KR100611561B1 - A mildewcide composition using NaOH, wood vinegar liquor, SiO2, platycodon root, chitosan - Google Patents

A mildewcide composition using NaOH, wood vinegar liquor, SiO2, platycodon root, chitosan Download PDF

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KR100611561B1
KR100611561B1 KR1020040028820A KR20040028820A KR100611561B1 KR 100611561 B1 KR100611561 B1 KR 100611561B1 KR 1020040028820 A KR1020040028820 A KR 1020040028820A KR 20040028820 A KR20040028820 A KR 20040028820A KR 100611561 B1 KR100611561 B1 KR 100611561B1
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chitosan
naoh
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wood vinegar
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Abstract

본 발명은 식물의 흰가루병 과 곰팡이병 예방 및 억제, 나아가서는 치료에 관한 조성물로서, 더욱 상세하게는 각종 식물의 곰팡이병에 적용시 곰팡이균의 포자를 분해하고 세포막을 파괴하여 식물의 정상적인 성장을 도와 주며, 비료성분으로서 조성된 물질이므로 식물에게 영양을 주며 곰팡이 균을 사멸시킴으로 사람과 식물과 토양이 농약으로부터 벗어날 수 있는 친환경적인 조성물 및 그 제조법에 관한 것으로 농약 사용절감과 환경오염방지는 물론 농가소득을 증대시키고자 한다.The present invention is a composition related to the prevention and suppression, further treatment of powdery mildew and fungal diseases of plants, and more particularly, when applied to fungal diseases of various plants to decompose spores of fungi and destroy cell membranes to help the normal growth of plants. It is a substance that is formulated as a fertilizer, and it provides nutrition to plants and kills fungi, and it is an eco-friendly composition and method of manufacturing that can free people, plants and soil from pesticides. To increase

NaOH, 목초액, 규산, 길경, 키토산, 흰가루병, 곰팡이병NaOH, wood vinegar, silicic acid, Giltyeong, chitosan, powdery mildew, fungal disease

Description

NaOH와 목초액, 규산, 길경 및 키토산을 이용한 흰가루병 예방, 치료 및 억제용 살균제 조성물{A mildewcide composition using NaOH, wood vinegar liquor, SiO2, platycodon root, chitosan}A mildewcide composition using NaOH, wood vinegar liquor, SiO2, platycodon root, chitosan using NaOH, wood vinegar, silicic acid, gilyeong and chitosan

도 1은 본 발명에 따른 살균제 조성물의 제조공정도를 나타낸 것이다.Figure 1 shows a manufacturing process of the fungicide composition according to the present invention.

본 발명은 수용성규산, NaOH 및 유기성자재인 길경, 목초액, 키토산을 첨가하여 친환경적 흰가루병과 곰팡이억제용 조성물과 그 제조법에 관한 것이다. 종래의 기술로 제조되는 흰가루와 곰팡이억제 조성물은 대부분 살균제계열의 화학농약으로 다량 반복 사용에 따라 토양 및 수계에 오염을 유발할 수 있는 문제점을 갖고 있다.The present invention relates to an environment-friendly powdery mildew and mildew inhibiting composition and its manufacturing method by adding water-soluble silicic acid, NaOH, and organic materials such as Gilkyung, herbaceous acid, and chitosan. White powder and mold inhibitor composition prepared by the prior art has a problem that can cause contamination in soil and water according to the repeated use of a large amount of chemical pesticides of most fungicides.

따라서 본 발명은 토양 및 수계에 영향을 주지 않고 흰가루와 곰팡이에 효과적으로 작용하여 이들에 의한 병해방지와 농가소득증대를 이루고자하며 병 방제는 물론 미네랄을 함유하여 작물에 영양을 공급하여 작물의 안정된 생육을 도모하고 품질을 향상시킬 수 있는 친환경적 농업자재를 개발하는 것이다.Therefore, the present invention is effective to white powder and mold without affecting the soil and water system to achieve disease prevention and increase farm household income by these, and to provide stable nutrition of crops by supplying nutrients to the crop containing minerals as well as disease control. It is to develop eco-friendly agricultural materials that can promote and improve quality.

본 발명은 수용성규산, NaOH 및 유기성자재인 길경, 목초액, 키토산을 첨가하여 친환경적 흰가루병과 곰팡이억제용 조성물과 그 제조법에 관한 것이며 사용된 원료와 특성은 다음과 같다.The present invention relates to an environment-friendly powdery mildew and mildew suppression composition and a method for preparing the same by adding water-soluble silicic acid, NaOH and organic materials such as Gilkyung, herbaceous acid, and chitosan. The raw materials and properties used are as follows.

