JPS6357383B2 - - Google Patents
Info
- Publication number
- JPS6357383B2 JPS6357383B2 JP59017418A JP1741884A JPS6357383B2 JP S6357383 B2 JPS6357383 B2 JP S6357383B2 JP 59017418 A JP59017418 A JP 59017418A JP 1741884 A JP1741884 A JP 1741884A JP S6357383 B2 JPS6357383 B2 JP S6357383B2
- Authority
- JP
- Japan
- Prior art keywords
- manufacturing
- silicon
- aluminum
- water
- alcohol
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- KZHJGOXRZJKJNY-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Si]=O.O=[Al]O[Al]=O.O=[Al]O[Al]=O.O=[Al]O[Al]=O KZHJGOXRZJKJNY-UHFFFAOYSA-N 0.000 claims description 25
- 229910052863 mullite Inorganic materials 0.000 claims description 25
- 239000000843 powder Substances 0.000 claims description 17
- 238000004519 manufacturing process Methods 0.000 claims description 15
- 239000000203 mixture Substances 0.000 claims description 13
- 238000005245 sintering Methods 0.000 claims description 8
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 7
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 7
- VSCWAEJMTAWNJL-UHFFFAOYSA-K aluminium trichloride Chemical compound Cl[Al](Cl)Cl VSCWAEJMTAWNJL-UHFFFAOYSA-K 0.000 claims description 6
- 239000000919 ceramic Substances 0.000 claims description 6
- 238000005118 spray pyrolysis Methods 0.000 claims description 6
- BOTDANWDWHJENH-UHFFFAOYSA-N Tetraethyl orthosilicate Chemical compound CCO[Si](OCC)(OCC)OCC BOTDANWDWHJENH-UHFFFAOYSA-N 0.000 claims description 5
- AZDRQVAHHNSJOQ-UHFFFAOYSA-N alumane Chemical class [AlH3] AZDRQVAHHNSJOQ-UHFFFAOYSA-N 0.000 claims description 5
- BNGXYYYYKUGPPF-UHFFFAOYSA-M (3-methylphenyl)methyl-triphenylphosphanium;chloride Chemical compound [Cl-].CC1=CC=CC(C[P+](C=2C=CC=CC=2)(C=2C=CC=CC=2)C=2C=CC=CC=2)=C1 BNGXYYYYKUGPPF-UHFFFAOYSA-M 0.000 claims description 4
- 238000001354 calcination Methods 0.000 claims description 4
- CRNJBCMSTRNIOX-UHFFFAOYSA-N methanolate silicon(4+) Chemical compound [Si+4].[O-]C.[O-]C.[O-]C.[O-]C CRNJBCMSTRNIOX-UHFFFAOYSA-N 0.000 claims description 4
- 239000003021 water soluble solvent Substances 0.000 claims description 4
- IDJROVMRGKXECW-UHFFFAOYSA-N [Si+4].CCC[O-].CCC[O-].CCC[O-].CCC[O-] Chemical compound [Si+4].CCC[O-].CCC[O-].CCC[O-].CCC[O-] IDJROVMRGKXECW-UHFFFAOYSA-N 0.000 claims description 2
- 239000002904 solvent Substances 0.000 claims description 2
- UQMOLLPKNHFRAC-UHFFFAOYSA-N tetrabutyl silicate Chemical compound CCCCO[Si](OCCCC)(OCCCC)OCCCC UQMOLLPKNHFRAC-UHFFFAOYSA-N 0.000 claims description 2
- 229910052710 silicon Inorganic materials 0.000 claims 3
- 239000010703 silicon Substances 0.000 claims 3
- -1 silicon alkoxide Chemical class 0.000 claims 3
- HDYRYUINDGQKMC-UHFFFAOYSA-M acetyloxyaluminum;dihydrate Chemical compound O.O.CC(=O)O[Al] HDYRYUINDGQKMC-UHFFFAOYSA-M 0.000 claims 1
- 125000000217 alkyl group Chemical group 0.000 claims 1
- DIZPMCHEQGEION-UHFFFAOYSA-H aluminium sulfate (anhydrous) Chemical compound [Al+3].[Al+3].[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O DIZPMCHEQGEION-UHFFFAOYSA-H 0.000 claims 1
- 229940009827 aluminum acetate Drugs 0.000 claims 1
- 238000001272 pressureless sintering Methods 0.000 claims 1
- 238000000197 pyrolysis Methods 0.000 claims 1
- 238000000034 method Methods 0.000 description 10
- 239000002245 particle Substances 0.000 description 9
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 5
- 239000012535 impurity Substances 0.000 description 4
- 239000002994 raw material Substances 0.000 description 4
- 150000004703 alkoxides Chemical class 0.000 description 3
- 239000007791 liquid phase Substances 0.000 description 3
- 238000002156 mixing Methods 0.000 description 3
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 2
- 239000004927 clay Substances 0.000 description 2
- 238000000975 co-precipitation Methods 0.000 description 2
- 238000011109 contamination Methods 0.000 description 2
- 238000000354 decomposition reaction Methods 0.000 description 2
- 229910003460 diamond Inorganic materials 0.000 description 2
- 239000010432 diamond Substances 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 239000011224 oxide ceramic Substances 0.000 description 2
- 229910052574 oxide ceramic Inorganic materials 0.000 description 2
- 238000011160 research Methods 0.000 description 2
- 238000003980 solgel method Methods 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- 238000002076 thermal analysis method Methods 0.000 description 2
- 229910018072 Al 2 O 3 Inorganic materials 0.000 description 1
