KR101291757B1 - 나노결정 비스무트-몰리브덴 혼합 산화물의 제조 방법 - Google Patents

나노결정 비스무트-몰리브덴 혼합 산화물의 제조 방법 Download PDF

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KR101291757B1
KR101291757B1 KR1020107024681A KR20107024681A KR101291757B1 KR 101291757 B1 KR101291757 B1 KR 101291757B1 KR 1020107024681 A KR1020107024681 A KR 1020107024681A KR 20107024681 A KR20107024681 A KR 20107024681A KR 101291757 B1 KR101291757 B1 KR 101291757B1
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bismuth
mixed oxide
molybdenum
molybdenum mixed
nanocrystalline
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KR20100134091A (ko
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알프레드 하게메이어
올리버 웨그너
실비아 네우만
한스-조르그 워크
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쉬드-케미 아이피 게엠베하 운트 코 카게
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    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G39/00—Compounds of molybdenum
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/002—Mixed oxides other than spinels, e.g. perovskite
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/16—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B01J23/24—Chromium, molybdenum or tungsten
    • B01J23/31—Chromium, molybdenum or tungsten combined with bismuth
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B01J23/76—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36
    • B01J23/84—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36 with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B01J23/85—Chromium, molybdenum or tungsten
    • B01J23/88—Molybdenum
    • B01J23/887—Molybdenum containing in addition other metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36
    • B01J23/8876—Arsenic, antimony or bismuth
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/70—Catalysts, in general, characterised by their form or physical properties characterised by their crystalline properties, e.g. semi-crystalline
    • B01J35/77—Compounds characterised by their crystallite size
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/0009—Use of binding agents; Moulding; Pressing; Powdering; Granulating; Addition of materials ameliorating the mechanical properties of the product catalyst
    • B01J37/0027—Powdering
    • B01J37/0045—Drying a slurry, e.g. spray drying
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/0236—Drying, e.g. preparing a suspension, adding a soluble salt and drying
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/08—Heat treatment
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G39/00—Compounds of molybdenum
    • C01G39/006—Compounds containing molybdenum, with or without oxygen or hydrogen, and containing two or more other elements
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G53/00—Compounds of nickel
    • C01G53/80—Compounds containing nickel, with or without oxygen or hydrogen, and containing one or more other elements
    • C01G53/82—Compounds containing nickel, with or without oxygen or hydrogen, and containing two or more other elements
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/21—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
    • C07C51/25—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of unsaturated compounds containing no six-membered aromatic ring
    • C07C51/252—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of unsaturated compounds containing no six-membered aromatic ring of propene, butenes, acrolein or methacrolein
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2523/00—Constitutive chemical elements of heterogeneous catalysts
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J35/61—Surface area
    • B01J35/612—Surface area less than 10 m2/g
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J35/61—Surface area
    • B01J35/613—10-100 m2/g
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/0215—Coating
    • B01J37/0232—Coating by pulverisation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/03—Precipitation; Co-precipitation
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/70—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
    • C01P2002/72—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by d-values or two theta-values, e.g. as X-ray diagram
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/51—Particles with a specific particle size distribution
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/12—Surface area

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Catalysts (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)
KR1020107024681A 2008-04-04 2009-04-03 나노결정 비스무트-몰리브덴 혼합 산화물의 제조 방법 Expired - Fee Related KR101291757B1 (ko)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
DE102008017308.8 2008-04-04
DE102008017308.8A DE102008017308B4 (de) 2008-04-04 2008-04-04 Verfahren zur Herstellung von nanokristallinen Bismut-Molybdänmischoxidkatalysatoren
PCT/EP2009/002475 WO2009121625A1 (de) 2008-04-04 2009-04-03 Verfahren zur herstellung von nanokristallinem bismut-molybdänmischoxid

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KR20100134091A KR20100134091A (ko) 2010-12-22
KR101291757B1 true KR101291757B1 (ko) 2013-07-31

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US (1) US8480998B2 (enExample)
EP (1) EP2260004B1 (enExample)
JP (1) JP5458088B2 (enExample)
KR (1) KR101291757B1 (enExample)
CN (1) CN101983174A (enExample)
BR (1) BRPI0910602A2 (enExample)
DE (1) DE102008017308B4 (enExample)
WO (1) WO2009121625A1 (enExample)
ZA (1) ZA201006739B (enExample)