규산은 액상규산나트륨(L-sodium silicate, Na2O·SiO2·H2O)을 사용하였으며 특성은 표 1과 같다.Silicate was used as liquid sodium silicate (L-sodium silicate, Na 2 O · SiO 2 · H 2 O) and its properties are shown in Table 1.

[표 1] 액상규산나트륨의 특성[Table 1] Characteristics of liquid sodium silicate

Figure 112004506476028-pat00001
Figure 112004506476028-pat00001

NaOH는 98％순도의 시약을 사용하였으며 길경은 도라지의 껍질을 벗기거나 그대로 건조한 것으로 사포닌을 함유하여 세포에 대해서는 표면 활성제로서 작용하여, 세포막의 구조를 파괴하거나, 물질의 투과성을 높이는 작용을 한다. 목초액은 참나무로 제조한 것으로 목초액의 원료가 되는 원목의 주성분은 탄수화물인 셀롤로오스성분(헤미세룰로오스와 셀룰로오스로 전체의 70∼75％)과 탄화수소인 리그닌(전체의 20∼25％)인데 이것이 전체의 95％를 차지하며 살균 및 미네랄을 함유하여 작물에 영양을 공급해준다. 키토산은 게나 가재, 새우 껍데기에 들어 있는 키틴을 탈아세틸화하여 얻어낸 물질을 말한다. 1811년 프랑스의 자연사학자 브라코노가 버섯에 포함되어 있는 미지의 성분, 즉 키틴을 발견한 것이 시초이다. 그 후 1859년 화학자 루게가 키틴을 아세틸화하여 새로운 물질을 얻어냈으며, 1894년에 과학자 후페 자이라가 이를 키토산이라 명명하였다. 특성은 노폐해진 세포를 활성화 및 면역력을 강화해주는데 본 발명에 사용된 키토산은 게껍질에서 추출하였으며 키틴함량은 4％이다.NaOH used 98% purity reagent and Gilkyung peeled or dried as it is, saponin contained as saponin and acts as a surface activator for the cell, destroying the structure of the cell membrane or enhancing the permeability of the material. Wood vinegar is made from oak, and the main component of the wood, which is the raw material of wood vinegar, is cellulose component (70-75% of all hemicellulose and cellulose) of carbohydrate and lignin (20-25% of the whole) It accounts for 95% of the total and contains sterile and minerals to nourish crops. Chitosan refers to a substance obtained by deacetylating chitin in crabs, crayfish, and shrimp shells. In 1811, French natural historian Bracono discovered the unknown ingredient, chitin, contained in mushrooms. Later, in 1859, the chemist Rugue acetylated chitin to obtain a new material, which in 1894 was named chitosan. The characteristics activate activated cells and enhance immunity. The chitosan used in the present invention was extracted from the crab shell and the chitin content was 4%.

이들 원료의 혼합에 의한 흰가루병과 곰팡이 억제를 위한 액상조성물을 제조하는 발명의 상세한 설명은 다음과 같다.Detailed description of the invention for producing a liquid composition for suppressing powdery mildew and mildew by mixing these raw materials is as follows.

(1) 액상혼합물을 제조하는 공정(1) Process of producing a liquid mixture

물 100ℓ(≒100Kg)에 대하여 순도 98％의 NaOH를 35∼45㎏을 완전히 녹인 후 목초액 25∼35㎏을 첨가하고 액상 규산나트륨 3.0∼4.0㎏과 키토산 2.5∼3.5㎏을 넣어 액상 혼합물을 제조한다.Dissolve 35-45 kg of NaOH with a purity of 98% NaOH with 100 L of water, add 25-35 kg of wood vinegar, and add 3.0-4.0 kg of liquid sodium silicate and 2.5-3.5 kg of chitosan to prepare a liquid mixture. .

〈실시예 1〉<Example 1>

NaOH를 물 100리터에 35kg을 완전히 녹인 후 목초액 25kg을 첨가하고 액상규산나트륨 3.0kg과 키토산 2.5kg을 넣어 액상혼합물을 제조한다.After dissolving 35 kg of NaOH in 100 liters of water, 25 kg of wood vinegar is added and 3.0 kg of liquid sodium silicate and 2.5 kg of chitosan are added to prepare a liquid mixture.

