KR100550440B1 - 실리콘단결정 인상용 석영 유리 도가니 및 그의 제조방법 - Google Patents
실리콘단결정 인상용 석영 유리 도가니 및 그의 제조방법 Download PDFInfo
- Publication number
- KR100550440B1 KR100550440B1 KR1019990018459A KR19990018459A KR100550440B1 KR 100550440 B1 KR100550440 B1 KR 100550440B1 KR 1019990018459 A KR1019990018459 A KR 1019990018459A KR 19990018459 A KR19990018459 A KR 19990018459A KR 100550440 B1 KR100550440 B1 KR 100550440B1
- Authority
- KR
- South Korea
- Prior art keywords
- quartz glass
- single crystal
- crucible
- silicon dioxide
- glass crucible
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 title claims abstract description 251
- 239000013078 crystal Substances 0.000 title claims abstract description 81
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 title claims abstract description 74
- 229910052710 silicon Inorganic materials 0.000 title claims abstract description 74
- 239000010703 silicon Substances 0.000 title claims abstract description 74
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 30
- 239000000843 powder Substances 0.000 claims description 83
- 239000007789 gas Substances 0.000 claims description 58
- 238000000034 method Methods 0.000 claims description 36
- 238000010438 heat treatment Methods 0.000 claims description 28
- 238000002844 melting Methods 0.000 claims description 17
- 230000008018 melting Effects 0.000 claims description 17
- 239000002245 particle Substances 0.000 claims description 15
- 125000002887 hydroxy group Chemical group [H]O* 0.000 claims description 13
- 230000008021 deposition Effects 0.000 claims description 9
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims description 6
- 229910052739 hydrogen Inorganic materials 0.000 claims description 4
- 239000001257 hydrogen Substances 0.000 claims description 4
- 239000000758 substrate Substances 0.000 claims description 2
- 230000007547 defect Effects 0.000 abstract description 9
- 238000002425 crystallisation Methods 0.000 abstract description 6
- 230000008025 crystallization Effects 0.000 abstract description 6
- 239000010410 layer Substances 0.000 description 54
- 235000012239 silicon dioxide Nutrition 0.000 description 27
- 239000010453 quartz Substances 0.000 description 26
- 238000010891 electric arc Methods 0.000 description 12
- 238000001000 micrograph Methods 0.000 description 8
- 230000015572 biosynthetic process Effects 0.000 description 7
- 230000000052 comparative effect Effects 0.000 description 7
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 6
- 239000002994 raw material Substances 0.000 description 5
- 238000004458 analytical method Methods 0.000 description 4
- 229910002804 graphite Inorganic materials 0.000 description 4
- 239000010439 graphite Substances 0.000 description 4
- 229910021420 polycrystalline silicon Inorganic materials 0.000 description 4
- 229920005591 polysilicon Polymers 0.000 description 4
- 230000000694 effects Effects 0.000 description 3
- 238000004868 gas analysis Methods 0.000 description 3
- 239000011521 glass Substances 0.000 description 3
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 description 3
- 238000000465 moulding Methods 0.000 description 3
- 230000002093 peripheral effect Effects 0.000 description 3
- 229910052799 carbon Inorganic materials 0.000 description 2
- 239000003575 carbonaceous material Substances 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- AZDRQVAHHNSJOQ-UHFFFAOYSA-N alumane Chemical group [AlH3] AZDRQVAHHNSJOQ-UHFFFAOYSA-N 0.000 description 1
