JPS6135790A - ポリ‐β‐ヒドロキシブチレートの抽出方法 - Google Patents
ポリ‐β‐ヒドロキシブチレートの抽出方法Info
- Publication number
- JPS6135790A JPS6135790A JP14814085A JP14814085A JPS6135790A JP S6135790 A JPS6135790 A JP S6135790A JP 14814085 A JP14814085 A JP 14814085A JP 14814085 A JP14814085 A JP 14814085A JP S6135790 A JPS6135790 A JP S6135790A
- Authority
- JP
- Japan
- Prior art keywords
- solvent
- poly
- water
- hydroxybutyrate
- extraction
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 238000000605 extraction Methods 0.000 title claims description 23
- 239000002904 solvent Substances 0.000 claims description 42
- 238000000034 method Methods 0.000 claims description 30
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 24
- 229920001397 Poly-beta-hydroxybutyrate Polymers 0.000 claims description 23
- 229920000331 Polyhydroxybutyrate Polymers 0.000 claims description 23
- 244000005700 microbiome Species 0.000 claims description 22
- 238000009835 boiling Methods 0.000 claims description 12
- 239000007900 aqueous suspension Substances 0.000 claims description 8
- WSLDOOZREJYCGB-UHFFFAOYSA-N 1,2-Dichloroethane Chemical compound ClCCCl WSLDOOZREJYCGB-UHFFFAOYSA-N 0.000 claims description 6
- 125000001931 aliphatic group Chemical group 0.000 claims description 4
- SJZRECIVHVDYJC-UHFFFAOYSA-M 4-hydroxybutyrate Chemical compound OCCCC([O-])=O SJZRECIVHVDYJC-UHFFFAOYSA-M 0.000 claims description 3
- 229920006395 saturated elastomer Polymers 0.000 claims description 3
- HRYZWHHZPQKTII-UHFFFAOYSA-N chloroethane Chemical compound CCCl HRYZWHHZPQKTII-UHFFFAOYSA-N 0.000 claims description 2
- 229960003750 ethyl chloride Drugs 0.000 claims description 2
- SNMVRZFUUCLYTO-UHFFFAOYSA-N n-propyl chloride Chemical compound CCCCl SNMVRZFUUCLYTO-UHFFFAOYSA-N 0.000 claims description 2
- 238000010533 azeotropic distillation Methods 0.000 claims 2
- NEHMKBQYUWJMIP-UHFFFAOYSA-N anhydrous methyl chloride Natural products ClC NEHMKBQYUWJMIP-UHFFFAOYSA-N 0.000 claims 1
- NEHMKBQYUWJMIP-OUBTZVSYSA-N chloromethane Chemical group Cl[13CH3] NEHMKBQYUWJMIP-OUBTZVSYSA-N 0.000 claims 1
- 239000007788 liquid Substances 0.000 claims 1
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 6
- 230000001580 bacterial effect Effects 0.000 description 6
- 210000004027 cell Anatomy 0.000 description 6
- 239000002609 medium Substances 0.000 description 5
- 238000010438 heat treatment Methods 0.000 description 4
- 239000000725 suspension Substances 0.000 description 4
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
- 238000001816 cooling Methods 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- 229920000642 polymer Polymers 0.000 description 3
- WHBMMWSBFZVSSR-UHFFFAOYSA-N 3-hydroxybutyric acid Chemical compound CC(O)CC(O)=O WHBMMWSBFZVSSR-UHFFFAOYSA-N 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- -1 aliphatic alcohols Chemical class 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 description 2
- 239000003960 organic solvent Substances 0.000 description 2
- 230000001376 precipitating effect Effects 0.000 description 2
- 238000011084 recovery Methods 0.000 description 2
- 238000000926 separation method Methods 0.000 description 2
- ZOAHZKDNMRNHFC-UHFFFAOYSA-N 1,2-dichloroethane;ethane Chemical compound CC.ClCCCl ZOAHZKDNMRNHFC-UHFFFAOYSA-N 0.000 description 1
- HIXDQWDOVZUNNA-UHFFFAOYSA-N 2-(3,4-dimethoxyphenyl)-5-hydroxy-7-methoxychromen-4-one Chemical compound C=1C(OC)=CC(O)=C(C(C=2)=O)C=1OC=2C1=CC=C(OC)C(OC)=C1 HIXDQWDOVZUNNA-UHFFFAOYSA-N 0.000 description 1
