KR100492653B1 - 헤테로사이클릭카벤의제조방법 - Google Patents

헤테로사이클릭카벤의제조방법 Download PDF

Info

Publication number
KR100492653B1
KR100492653B1 KR10-1998-0707423A KR19980707423A KR100492653B1 KR 100492653 B1 KR100492653 B1 KR 100492653B1 KR 19980707423 A KR19980707423 A KR 19980707423A KR 100492653 B1 KR100492653 B1 KR 100492653B1
Authority
KR
South Korea
Prior art keywords
mmol
formula
nmr
mhz
ammonia
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
KR10-1998-0707423A
Other languages
English (en)
Korean (ko)
Other versions
KR20000064700A (ko
Inventor
볼프강 아. 헤르만
크리스티안 쾨허
루카스 고오쎈
Original Assignee
셀라네제 쉐미칼스 오이로페 게엠베하
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 셀라네제 쉐미칼스 오이로페 게엠베하 filed Critical 셀라네제 쉐미칼스 오이로페 게엠베하
Publication of KR20000064700A publication Critical patent/KR20000064700A/ko
Application granted granted Critical
Publication of KR100492653B1 publication Critical patent/KR100492653B1/ko
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D233/00—Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings
    • C07D233/04—Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings having one double bond between ring members or between a ring member and a non-ring member
    • C07D233/06—Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings having one double bond between ring members or between a ring member and a non-ring member with only hydrogen atoms or radicals containing only hydrogen and carbon atoms, directly attached to ring carbon atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D233/00—Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings
    • C07D233/04—Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings having one double bond between ring members or between a ring member and a non-ring member
    • C07D233/20—Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings having one double bond between ring members or between a ring member and a non-ring member with substituted hydrocarbon radicals, directly attached to ring carbon atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D249/00—Heterocyclic compounds containing five-membered rings having three nitrogen atoms as the only ring hetero atoms
    • C07D249/02—Heterocyclic compounds containing five-membered rings having three nitrogen atoms as the only ring hetero atoms not condensed with other rings
    • C07D249/08—1,2,4-Triazoles; Hydrogenated 1,2,4-triazoles
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D401/00—Heterocyclic compounds containing two or more hetero rings, having nitrogen atoms as the only ring hetero atoms, at least one ring being a six-membered ring with only one nitrogen atom
    • C07D401/14—Heterocyclic compounds containing two or more hetero rings, having nitrogen atoms as the only ring hetero atoms, at least one ring being a six-membered ring with only one nitrogen atom containing three or more hetero rings
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02—Phosphorus compounds
    • C07F9/547—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom
    • C07F9/645—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having two nitrogen atoms as the only ring hetero atoms
    • C07F9/6503—Five-membered rings
    • C07F9/6506—Five-membered rings having the nitrogen atoms in positions 1 and 3

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Molecular Biology (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Heterocyclic Carbon Compounds Containing A Hetero Ring Having Nitrogen And Oxygen As The Only Ring Hetero Atoms (AREA)
  • Plural Heterocyclic Compounds (AREA)
  • Catalysts (AREA)
KR10-1998-0707423A 1996-03-20 1997-03-14 헤테로사이클릭카벤의제조방법 Expired - Fee Related KR100492653B1 (ko)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
DE19610908A DE19610908A1 (de) 1996-03-20 1996-03-20 Verfahren zur Herstellung heterocyclischer Carbene
DE19610908.6 1996-03-20
PCT/EP1997/001296 WO1997034875A1 (de) 1996-03-20 1997-03-14 Verfahren zur herstellung heterocyclischer carbene

Publications (2)

Publication Number Publication Date
KR20000064700A KR20000064700A (ko) 2000-11-06
KR100492653B1 true KR100492653B1 (ko) 2005-11-11

Family

ID=7788826

Family Applications (1)

Application Number Title Priority Date Filing Date
KR10-1998-0707423A Expired - Fee Related KR100492653B1 (ko) 1996-03-20 1997-03-14 헤테로사이클릭카벤의제조방법

Country Status (14)

Country Link
US (1) US6025496A (cg-RX-API-DMAC10.html)
EP (1) EP0888308A1 (cg-RX-API-DMAC10.html)
JP (1) JP2000507239A (cg-RX-API-DMAC10.html)
KR (1) KR100492653B1 (cg-RX-API-DMAC10.html)
CN (1) CN1216536A (cg-RX-API-DMAC10.html)
AU (1) AU710591B2 (cg-RX-API-DMAC10.html)
BR (1) BR9708234A (cg-RX-API-DMAC10.html)
CA (1) CA2250086A1 (cg-RX-API-DMAC10.html)
DE (1) DE19610908A1 (cg-RX-API-DMAC10.html)
ID (1) ID16265A (cg-RX-API-DMAC10.html)
PL (1) PL329010A1 (cg-RX-API-DMAC10.html)
TW (1) TW412530B (cg-RX-API-DMAC10.html)
WO (1) WO1997034875A1 (cg-RX-API-DMAC10.html)
ZA (1) ZA972198B (cg-RX-API-DMAC10.html)