- 230000009172 bursting Effects 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 229910052906 cristobalite Inorganic materials 0.000 description 1
- 230000006837 decompression Effects 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 238000004880 explosion Methods 0.000 description 1
- 239000010419 fine particle Substances 0.000 description 1
- 238000005187 foaming Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000000155 melt Substances 0.000 description 1
- 238000012856 packing Methods 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 238000007493 shaping process Methods 0.000 description 1
- 239000000377 silicon dioxide Substances 0.000 description 1
- 229910052814 silicon oxide Inorganic materials 0.000 description 1
- 238000003980 solgel method Methods 0.000 description 1
- 239000002344 surface layer Substances 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 238000009423 ventilation Methods 0.000 description 1
Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C30—CRYSTAL GROWTH
- C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
- C30B15/00—Single-crystal growth by pulling from a melt, e.g. Czochralski method
- C30B15/10—Crucibles or containers for supporting the melt
- C30B15/12—Double crucible methods
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
- C03B19/00—Other methods of shaping glass
- C03B19/09—Other methods of shaping glass by fusing powdered glass in a shaping mould
- C03B19/095—Other methods of shaping glass by fusing powdered glass in a shaping mould by centrifuging, e.g. arc discharge in rotating mould
-
- C—CHEMISTRY; METALLURGY
- C30—CRYSTAL GROWTH
- C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
- C30B15/00—Single-crystal growth by pulling from a melt, e.g. Czochralski method
- C30B15/10—Crucibles or containers for supporting the melt
-
- C—CHEMISTRY; METALLURGY
- C30—CRYSTAL GROWTH
- C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
- C30B35/00—Apparatus not otherwise provided for, specially adapted for the growth, production or after-treatment of single crystals or of a homogeneous polycrystalline material with defined structure
- C30B35/002—Crucibles or containers
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S117/00—Single-crystal, oriented-crystal, and epitaxy growth processes; non-coating apparatus therefor
- Y10S117/90—Apparatus characterized by composition or treatment thereof, e.g. surface finish, surface coating
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T117/00—Single-crystal, oriented-crystal, and epitaxy growth processes; non-coating apparatus therefor
- Y10T117/10—Apparatus
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T117/00—Single-crystal, oriented-crystal, and epitaxy growth processes; non-coating apparatus therefor
- Y10T117/10—Apparatus
- Y10T117/1024—Apparatus for crystallization from liquid or supercritical state
- Y10T117/1032—Seed pulling
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T117/00—Single-crystal, oriented-crystal, and epitaxy growth processes; non-coating apparatus therefor
- Y10T117/10—Apparatus
- Y10T117/1024—Apparatus for crystallization from liquid or supercritical state
- Y10T117/1032—Seed pulling
- Y10T117/1052—Seed pulling including a sectioned crucible [e.g., double crucible, baffle]
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Crystallography & Structural Chemistry (AREA)
- Metallurgy (AREA)
- Manufacturing & Machinery (AREA)
- Crystals, And After-Treatments Of Crystals (AREA)
- Glass Melting And Manufacturing (AREA)