〈실시예 2〉<Example 2>

NaOH를 물 100리터에 40kg을 완전히 녹인 후 목초액 30kg을 첨가하고 액상규산나트륨 3.5kg과 키토산 3.0kg을 넣어 액상혼합물을 제조한다.After dissolving 40 kg NaOH completely in 100 liters of water, 30 kg of wood vinegar is added and 3.5 kg of liquid sodium silicate and 3.0 kg of chitosan are added to prepare a liquid mixture.

〈실시예 3〉<Example 3>

NaOH를 물 100리터에 45kg을 완전히 녹인 후 목초액 35kg을 첨가하고 액상규산나트륨 4.0kg과 키토산 3.5kg을 넣어 액상혼합물을 제조한다.After dissolving 45 kg of NaOH in 100 liters of water, 35 kg of wood vinegar is added and 4.0 kg of liquid silicate and 3.5 kg of chitosan are added to prepare a liquid mixture.

(2) 길경첨가에 의한 최종 혼합조성물을 제조하는 공정(2) Process of preparing final mixed composition by way of street light

실시예 1, 2, 3에 따라 제조한 조성물에 길경의 함량을 0.1∼1.0중량％로 달리하여 첨가하여 최종 혼합조성물을 제조한다.To the composition prepared according to Examples 1, 2 and 3, the content of the path diameter was added differently from 0.1 to 1.0% by weight to prepare a final mixed composition.

〈실시예 4〉<Example 4>

실시예 1의 액상혼합물 100리터에 길경 100g을 균일하게 혼합한다. 마찬가지로 실시예 1의 액상혼합물 100리터에 길경 500g을 균일하게 혼합(실시예 5), 실시예 1의 액상혼합물 100리터에 길경 1000g을 균일하게 혼합(실시예 6), 실시예 2의 액상혼합물 100리터에 길경 100g을 균일하게 혼합(실시예 7), 실시예 2의 액상혼합물 100리터에 길경 500g을 균일하게 혼합(실시예 8), 실시예 2의 액상혼합물 100리터에 길경 1000g을 균일하게 혼합(실시예 9), 실시예 3의 액상혼합물 100리터에 길경 100g을 균일하게 혼합(실시예 10), 실시예 3의 액상혼합물 100리터에 길경 500g을 균일하게 혼합(실시예 11), 실시예 3의 액상혼합물 100리터에 길경 1000g을 균일하게 혼합(실시예 12)하여 최종 혼합조성물을 제조한다.To 100 liters of the liquid mixture of Example 1, 100 g of the path diameter is uniformly mixed. Similarly, 500 g of a long diameter was uniformly mixed with 100 liters of the liquid mixture of Example 1 (Example 5), and 1000 g of a long diameter was uniformly mixed with 100 liters of the liquid mixture of Example 1 (Example 6), 100 of the liquid mixture of Example 2 Uniformly mixing 100 g of the long diameter in the liter (Example 7), uniformly mixing 500 g of the long diameter in the 100 liters of the liquid mixture of Example 2 (Example 8), uniformly mixing 1000 g of the long diameter in 100 liters of the liquid mixture of Example 2 (Example 9), 100 g of length diameter was uniformly mixed with 100 liters of the liquid mixture of Example 3 (Example 10), 500 g of length diameter was uniformly mixed with 100 liters of the liquid mixture of Example 3 (Example 11), Example To 100 liters of the liquid mixture of 3 uniformly mixed with a diameter of 1000g (Example 12) to prepare a final mixed composition.

이상의 실시예에서 제조한 혼합조성물의 흰가루병 및 곰팡이억제에 대한 작물재배실험을 실시한 결과는 다음과 같다.Crop cultivation experiments for powdery mildew and mold suppression of the mixed composition prepared in the above examples are as follows.

〈작물실험〉〈Crop Experiments〉

본 발명에서 제조한 혼합조성물의 비효시험을 대전광역시 우명동에 소재한 연동 시설하우스 600평에서 2003년 10월에 딸기를 정식하여 12월부터 2004년 4월에 실시하였다. 흰가루병의 병징이 나타나기 시작한 재배구를 10평으로 구분하여 본 혼합조성물 3ℓ/ha를 400배 희석하여 엽면시비한 결과최대 97％의 병억제 효과를 볼 수 있었으며 실시예에 따른 혼합조성물의 딸기에 대한 사용 효과는 표 2와 같 다.The fermentation test of the mixed composition prepared in the present invention was carried out from December to April 2004 in the form of strawberries in October 2003 at the 600 pyeong interlocking facility house located in Umyeong-dong, Daejeon. As a result of diluting the mixed composition 3ℓ / ha 400 times by dividing the cultivation zones starting to appear the symptoms of powdery mildew powder by 10 pyeong, the leaf inhibition effect of up to 97% was observed. The use effect is shown in Table 2.