Families Citing this family (32)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE19815275B4 (de) * 1998-04-06 2009-06-25 Evonik Degussa Gmbh Alkylidenkomplexe des Rutheniums mit N-heterozyklischen Carbenliganden und deren Verwendung als hochaktive, selektive Katalysatoren für die Olefin-Metathese
US7285593B1 (en) 1998-05-19 2007-10-23 Advanced Polymer Technologies, Inc. Polyolefin compositions optionally having variable toughness and/or hardness
FR2778916B1 (fr) 1998-05-20 2000-06-30 Rhone Poulenc Fibres Nouveaux complexes organometalliques comprenant des carbenes heterocycliques cationiques et leur procede de preparation
GB9814282D0 (en) * 1998-07-01 1998-09-02 Borealis As Catalysts
WO2000015339A1 (en) 1998-09-10 2000-03-23 University Of New Orleans Foundation Catalyst complex with carbene ligand
US6316380B1 (en) * 1998-09-10 2001-11-13 University Of New Orleans Research & Technology Foundation Catalyst system comprising transition metal and imidazoline-2-ylidene or imidazolidine-2-ylidene
AU3997900A (en) 1999-02-05 2000-08-25 Materia, Inc. Metathesis-active adhesion agents and methods for enhancing polymer adhesion to surfaces
US20140088260A1 (en) 1999-02-05 2014-03-27 Materia, Inc. Metathesis-active adhesion agents and methods for enhancing polymer adhesion to surfaces
MXPA01007857A (es) 1999-02-05 2003-06-04 Materia Inc Composiciones de poliolefina que tienen densidad variable y metodos para su produccion y uso.
DE60039166D1 (de) * 1999-03-31 2008-07-24 California Inst Of Techn Mit triazolydin-liganden koordinierte rutheniummetall-alkyliden-komplexe die hohe olefin-metathese-aktivität aufweisen
US7329758B1 (en) * 1999-05-24 2008-02-12 California Institute Of Technology Imidazolidine-based metal carbene metathesis catalysts
DE10025623A1 (de) * 2000-05-24 2001-12-06 Bayer Ag Immobilisierte Palladiumkomplexe
WO2002038566A2 (en) * 2000-11-10 2002-05-16 The University Of Akron Carbene porphyrins and carbene porphyrinoids for use in medical diagnosis and treatment
GB0031078D0 (en) * 2000-12-20 2001-01-31 Borealis Tech Oy Compounds
CN1265881C (zh) * 2001-03-23 2006-07-26 加州理工学院 采用热活化n－杂环卡宾前体制备的高活性金属卡宾易位催化剂
US6838489B2 (en) * 2001-03-23 2005-01-04 Cymetech, Llc High activity metal carbene metathesis catalysts generated using a thermally activated N-heterocyclic carbene precursor
AU2003217232A1 (en) 2002-02-04 2003-09-02 Massachusetts Institute Of Technology Transition-metal-catalyzed carbon-nitrogen bond-forming methods using carbene ligands
WO2005016941A1 (de) * 2003-08-11 2005-02-24 Merck Patent Gmbh Immobilisierbare n-heterozyklische carbene
US20080267867A1 (en) * 2003-09-05 2008-10-30 Youngs Wiley J Metal Complexes of N-Heterocyclic Carbenes as Radiopharmaceuticals and Antibiotics
US8519146B2 (en) * 2004-09-07 2013-08-27 The University Of Akron Metal complexes of N-heterocyclic carbenes as antibiotics
JP4680518B2 (ja) * 2004-02-25 2011-05-11 株式会社きもと イミダゾールカルベン付加体の製造方法
JP4680519B2 (ja) * 2004-02-25 2011-05-11 株式会社きもと イミダゾールカルベン金属錯体の製造方法
DE102004060247A1 (de) * 2004-12-15 2006-06-29 Studiengesellschaft Kohle Mbh Neue N-heterocyclische Carbene und ihre Anwendung in der Katalyse
CA2688412A1 (en) * 2007-05-31 2008-12-11 The University Of Akron Metal complexes incorporated within biodegradable nanoparticles and their use
WO2009015112A2 (en) * 2007-07-23 2009-01-29 The University Of Akron Metal complexes incorporated within biodegradable nanoparticles and their use
EP2417061A4 (en) * 2009-04-09 2016-04-20 California Inst Of Techn MOLECULAR SIEVES AND CORRESPONDING METHODS AND STRUCTURAL ALIGNMENT EQUIPMENT
AP2011006003A0 (en) 2009-05-05 2011-12-31 Stepan Co Sulfonated internal olefin surfactant for enhancedoil recovery.
EP2261217A1 (en) * 2009-06-10 2010-12-15 Politecnico di Milano Imidazolium salts having liquid crystal characteristics, useful as electrolytes
US8227371B2 (en) 2010-09-24 2012-07-24 Exxonmobil Chemical Patents Inc. Class of olefin metathesis catalysts, methods of preparation, and processes for the use thereof
US9181360B2 (en) 2011-08-12 2015-11-10 Exxonmobil Chemical Patents Inc. Polymers prepared by ring opening / cross metathesis
JP7100312B2 (ja) * 2018-02-23 2022-07-13 東ソー株式会社 新規セリウム錯体、及び発光材
JP7212409B2 (ja) 2018-10-10 2023-01-25 コリア リサーチ インスティチュート オブ バイオサイエンス アンド バイオテクノロジー カルベン化合物、カルベン‐金属ナノ粒子複合体およびその製造方法