- 239000002028 Biomass Substances 0.000 description 1
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- 241000252867 Cupriavidus metallidurans Species 0.000 description 1
- 101000993982 Nicotiana tabacum Proteinase inhibitor I-B Proteins 0.000 description 1
- 150000001338 aliphatic hydrocarbons Chemical class 0.000 description 1
- 150000001491 aromatic compounds Chemical class 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 210000000170 cell membrane Anatomy 0.000 description 1
- 230000001413 cellular effect Effects 0.000 description 1
- 238000003776 cleavage reaction Methods 0.000 description 1
- 238000010924 continuous production Methods 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 230000018044 dehydration Effects 0.000 description 1
- 238000006297 dehydration reaction Methods 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 238000010981 drying operation Methods 0.000 description 1
- 238000005265 energy consumption Methods 0.000 description 1
- RTZKZFJDLAIYFH-UHFFFAOYSA-N ether Substances CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 230000001747 exhibiting effect Effects 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 239000001963 growth medium Substances 0.000 description 1
- 238000009434 installation Methods 0.000 description 1
- 150000002576 ketones Chemical class 0.000 description 1
- 150000002632 lipids Chemical class 0.000 description 1
- 239000007791 liquid phase Substances 0.000 description 1
- 230000002934 lysing effect Effects 0.000 description 1
- 238000000465 moulding Methods 0.000 description 1
- 239000003208 petroleum Substances 0.000 description 1
- 239000012071 phase Substances 0.000 description 1
- 238000011403 purification operation Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 230000007017 scission Effects 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 230000002194 synthesizing effect Effects 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
- C12P7/00—Preparation of oxygen-containing organic compounds
- C12P7/62—Carboxylic acid esters
- C12P7/625—Polyesters of hydroxy carboxylic acids
Landscapes
- Organic Chemistry (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Zoology (AREA)
- Life Sciences & Earth Sciences (AREA)
- Wood Science & Technology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Microbiology (AREA)
- General Chemical & Material Sciences (AREA)
- Biotechnology (AREA)
- Health & Medical Sciences (AREA)
- Biochemistry (AREA)
- Bioinformatics & Cheminformatics (AREA)
- General Engineering & Computer Science (AREA)
- General Health & Medical Sciences (AREA)
- Genetics & Genomics (AREA)
- Preparation Of Compounds By Using Micro-Organisms (AREA)
- Extraction Or Liquid Replacement (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR8410921A FR2567149B1 (fr) | 1984-07-06 | 1984-07-06 | Procede pour l'extraction de poly-beta-hydroxybutyrates au moyen d'un solvant a partir d'une suspension aqueuse de micro-organismes |
| FR8410921 | 1984-07-06 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS6135790A true JPS6135790A (ja) | 1986-02-20 |
| JPH0581239B2 JPH0581239B2 (enExample) | 1993-11-11 |
Family
ID=9305955
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP14814085A Granted JPS6135790A (ja) | 1984-07-06 | 1985-07-05 | ポリ‐β‐ヒドロキシブチレートの抽出方法 |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US4705604A (enExample) |
