas and / or reactive gas injected in the top pumping manner can be exhausted.
Referring to FIG. 4, the
In this regard, in the present embodiment, an experiment was conducted to determine the flow of the fluid according to the separation distance h2 between the purge
The
The first
The first to third
The first to
A plurality of
The diffusion holes 12a, 22a, and 32a may be formed to face each other at a corresponding position on one side surface and the other side surface of each partition wall. Specifically, the
The number of the
[Equation]
The number of
More specifically, the number of the diffusion holes 22a formed on the lower side of the
While the present invention has been described in connection with what is presently considered to be practical exemplary embodiments, it is to be understood that the invention is not limited to the disclosed embodiments. Therefore, the scope of the present invention should not be limited to the described embodiments, but should be determined by the scope of the appended claims and equivalents thereof.
While the present invention has been particularly shown and described with reference to exemplary embodiments thereof, it is to be understood that the invention is not limited to the disclosed exemplary embodiments, but, on the contrary, Modification is possible. Accordingly, the spirit of the present invention should be understood only in accordance with the following claims, and all equivalents or equivalent variations thereof are included in the scope of the present invention.
10: first gas diffusion region
12: first partition
20: second gas diffusion region
22: second partition
30: first gas diffusion region
32: first partition
110: Case
120: gas supply unit
122: source gas supply unit
122a: a first source gas supply part
122b: the second source gas supply part
124: purge gas supply unit
124a: first purge gas supply part
124b: the second purge gas supply part
124c: third purge gas supply part
124d: fourth purge gas supply section
126: Reaction gas supply unit
126a: the first reaction gas supply part
126b: the second reaction gas supply part
126c: the third reaction gas supply part
122c, 126d:
128: outer purge gas supply part
12a, 22a, 32a: diffusion holes
130: stage
Claims (10)
And a gas supply unit provided in the case and injecting an atomic layer deposition gas containing a source gas, a purge gas, and a reactive gas into another region of the substrate to be vaporized at the same time,
The gas supply part
The atomic layer deposition gas is diffused from one side to the other side through diffusion holes provided for each stage,
The gas supply part
A purge gas supply unit for supplying the purge gas and a reaction gas supply unit for spraying the reaction gas,
Wherein the source gas supply unit, the purge gas supply unit, and the reaction gas supply unit are arranged side by side at regular intervals along the longitudinal direction of the case,
Further comprising an outer purge gas supply unit disposed at an outer periphery along the circumferential direction of the gas supply unit and communicating with each other for separating an inner space to which gas is supplied and an outer space to which no gas is supplied,
The gas supply part
A first gas diffusion region that is a space formed in an upper portion of the gas supply unit;
A second gas diffusion region formed in the source gas supply unit and the reaction gas supply unit, the second gas diffusion region being a space connected to the first gas diffusion region; And
And a third gas diffusion region formed in the source gas supply unit and the reaction gas supply unit, the third gas diffusion region being a space connected to the second gas diffusion region,
The first to third gas diffusion regions
A first gas barrier provided between the first gas diffusion region and the second gas diffusion region;
A second gas barrier provided between the second gas diffusion region and the third gas diffusion region; And
And a third partition disposed below the third gas diffusion region,
The diffusion holes are formed at a plurality of positions on the upper and lower surfaces of the first to third barrier ribs. The diffusion holes are formed at regular intervals along the longitudinal direction of the first to third barrier ribs, Lt; / RTI >
Characterized in that the number of diffusion holes satisfies the following equation.
[Equation]
The number of diffusion holes formed in the first bank, the number of diffusion holes formed in the second bank, and the number of diffusion holes formed in the third bank.
Wherein the number of diffusion holes formed in the first barrier rib is 3 to 5, the number of diffusion holes formed in the second barrier rib is 8 to 12, and the number of diffusion holes formed in the third barrier rib is 240 to 260. Gas supply module for deposition.
The substrate to be vapor-deposited is provided on the other side of the gas supply unit,
The separation distance between the purge gas supply unit and the deposition target substrate
Wherein the distance between the reaction gas supply unit and the deposition target substrate is smaller than the distance between the source gas supply unit and the deposition target substrate.
Priority Applications (2)
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KR1020170048384A KR101972389B1 (en) | 2017-04-14 | 2017-04-14 | Gas supply module for atomic layer deposition |
PCT/KR2018/004393 WO2018190696A1 (en) | 2017-04-14 | 2018-04-16 | Gas supply module for atomic layer deposition |
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KR1020170048384A KR101972389B1 (en) | 2017-04-14 | 2017-04-14 | Gas supply module for atomic layer deposition |
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KR20180115912A KR20180115912A (en) | 2018-10-24 |
KR101972389B1 true KR101972389B1 (en) | 2019-04-25 |
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WO (1) | WO2018190696A1 (en) |
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WO2022169065A1 (en) * | 2021-02-08 | 2022-08-11 | 주식회사 넥서스비 | Roll-to-roll atomic layer deposition apparatus |
KR20230100987A (en) | 2021-12-29 | 2023-07-06 | 주식회사 넥서스비 | Atmoic layer depositing apparatus and atmoic layer depositing method using the same |
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KR20090097401A (en) * | 2008-03-11 | 2009-09-16 | (주)퓨전에이드 | Apparatus and method for depositing thin film |
EP2159304A1 (en) * | 2008-08-27 | 2010-03-03 | Nederlandse Organisatie voor toegepast- natuurwetenschappelijk onderzoek TNO | Apparatus and method for atomic layer deposition |
KR20110076386A (en) | 2009-12-29 | 2011-07-06 | 세메스 주식회사 | Atomic layer depositon apparatus used in manufacturing semiconductor device |
KR102070400B1 (en) * | 2012-06-29 | 2020-01-28 | 주성엔지니어링(주) | Apparatus and method for processing substrate |
KR101526861B1 (en) * | 2013-08-16 | 2015-06-09 | 주식회사 테스 | Gas supply unit and thin film deposition apparatus having the same |
KR102150361B1 (en) * | 2014-02-19 | 2020-09-01 | 주식회사 케이씨텍 | Atomic layer deposition apparatus |
KR20160053493A (en) * | 2014-11-05 | 2016-05-13 | 주식회사 케이씨텍 | Gas supplying device and atomic layer deposition apparatus having the same |
KR20160134908A (en) * | 2015-05-13 | 2016-11-24 | 참엔지니어링(주) | Substrate processing apparatus |
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KR20180115912A (en) | 2018-10-24 |
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