Applications Claiming Priority (4)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP1998-159880 | 1998-05-25 | ||
| JP15988098 | 1998-05-25 | ||
| JP02262899A JP4398527B2 (ja) | 1998-05-25 | 1999-01-29 | シリコン単結晶引き上げ用石英ガラスるつぼ |
| JP1999-022628 | 1999-01-29 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| KR19990088478A KR19990088478A (ko) | 1999-12-27 |
| KR100550440B1 true KR100550440B1 (ko) | 2006-02-08 |
Family
ID=26359887
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| KR1019990018459A Expired - Lifetime KR100550440B1 (ko) | 1998-05-25 | 1999-05-21 | 실리콘단결정 인상용 석영 유리 도가니 및 그의 제조방법 |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US6797061B2 (enExample) |
| EP (1) | EP1020546A4 (enExample) |
| JP (1) | JP4398527B2 (enExample) |
| KR (1) | KR100550440B1 (enExample) |
| TW (1) | TW509664B (enExample) |
| WO (1) | WO1999061685A1 (enExample) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR101406915B1 (ko) * | 2010-12-03 | 2014-06-12 | 쟈판 스파 쿼츠 가부시키가이샤 | 실리카 유리 도가니의 제조 방법 |
Families Citing this family (19)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP4549008B2 (ja) | 2002-05-17 | 2010-09-22 | 信越石英株式会社 | 水素ドープシリカ粉及びそれを用いたシリコン単結晶引上げ用石英ガラスルツボ |
| JP4086283B2 (ja) * | 2002-07-31 | 2008-05-14 | 信越石英株式会社 | シリコン単結晶引上げ用石英ガラスルツボおよびその製造方法 |
| US7427327B2 (en) * | 2005-09-08 | 2008-09-23 | Heraeus Shin-Etsu America, Inc. | Silica glass crucible with barium-doped inner wall |
| US7383696B2 (en) * | 2005-09-08 | 2008-06-10 | Heraeus Shin-Etsu America, Inc. | Silica glass crucible with bubble-free and reduced bubble growth wall |
| US20070084400A1 (en) * | 2005-10-19 | 2007-04-19 | General Electric Company | Quartz glass crucible and method for treating surface of quartz glass crucible |
| JP5046753B2 (ja) * | 2006-06-26 | 2012-10-10 | 信越化学工業株式会社 | 光ファイバ母材の製造方法及びその装置 |
| TWI408259B (zh) * | 2006-09-28 | 2013-09-11 | Shinetsu Quartz Prod | 具有鋇摻雜內壁的矽玻璃坩堝 |
| US7993556B2 (en) | 2007-08-08 | 2011-08-09 | Heraeus Shin-Etsu America, Inc. | Method for making a silica glass crucible |
| JP4702898B2 (ja) * | 2007-09-18 | 2011-06-15 | 信越石英株式会社 | シリコン単結晶引上げ用石英ガラスルツボの製造方法 |
| JP5273512B2 (ja) * | 2007-10-25 | 2013-08-28 | 株式会社Sumco | 石英ガラスルツボとその製造方法および用途 |
| JP4671999B2 (ja) * | 2007-11-30 | 2011-04-20 | ジャパンスーパークォーツ株式会社 | 石英ガラスルツボの試験方法 |
| JP4995069B2 (ja) * | 2007-12-28 | 2012-08-08 | ジャパンスーパークォーツ株式会社 | 内面結晶化ルツボおよび該ルツボを用いた引上げ方法 |
| EP2264226A4 (en) * | 2008-03-31 | 2011-07-27 | Japan Super Quartz Corp | QUARTZ GLASS LEVER AND MANUFACTURING METHOD THEREFOR |
| DE102008026890B3 (de) * | 2008-06-05 | 2009-06-04 | Heraeus Quarzglas Gmbh & Co. Kg | Verfahren und Vorrichtung zur Herstellung eines Tiegels aus Quarzglas |
| JP5523018B2 (ja) * | 2008-08-30 | 2014-06-18 | 株式会社Sumco | 石英ルツボの製造装置 |
| JP5142912B2 (ja) * | 2008-09-22 | 2013-02-13 | ジャパンスーパークォーツ株式会社 | アーク放電方法、アーク放電装置、石英ガラスルツボ製造装置 |
| JP5467418B2 (ja) * | 2010-12-01 | 2014-04-09 | 株式会社Sumco | 造粒シリカ粉の製造方法、シリカガラスルツボの製造方法 |
| US20140041575A1 (en) * | 2012-03-23 | 2014-02-13 | Shin-Etsu Quartz Products Co., Ltd. | Silica container for pulling single crystal silicon and method for producing the same |
| JP7163863B2 (ja) * | 2019-05-08 | 2022-11-01 | 株式会社Sumco | 石英ルツボ製造用モールド及びこれを用いた石英ルツボ製造装置 |
Family Cites Families (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE236084C (enExample) | ||||
| JPH0243720B2 (ja) * | 1982-09-10 | 1990-10-01 | Toshiba Ceramics Co | Handotaishoryosekieigarasuseiroshinkan |
| DD236084A1 (de) * | 1985-04-04 | 1986-05-28 | Technisches Glas Veb K | Verfahren zur herstellung von gelaeuterten rotationssymmetrischen kieselglashohlkoerpern |