[표 2] 혼합조성물의 흰가루병 억제효과[Table 2] Inhibition Effect of Powder Composition of Mixed Composition

Figure 112004506476028-pat00002
Figure 112004506476028-pat00002

Figure 112004506476028-pat00003
Figure 112004506476028-pat00003

표 2와 그림 1을 살펴본 결과 모든 처리구에서 92％ 이상의 흰가루병 억제를 보였으며, 특히 실시예 8, 11이 가장 높은 억제율을 보였다.As a result of looking at Table 2 and Figure 1, all treatments showed more than 92% powdery mildew inhibition, and in particular, Examples 8 and 11 showed the highest inhibition rate.

이상의 결과로부터 순도 98％의 NaOH를 물에 35∼45중량％, 목초액 25∼35중량％, 액상규산나트륨 3.0∼4.0중량％ 및 키토산 2.5∼3.5중량％를 넣어 제조한 액상혼합물에 길경 0.1∼1.0중량％를 첨가 및 균일하게 혼합하여 흰가루병과 곰팡이억제에 효과적인 최종혼합조성물을 제조할 수 있었다.From the above results, the liquid mixture prepared by adding NaOH having a purity of 98% to 35 to 45% by weight in water, 25 to 35% by weight of vinegar liquor, 3.0 to 4.0% by weight of liquid sodium silicate and 2.5 to 3.5% by weight of chitosan was used. By adding and uniformly mixing the weight percent it was possible to prepare a final mixture composition effective in suppressing powdery mildew and mildew.

이상에서 설명한 바와 같이 본 발명은 가성소다와 규산, 친환경자재인 목초액, 키토산 및 길경을 원료로 하여 흰가루병과 곰팡이억제에 우수한 효과를 나타내는 농업자재를 제공함으로써, 화학농약의 사용량과 방제횟수를 줄여 토양 및 수계 등의 환경생태계에 영향을 주지 않고 흰가루와 곰팡이에 효과적으로 작용하여 이들에 의한 병해방지와 농가소득증대와 더불어 병방제는 물론 미네랄을 함유하여 작물에 영양을 공급하여 작물의 안정된 생육을 도모하고 품질을 향상시킬 수 있을 것으로 기대된다. As described above, the present invention is made of caustic soda and silicic acid, environmentally friendly wood vinegar, chitosan, and Gilkyung as raw materials to provide agricultural materials exhibiting excellent effects on the control of powdery mildew and mildew, reducing the amount of chemical pesticides and the number of control soils It works effectively on white powder and mold without affecting the environmental ecosystem such as water and water, and prevents diseases caused by them and increases farm income, and also provides disease prevention and minerals to feed the crops to promote stable growth of crops. It is expected to be able to improve quality.

Claims (2)

물 100중량부를 기준으로 NaOH를 35∼45중량부, 목초액 25∼35중량부, 액상규산나트륨 3.0∼4.0중량부 및 키토산 2.5∼3.5중량부를 넣어 제조한 액상혼합물에 길경 0.1∼1.0중량부를 첨가 및 균일하게 혼합하여 얻어지는 흰가루병 예방, 치료 및 억제용 살균제 조성물.Add 0.1-1.0 parts by weight to a liquid mixture prepared by adding 35-45 parts by weight of NaOH, 25-35 parts by weight of wood vinegar solution, 3.0-4.0 parts by weight of liquid sodium silicate and 2.5-3.5 parts by weight of chitosan, based on 100 parts by weight of water. A fungicide composition for preventing, treating and inhibiting powdery mildew obtained by uniformly mixing. 제1항에 있어서, NaOH는 순도 98％이상, 액상 규산나트륨의 이산화규소(SiO2) 함량은 25.0∼35.0중량％, 목초액의 원료는 참나무, 키토산의 키틴함량은 3.7∼4.7중량％인 것을 특징으로 하는 흰가루병 예방, 치료 및 억제용 살균제 조성물.According to claim 1, NaOH is 98% or more purity, the content of silicon dioxide (SiO 2 ) of the liquid sodium silicate is 25.0 to 35.0% by weight, the raw material of the wood vinegar is oak, chitin content of chitosan is 3.7 to 4.7% by weight Fungicide composition for preventing, treating and inhibiting powdery mildew.
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