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE4230466A1 (de) * 1992-09-11 1994-03-17 Basf Ag Verfahren zur katalytischen Herstellung von Kondensationsprodukten des Formaldehyds
DE4447066A1 (de) * 1994-12-29 1996-07-04 Hoechst Ag Heterocyclische Carbene enthaltende Metallkomplexverbindungen

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
Angew. Chem. Int. Ed. Engl, 1995, 34(9), 1021-1023 *
JACS. 1992, 114, 5530-5534 *

Also Published As

Publication number Publication date
AU710591B2 (en) 1999-09-23
PL329010A1 (en) 1999-03-01
TW412530B (en) 2000-11-21
JP2000507239A (ja) 2000-06-13
AU2287897A (en) 1997-10-10
CA2250086A1 (en) 1997-09-25
ID16265A (id) 1997-09-18
WO1997034875A1 (de) 1997-09-25
EP0888308A1 (de) 1999-01-07
BR9708234A (pt) 1999-08-03
KR20000064700A (ko) 2000-11-06
DE19610908A1 (de) 1997-09-25
US6025496A (en) 2000-02-15
CN1216536A (zh) 1999-05-12
ZA972198B (en) 1997-09-17

Similar Documents

Publication Publication Date Title
KR100492653B1 (ko) 헤테로사이클릭카벤의제조방법
Herrmann et al. Heterocyclic carbenes: A high‐yielding synthesis of novel, functionalized N‐heterocyclic carbenes in liquid ammonia
Zhdankin et al. Alkynyliodonium salts in organic synthesis
Köcher et al. Heterocyclic carbenes. One-pot synthesis of rhodium and iridium carbene complexes
KR100377674B1 (ko) 헤테로사이클릭카르벤을갖는금속착화합물
JP5199887B2 (ja) 遷移金属カルベン錯体の製造方法
Toth et al. CO Insertion in Four-Coordinate cis-Methyl (carbonyl) platinum-Diphosphine Compounds. An Ionic Mechanism for Platinum-Diphosphine-Catalyzed Hydroformylation
US9994595B2 (en) Catalyst and battery components derived from condensation reactions with carba-closo-dodecaborate amines
Krüger Monosodium acetonitriles, their preparation, properties and reactions
Böhler et al. Synthesis of a transient tropylidene substituted N-heterocyclic carbene (tropNHC): rearrangement and formation of its gold complex
Wacker et al. Borane‐Substituted Imidazol‐2‐ylidenes: Syntheses, Structures, and Reactivity☆
Michelin et al. Transition metal-promoted cyclization reactions of nitrile ligands in complexes of platinum (II): synthesis of 2-oxazoline derivatives and x-ray structure of cis-Cl2Pt [cyclic N= C (Ph) OCH2] 2
Siewert et al. Terphenyl (bisamino) phosphines: electron-rich ligands for gold-catalysis
Rieger et al. A novel reaction of the cyano ligand opening an organometallic route to 4-amino imidazoles: four component condensation (4CC) with isocyanide, aldehyde and amine
US5663451A (en) Process for preparing aldehydes
CN110669062A (zh) α-芳基或烷基取代的甲硼烷加合物和制备方法及其应用
SMITH et al. Nitrogen Compounds of the Phosphoric and Phosphonic Acids. III. Preparation and Properties of Amides of Phenylphosphonic and Phenylphosphonothioic Acids1
Bolm et al. Synthesis, Reactions, and Molecular Structures of Ethylzinc Enolates of Chiral N‐Substituted β‐Carbonyl Sulfoximines
Shevchenko et al. Synthesis of Bulky 4-Amino-1, 3-diarylimidazolium Salts as NHC-Ligand Precursors and Derived M/NHC Complexes (M= Cu, Pd)
Hahn et al. Pd (II) complexes of N-allyl substituted N-heterocyclic carbenes
Alcalde et al. Coordination features of bis (N-heterocyclic carbenes) and bis (oxazolines) with 1, 3-alkylidene-2, 4, 6-trimethylbenzene spacers. Synthesis of the ligands and silver and palladium complexes
Dıez-Barra et al. 1, 2, 4-Triazole-Based Palladium Pincer Complexes. A New Type of Catalyst for the Heck Reaction
KR100965841B1 (ko) 구리촉매와 염기화합물 존재하에서 삼성분 짝지움 반응에의해 헤테로고리 화합물을 제조하는 방법 및 동 방법에의해 제조한 헤테로고리 화합물
US20140051870A1 (en) Cyclopropenylidene-stabilized phosphenium cations
Quezada-Miriel et al. Metalation behavior of a bis-saturated NHC ligand with a flexible m-xylyl linker