| US5389582A (en) * | 1985-11-06 | 1995-02-14 | Loxley; Ted A. | Cristobalite reinforcement of quartz glass |
| US4632686A (en) * | 1986-02-24 | 1986-12-30 | Gte Products Corporation | Method of manufacturing quartz glass crucibles with low bubble content |
| US4935046A (en) * | 1987-12-03 | 1990-06-19 | Shin-Etsu Handotai Company, Limited | Manufacture of a quartz glass vessel for the growth of single crystal semiconductor |
| JPH01148718A (ja) * | 1987-12-03 | 1989-06-12 | Shin Etsu Handotai Co Ltd | 石英るつぼの製造方法 |
| JP2933404B2 (ja) * | 1990-06-25 | 1999-08-16 | 信越石英 株式会社 | シリコン単結晶引き上げ用石英ガラスルツボとその製造方法 |
| JP2747856B2 (ja) * | 1991-10-31 | 1998-05-06 | 信越石英株式会社 | シリコン単結晶引上げ用石英ガラスルツボ及びその製造方法 |
| US5306473A (en) * | 1992-01-31 | 1994-04-26 | Toshiba Ceramics Co., Ltd. | Quartz glass crucible for pulling a single crystal |
| JP2736863B2 (ja) * | 1994-05-31 | 1998-04-02 | 信越石英株式会社 | 石英ガラスルツボの製造方法 |
| JP2830990B2 (ja) * | 1995-05-31 | 1998-12-02 | 信越石英株式会社 | 石英製二重ルツボの製造方法 |
| JPH0920586A (ja) * | 1995-06-30 | 1997-01-21 | Toshiba Ceramics Co Ltd | シリコン単結晶引上げ用石英ガラスルツボの製造方法 |
| JP3533416B2 (ja) * | 1996-02-06 | 2004-05-31 | 三菱住友シリコン株式会社 | 単結晶引上装置 |
| JP4285788B2 (ja) * | 1996-03-14 | 2009-06-24 | 信越石英株式会社 | 単結晶引き上げ用大口径石英るつぼの製造方法 |
| JP3764776B2 (ja) * | 1996-03-18 | 2006-04-12 | 信越石英株式会社 | 単結晶引き上げ用石英ガラスるつぼ及びその製造方法 |
| JP3798849B2 (ja) * | 1996-07-09 | 2006-07-19 | 信越石英株式会社 | 石英ルツボの製造装置及び方法 |
-
1999
- 1999-01-29 JP JP02262899A patent/JP4398527B2/ja not_active Expired - Fee Related
- 1999-05-13 TW TW088107805A patent/TW509664B/zh not_active IP Right Cessation
- 1999-05-21 KR KR1019990018459A patent/KR100550440B1/ko not_active Expired - Lifetime
- 1999-05-24 EP EP99921237A patent/EP1020546A4/en not_active Withdrawn
- 1999-05-24 WO PCT/JP1999/002703 patent/WO1999061685A1/ja not_active Ceased
-
2001
- 2001-11-14 US US09/987,463 patent/US6797061B2/en not_active Expired - Lifetime
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR101406915B1 (ko) * | 2010-12-03 | 2014-06-12 | 쟈판 스파 쿼츠 가부시키가이샤 | 실리카 유리 도가니의 제조 방법 |
Also Published As
| Publication number | Publication date |
|---|---|
| JP4398527B2 (ja) | 2010-01-13 |
| JP2000044386A (ja) | 2000-02-15 |
| US6797061B2 (en) | 2004-09-28 |
| EP1020546A4 (en) | 2001-10-10 |
| EP1020546A1 (en) | 2000-07-19 |
| US20020029737A1 (en) | 2002-03-14 |
| TW509664B (en) | 2002-11-11 |
| KR19990088478A (ko) | 1999-12-27 |
| WO1999061685A1 (en) | 1999-12-02 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PA0109 | Patent application |
Patent event code: PA01091R01D Comment text: Patent Application Patent event date: 19990521 |
|
| PG1501 | Laying open of application | ||
| A201 | Request for examination | ||
| PA0201 | Request for examination |
Patent event code: PA02012R01D Patent event date: 20040205 Comment text: Request for Examination of Application Patent event code: PA02011R01I Patent event date: 19990521 Comment text: Patent Application |
|
| E902 | Notification of reason for refusal | ||
| PE0902 | Notice of grounds for rejection |
Comment text: Notification of reason for refusal Patent event date: 20050909 Patent event code: PE09021S01D |
|
| E701 | Decision to grant or registration of patent right | ||
| PE0701 | Decision of registration |
Patent event code: PE07011S01D Comment text: Decision to Grant Registration Patent event date: 20060113 |
|
| GRNT | Written decision to grant | ||
| PR0701 | Registration of establishment |
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