| EP (1) | EP0168095B1 (enExample) |
| JP (1) | JPS6135790A (enExample) |
| AT (1) | ATE32102T1 (enExample) |
| DE (1) | DE3561472D1 (enExample) |
| FR (1) | FR2567149B1 (enExample) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2006035889A1 (ja) * | 2004-09-30 | 2006-04-06 | Kaneka Corporation | ポリヒドロキシアルカノエートの製造方法 |
Families Citing this family (86)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| AT390068B (de) * | 1988-07-07 | 1990-03-12 | Danubia Petrochemie | Extraktionsmittel fuer poly-d(-)-3-hydroxybuttersaeure |
| US5147791A (en) * | 1989-04-06 | 1992-09-15 | University Of New Mexico | Enzyme catalyzed synthesis of polyesters |
| US5334520A (en) * | 1990-05-25 | 1994-08-02 | Center For Innovative Technology | Production of poly-beta-hydroxybutyrate in transformed escherichia coli |
| US5518907A (en) * | 1989-06-07 | 1996-05-21 | Center For Innovative Technology | Cloning and expression in Escherichia coli of the Alcaligenes eutrophus H16 poly-beta-hydroxybutyrate biosynthetic pathway |
| AT395319B (de) * | 1990-10-05 | 1992-11-25 | Danubia Petrochem Polymere | Verfahren zur gewinnung eines polyhydroxyalkanoates aus dem zellmaterial eines mikroorganismus und polyhydroxyalkanoatflocken |
| US5229158A (en) * | 1990-11-21 | 1993-07-20 | Manssur Yalpani | Polyhydroxyalkanoate cream substitutes |
| US5225227A (en) * | 1990-11-21 | 1993-07-06 | Manssur Yalpani | Polyhydroxyalkanoate flavor delivery system |
| US5256393A (en) * | 1991-04-16 | 1993-10-26 | Mallinckrodt Medical, Inc. | Use of azeotropic distillation in process to dry 5-amino-N,N'bis (2,3-dihydroxypropyl)-2,4,6-triiodoisphthalamide |
| RU2199587C2 (ru) * | 1995-08-21 | 2003-02-27 | Дзе Проктер Энд Гэмбл Компани | Способ выделения полигидроксиалканоата из биомассы и полигидроксиалканоат, полученный данным способом |
| US5942597A (en) * | 1995-08-21 | 1999-08-24 | The Procter & Gamble Company | Solvent extraction of polyhydroxyalkanoates from biomass |
| US5821299A (en) * | 1996-02-16 | 1998-10-13 | The Proctor & Gamble Company | Solvent extraction of polyhydroxy-alkanoates from biomass facilitated by the use of marginal nonsolvent |
| AU6974398A (en) * | 1997-04-15 | 1998-11-11 | Monsanto Company | High temperature pha extraction using pha-poor solvents |
| US6043063A (en) * | 1997-04-15 | 2000-03-28 | Monsanto Company | Methods of PHA extraction and recovery using non-halogenated solvents |
| AU757682B2 (en) | 1998-04-08 | 2003-02-27 | Metabolix, Inc. | Methods for separation and purification of biopolymers |
| US6340580B1 (en) * | 1999-05-12 | 2002-01-22 | Metabolix, Inc. | Methods for purifying polyhydroxy alkanoates |
| AU2004293501B2 (en) * | 2003-11-28 | 2009-10-29 | Phb Industrial S.A. | Process for recovering polyhydroxialkanoates ("PHAs") from cellular biomass |
| EP1781798B1 (en) * | 2004-08-06 | 2010-06-02 | PHB Industrial S.A. | Use of fatty alcohols as plasticizer to improve the physical-mechanical properties and processability of phb and its co-polymers |
| US20060105440A1 (en) * | 2004-09-30 | 2006-05-18 | Koichi Kinoshita | Method of producing polyhydroxyalkanoate |
| BRPI0501844B1 (pt) * | 2005-03-04 | 2019-12-24 | Phb Ind S/A | processo para extração e recuperação de polihidroxialcanoatos (phas) a partir de uma biomassa celular bacteriana |
| US7514525B2 (en) * | 2007-03-09 | 2009-04-07 | University Of Hawaii | Recovery and purification of polyhydroxyalkanoates |
