JPS6249276B2 - - Google Patents

Info

Publication number

JPS6249276B2

JPS6249276B2 JP27074184A JP27074184A JPS6249276B2 JP S6249276 B2 JPS6249276 B2 JP S6249276B2 JP 27074184 A JP27074184 A JP 27074184A JP 27074184 A JP27074184 A JP 27074184A JP S6249276 B2 JPS6249276 B2 JP S6249276B2

Authority

JP

Japan

Prior art keywords

compound

formula

group

germanium

compounds

Prior art date

1984-12-24

Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)

Expired

Links

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• 150000002291 germanium compounds Chemical class 0.000 claims description 9
• GSEJCLTVZPLZKY-UHFFFAOYSA-N Triethanolamine Chemical compound OCCN(CCO)CCO GSEJCLTVZPLZKY-UHFFFAOYSA-N 0.000 claims description 8
• 125000000217 alkyl group Chemical group 0.000 claims description 7
• 238000004519 manufacturing process Methods 0.000 claims description 4
• 125000003277 amino group Chemical group 0.000 claims description 3
• 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 claims description 3
• 125000004435 hydrogen atom Chemical group [H]* 0.000 claims description 3
• 125000002887 hydroxy group Chemical group [H]O* 0.000 claims description 3
• 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 claims description 3
• 125000004430 oxygen atom Chemical group O* 0.000 claims description 3
• 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 claims description 3
• 229910052717 sulfur Inorganic materials 0.000 claims description 2
• 125000004434 sulfur atom Chemical group 0.000 claims description 2
• 150000001875 compounds Chemical class 0.000 description 31
• UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 12
• 238000006243 chemical reaction Methods 0.000 description 9
• 229910052732 germanium Inorganic materials 0.000 description 8
• GNPVGFCGXDBREM-UHFFFAOYSA-N germanium atom Chemical compound [Ge] GNPVGFCGXDBREM-UHFFFAOYSA-N 0.000 description 8
• 229940093626 germanium sesquioxide Drugs 0.000 description 7
• 230000015572 biosynthetic process Effects 0.000 description 6
• 238000003786 synthesis reaction Methods 0.000 description 6
• 238000010992 reflux Methods 0.000 description 4
• 150000004703 alkoxides Chemical class 0.000 description 3
• QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical group [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 3
• 239000013078 crystal Substances 0.000 description 3
• 230000000694 effects Effects 0.000 description 3
• 238000000921 elemental analysis Methods 0.000 description 3
• 238000002844 melting Methods 0.000 description 3
• 230000008018 melting Effects 0.000 description 3
• 239000002904 solvent Substances 0.000 description 3
• 239000007858 starting material Substances 0.000 description 3
• ZJUHNMADISSFJZ-UHFFFAOYSA-N 2-trichlorogermylpropanoic acid Chemical class OC(=O)C(C)[Ge](Cl)(Cl)Cl ZJUHNMADISSFJZ-UHFFFAOYSA-N 0.000 description 2
• 125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 description 2
• -1 compound carboxyethyl germanium sesquioxide Chemical class 0.000 description 2
• GCFHZZWXZLABBL-UHFFFAOYSA-N ethanol;hexane Chemical compound CCO.CCCCCC GCFHZZWXZLABBL-UHFFFAOYSA-N 0.000 description 2
• 238000006460 hydrolysis reaction Methods 0.000 description 2
• 238000000034 method Methods 0.000 description 2
• 239000000203 mixture Substances 0.000 description 2
• 150000002894 organic compounds Chemical class 0.000 description 2
• 125000001424 substituent group Chemical group 0.000 description 2
• XRYJTKGEJGVBCC-UHFFFAOYSA-N 2-germylpropanoic acid Chemical class CC([GeH3])C(O)=O XRYJTKGEJGVBCC-UHFFFAOYSA-N 0.000 description 1
• HYHBWUIUJBNLNW-UHFFFAOYSA-N 3-germyl-3-phenylpropanoic acid Chemical compound OC(=O)CC([GeH3])C1=CC=CC=C1 HYHBWUIUJBNLNW-UHFFFAOYSA-N 0.000 description 1
• RWSOTUBLDIXVET-UHFFFAOYSA-N Dihydrogen sulfide Chemical compound S RWSOTUBLDIXVET-UHFFFAOYSA-N 0.000 description 1
• LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
• 230000000259 anti-tumor effect Effects 0.000 description 1
• VEFXTGTZJOWDOF-UHFFFAOYSA-N benzene;hydrate Chemical compound O.C1=CC=CC=C1 VEFXTGTZJOWDOF-UHFFFAOYSA-N 0.000 description 1
• 230000004531 blood pressure lowering effect Effects 0.000 description 1
• 150000001735 carboxylic acids Chemical class 0.000 description 1
• 239000003153 chemical reaction reagent Substances 0.000 description 1
• 238000007796 conventional method Methods 0.000 description 1
• MDKXBBPLEGPIRI-UHFFFAOYSA-N ethoxyethane;methanol Chemical compound OC.CCOCC MDKXBBPLEGPIRI-UHFFFAOYSA-N 0.000 description 1
• 238000001914 filtration Methods 0.000 description 1
• 229910000037 hydrogen sulfide Inorganic materials 0.000 description 1
• 239000002184 metal Substances 0.000 description 1
• 125000000082 organogermanium group Chemical group 0.000 description 1
• 125000001436 propyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
• 239000004065 semiconductor Substances 0.000 description 1
• 231100000331 toxic Toxicity 0.000 description 1
• 230000002588 toxic effect Effects 0.000 description 1
• MUDDKLJPADVVKF-UHFFFAOYSA-N trichlorogermane Chemical compound Cl[GeH](Cl)Cl MUDDKLJPADVVKF-UHFFFAOYSA-N 0.000 description 1