- 239000004115 Sodium Silicate Substances 0.000 description 1
- 230000002159 abnormal effect Effects 0.000 description 1
- 150000001242 acetic acid derivatives Chemical class 0.000 description 1
- 238000005452 bending Methods 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 150000001805 chlorine compounds Chemical class 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 238000010304 firing Methods 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- 238000007731 hot pressing Methods 0.000 description 1
- 230000003301 hydrolyzing effect Effects 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 238000000465 moulding Methods 0.000 description 1
- 150000002823 nitrates Chemical class 0.000 description 1
- 238000010298 pulverizing process Methods 0.000 description 1
- 238000012827 research and development Methods 0.000 description 1
- 239000012047 saturated solution Substances 0.000 description 1
- RMAQACBXLXPBSY-UHFFFAOYSA-N silicic acid Chemical compound O[Si](O)(O)O RMAQACBXLXPBSY-UHFFFAOYSA-N 0.000 description 1
- 239000000377 silicon dioxide Substances 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 description 1
- 229910052911 sodium silicate Inorganic materials 0.000 description 1
- RPACBEVZENYWOL-XFULWGLBSA-M sodium;(2r)-2-[6-(4-chlorophenoxy)hexyl]oxirane-2-carboxylate Chemical compound [Na+].C=1C=C(Cl)C=CC=1OCCCCCC[C@]1(C(=O)[O-])CO1 RPACBEVZENYWOL-XFULWGLBSA-M 0.000 description 1
- 239000006104 solid solution Substances 0.000 description 1
- 238000001179 sorption measurement Methods 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 150000003467 sulfuric acid derivatives Chemical class 0.000 description 1
- 230000002194 synthesizing effect Effects 0.000 description 1
Landscapes
- Compositions Of Oxide Ceramics (AREA)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP59017418A JPS60161371A (ja) | 1984-02-01 | 1984-02-01 | 高強度セラミツクス焼結体の製造法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP59017418A JPS60161371A (ja) | 1984-02-01 | 1984-02-01 | 高強度セラミツクス焼結体の製造法 |
Publications (2)
Publication Number | Publication Date |
---|---|
JPS60161371A JPS60161371A (ja) | 1985-08-23 |
JPS6357383B2 true JPS6357383B2 (ko) | 1988-11-11 |
Family
ID=11943457
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP59017418A Granted JPS60161371A (ja) | 1984-02-01 | 1984-02-01 | 高強度セラミツクス焼結体の製造法 |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS60161371A (ko) |
Families Citing this family (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH0611667B2 (ja) * | 1985-05-30 | 1994-02-16 | 工業技術院長 | 高温強度が優れたアルミナ・シリカ系セラミックス焼結体の製造方法 |
JPS62108765A (ja) * | 1985-11-08 | 1987-05-20 | 株式会社神戸製鋼所 | 強靭セラミツク材料の製造方法 |
JPS6389455A (ja) * | 1986-10-01 | 1988-04-20 | 東レ株式会社 | ムライト焼結体 |
JPS63159254A (ja) * | 1986-12-23 | 1988-07-02 | 株式会社ニッカト− | ムライト質電気絶縁材料の製造法 |
WO1992009543A1 (en) * | 1990-12-03 | 1992-06-11 | Manville Corporation | Method of preparing ceramic hollow particles |
WO2015186560A1 (ja) | 2014-06-06 | 2015-12-10 | 日本碍子株式会社 | ムライト焼結体、その製法及び複合基板 |
-
1984
- 1984-02-01 JP JP59017418A patent/JPS60161371A/ja active Granted
Also Published As
Publication number | Publication date |
---|---|
JPS60161371A (ja) | 1985-08-23 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
JPS6052083B2 (ja) | 高純度セラミツク粉末の製造法 | |
JPS62167209A (ja) | α−サイアロン質粉末及びその製造法 | |
JPS6357383B2 (ko) | ||
US5320792A (en) | Process for the preparation of LAS ceramic sintered bodies | |
JPH0640763A (ja) | 高度結晶質品の製造方法 | |
JPH0339967B2 (ko) | ||
US4774068A (en) | Method for production of mullite of high purity | |
CA1241523A (en) | Process for the preparation of lithium silicate | |
JPS6272556A (ja) | 緻密な多結晶MgAl↓2O↓4スピネルの製造方法 | |
JP2000159570A (ja) | 緻密なコーディエライト焼結体の製造方法 | |
JPS61281013A (ja) | 高純度ムライト質粉末の製造方法 | |
JPH03215348A (ja) | ジルコン焼結体及びその製造方法 | |
JPH0615421B2 (ja) | ムライト焼結体の製造方法 | |
JPS60141671A (ja) | ジルコニア焼結体の製造方法 | |
JP3496795B2 (ja) | 窒化珪素質粉末の製造方法 | |
JPS62202813A (ja) | ジルコニア均一分散ムライト質微粉末の製造方法 | |
JPS5926966A (ja) | セラミツクスグリ−ン成形体の製造方法 | |
JPS60145902A (ja) | サイアロン質粉末の製造法 | |
JPS62230667A (ja) | 固体電解質磁器の製造法 | |
JPS61236649A (ja) | セラミツクス粉末とその製造方法 | |
David et al. | Synthesis and characterization of cordierite from acetylacetonate/alkoxide precursors | |
JPS62265166A (ja) | 高温強度が優れたアルミナ・シリカ系セラミックス焼結体の製造方法 | |
JPS6272554A (ja) | 緻密な多結晶Al↓2O↓3焼結体の製造方法 | |
JPH0574525B2 (ko) | ||
JPH02102169A (ja) | ムライト組成物 |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
EXPY | Cancellation because of completion of term |