Legal Events

Date Code Title Description
PA0105 International application

St.27 status event code: A-0-1-A10-A15-nap-PA0105

R17-X000 Change to representative recorded

St.27 status event code: A-3-3-R10-R17-oth-X000

R17-X000 Change to representative recorded

St.27 status event code: A-3-3-R10-R17-oth-X000

PN2301 Change of applicant

St.27 status event code: A-3-3-R10-R13-asn-PN2301

St.27 status event code: A-3-3-R10-R11-asn-PN2301

PN2301 Change of applicant

St.27 status event code: A-3-3-R10-R13-asn-PN2301

St.27 status event code: A-3-3-R10-R11-asn-PN2301

PG1501 Laying open of application

St.27 status event code: A-1-1-Q10-Q12-nap-PG1501

A201 Request for examination
P11-X000 Amendment of application requested

St.27 status event code: A-2-2-P10-P11-nap-X000

P13-X000 Application amended

St.27 status event code: A-2-2-P10-P13-nap-X000

PA0201 Request for examination

St.27 status event code: A-1-2-D10-D11-exm-PA0201

R18-X000 Changes to party contact information recorded

St.27 status event code: A-3-3-R10-R18-oth-X000

E902 Notification of reason for refusal
PE0902 Notice of grounds for rejection

St.27 status event code: A-1-2-D10-D21-exm-PE0902

T11-X000 Administrative time limit extension requested

St.27 status event code: U-3-3-T10-T11-oth-X000

T11-X000 Administrative time limit extension requested

St.27 status event code: U-3-3-T10-T11-oth-X000

R17-X000 Change to representative recorded

St.27 status event code: A-3-3-R10-R17-oth-X000

T11-X000 Administrative time limit extension requested

St.27 status event code: U-3-3-T10-T11-oth-X000

T11-X000 Administrative time limit extension requested

St.27 status event code: U-3-3-T10-T11-oth-X000

P11-X000 Amendment of application requested

St.27 status event code: A-2-2-P10-P11-nap-X000

P13-X000 Application amended

St.27 status event code: A-2-2-P10-P13-nap-X000

P11-X000 Amendment of application requested

St.27 status event code: A-2-2-P10-P11-nap-X000

P13-X000 Application amended

St.27 status event code: A-2-2-P10-P13-nap-X000

E701 Decision to grant or registration of patent right
PE0701 Decision of registration

St.27 status event code: A-1-2-D10-D22-exm-PE0701

GRNT Written decision to grant
PR0701 Registration of establishment

St.27 status event code: A-2-4-F10-F11-exm-PR0701

PR1002 Payment of registration fee

St.27 status event code: A-2-2-U10-U12-oth-PR1002

Fee payment year number: 1

PG1601 Publication of registration

St.27 status event code: A-4-4-Q10-Q13-nap-PG1601

PN2301 Change of applicant

St.27 status event code: A-5-5-R10-R11-asn-PN2301

PN2301 Change of applicant

St.27 status event code: A-5-5-R10-R14-asn-PN2301

LAPS Lapse due to unpaid annual fee
PC1903 Unpaid annual fee

St.27 status event code: A-4-4-U10-U13-oth-PC1903

Not in force date: 20080525

Payment event data comment text: Termination Category : DEFAULT_OF_REGISTRATION_FEE

PC1903 Unpaid annual fee

St.27 status event code: N-4-6-H10-H13-oth-PC1903

Ip right cessation event data comment text: Termination Category : DEFAULT_OF_REGISTRATION_FEE

Not in force date: 20080525

P22-X000 Classification modified

St.27 status event code: A-4-4-P10-P22-nap-X000

P22-X000 Classification modified

St.27 status event code: A-4-4-P10-P22-nap-X000