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DE102013004755B4 (de) 2013-03-20 2014-12-11 Clariant International Ltd. Kompositmaterial enthaltend ein Bismut-Molybdän-Nickel-Mischoxid oder ein Bismut-Molybdän-Cobalt-Mischoxid und SiO2
KR101554318B1 (ko) 2013-05-24 2015-09-18 주식회사 엘지화학 아크롤레인 및 아크릴산 제조용 촉매와 이의 제조 방법
WO2016032284A1 (ko) * 2014-08-29 2016-03-03 주식회사 엘지화학 봉형 산화 몰리브덴의 제조방법 및 산화 몰리브덴 복합체의 제조방법
US9815045B2 (en) 2015-03-23 2017-11-14 Clariant Corporation Metal oxide catalyst material and processes for making and using same
EP3120926A1 (de) * 2015-07-20 2017-01-25 Evonik Degussa GmbH Verfahren zur herstellung von mischoxidkatalysatoren
JP6906541B2 (ja) 2015-11-16 2021-07-21 ヒーリー，エルエルシー エネルギー貯蔵、触媒、光電池およびセンサーの用途のための合成された表面官能化・酸性化金属酸化物材料
WO2020252389A1 (en) 2019-06-12 2020-12-17 HHeLI, LLC Blended active materials for battery cells
WO2018093945A1 (en) 2016-11-15 2018-05-24 Hheli, Llc. A surface-functionalized, acidified metal oxide material in an acidified electrolyte system or an acidified electrode system
EP3323510A1 (en) * 2016-11-21 2018-05-23 Evonik Degussa GmbH Process for the preparation of a mixed oxide catalyst by flame spray pyrolysis
US10479759B2 (en) 2017-02-08 2019-11-19 Clariant Corporation Synthetic methods for the preparation of propylene ammoxidation catalysts
US10479760B2 (en) 2017-02-08 2019-11-19 Clariant Corporation Synthetic methods for the preparation of propylene ammoxidation catalysts
CA3292115A1 (en) 2017-04-10 2025-11-29 HHeLI, LLC A battery cathode nanomaterial comprising an acidified tin oxide
CN110945689B (zh) 2017-05-17 2023-08-18 氢氦锂有限公司 具有新型组分的电池单元
JP7309619B2 (ja) 2017-05-17 2023-07-18 ヒーリー，エルエルシー 酸性化カソードおよびリチウムアノードを有する電池
CN106984299B (zh) * 2017-05-27 2019-04-23 北方民族大学 水热合成三维Bi4MoO9/TiO2纳米结构异质结的方法
US10978731B2 (en) 2017-06-21 2021-04-13 HHeLI, LLC Ultra high capacity performance battery cell
CA3076501A1 (en) 2017-09-22 2019-03-28 HHeLI, LLC Construction of ultra high capacity performance battery cells
DE102018205398A1 (de) * 2018-04-10 2019-10-10 Fraunhofer-Gesellschaft zur Förderung der angewandten Forschung e.V. Verfahren zur Herstellung von Mischoxid-Pulvern sowie ein Mischoxid-Pulver
CN112867932B (zh) 2018-09-10 2025-04-15 氢氦锂有限公司 超高容量性能电池单元的使用方法
JP7170375B2 (ja) * 2019-03-18 2022-11-14 日本化薬株式会社 触媒及びそれを用いた不飽和アルデヒド、不飽和カルボン酸の製造方法
US12278342B2 (en) 2019-06-12 2025-04-15 HHeLI, LLC Alkaline and acidified metal oxide blended active materials
CN113019442B (zh) * 2019-12-09 2022-05-17 中国科学院大连化学物理研究所 一种担载型丙烯氧化制丙烯酸催化剂及其制备和应用
KR102795505B1 (ko) * 2020-10-16 2025-04-11 주식회사 엘지화학 몰리브덴-비스무트계 복합 금속 산화물의 제조방법
DE102021108191A1 (de) 2021-03-31 2022-10-06 Clariant Produkte (Deutschland) Gmbh Molybdän-bismut-eisen-nickel-mischoxid-material und verfahren zu dessen herstellung

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JP5458088B2 (ja) 2014-04-02
JP2011516377A (ja) 2011-05-26
WO2009121625A1 (de) 2009-10-08
ZA201006739B (en) 2011-09-28
CN101983174A (zh) 2011-03-02
EP2260004A1 (de) 2010-12-15
US8480998B2 (en) 2013-07-09
DE102008017308B4 (de) 2014-09-25
BRPI0910602A2 (pt) 2015-09-22
US20110092734A1 (en) 2011-04-21
KR20100134091A (ko) 2010-12-22
DE102008017308A1 (de) 2009-10-08
EP2260004B1 (de) 2018-06-27

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