| CN102634063A (zh) * | 2011-02-10 | 2012-08-15 | 元智大学 | 降解聚羟基烷酸类高分子的方法 |
| ES2448823B1 (es) | 2012-08-14 | 2014-10-13 | Neol Biosolutions, S.A. | Producción de bioplásticos |
| KR102354675B1 (ko) | 2013-08-15 | 2022-01-24 | 인튜어티브 서지컬 오퍼레이션즈 인코포레이티드 | 의료 절차 확인을 위한 시스템 및 방법 |
| CZ307015B6 (cs) | 2014-06-03 | 2017-11-15 | Nafigate Corporation, A.S. | Způsob izolace polyhydroxyalkanoátů z biomasy fermentované mikroorganismy produkujícími polyhydroxyalkanoáty a/nebo z biomasy obsahující alespoň jednu plodinu produkující polyhydroxyalkanoáty |
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Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS59205992A (ja) * | 1983-04-28 | 1984-11-21 | インペリアル・ケミカル・インダストリ−ズ・ピ−エルシ− | ヒドロキシブチレ−ト重合体の抽出方法 |
Family Cites Families (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US1934677A (en) * | 1930-09-02 | 1933-11-14 | California Packing Corp | Method of treating fish |
| US2602045A (en) * | 1946-08-03 | 1952-07-01 | Commercial Solvents Corp | Azeotropic distillation process for preparing pure, crystalline penicillin salts |
| DE1263006B (de) * | 1964-05-22 | 1968-03-14 | Huels Chemische Werke Ag | Verfahren zur Aufarbeitung der bei der Herstellung von 2-Alkyl-delta 2-oxazolinen anfallenden wasserhaltigen Reaktionsgemische |
| US3687819A (en) * | 1970-04-03 | 1972-08-29 | Viobin Corp | Process and apparatus for producing fat and nutritious defatted solids from fatty biological material containing water |
| JPS5428895A (en) * | 1977-08-01 | 1979-03-03 | Kao Corp | Dehydration purification of fermentation products |
| FR2446859A1 (fr) * | 1979-01-22 | 1980-08-14 | Solvay | Procede de separation de poly-b-hydroxybutyrates d'une biomasse |
| EP0015123B1 (en) * | 1979-02-21 | 1982-12-22 | Imperial Chemical Industries Plc | A process for the extraction of poly-3-hydroxy-butyric acid from microbial cells |
| FR2486072A1 (fr) * | 1980-07-03 | 1982-01-08 | Solvay | Procede pour la fabrication de l'acide b-hydroxybutyrique et de ses oligocondensats |
| DE3161370D1 (en) * | 1980-08-13 | 1983-12-15 | Ici Plc | Extraction of poly(beta-hydroxy butyric acid) |
| DE3264345D1 (en) * | 1981-02-12 | 1985-08-01 | Ici Plc | Extraction of poly(beta-hydroxybutyric acid) |
| GB2120671B (en) * | 1982-05-27 | 1986-02-12 | Ici Plc | Separation process |
-
1984
- 1984-07-06 FR FR8410921A patent/FR2567149B1/fr not_active Expired
-
1985
- 1985-06-19 US US06/746,381 patent/US4705604A/en not_active Expired - Fee Related
- 1985-06-25 DE DE8585201004T patent/DE3561472D1/de not_active Expired
- 1985-06-25 AT AT85201004T patent/ATE32102T1/de not_active IP Right Cessation
- 1985-06-25 EP EP85201004A patent/EP0168095B1/fr not_active Expired
- 1985-07-05 JP JP14814085A patent/JPS6135790A/ja active Granted
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS59205992A (ja) * | 1983-04-28 | 1984-11-21 | インペリアル・ケミカル・インダストリ−ズ・ピ−エルシ− | ヒドロキシブチレ−ト重合体の抽出方法 |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2006035889A1 (ja) * | 2004-09-30 | 2006-04-06 | Kaneka Corporation | ポリヒドロキシアルカノエートの製造方法 |
| JPWO2006035889A1 (ja) * | 2004-09-30 | 2008-05-15 | 株式会社カネカ | ポリヒドロキシアルカノエートの製造方法 |
| JP5507793B2 (ja) * | 2004-09-30 | 2014-05-28 | メレディアン， インク． | ポリヒドロキシアルカノエートの製造方法 |
Also Published As
| Publication number | Publication date |
|---|---|
| DE3561472D1 (en) | 1988-02-25 |
| FR2567149A1 (fr) | 1986-01-10 |
| FR2567149B1 (fr) | 1986-12-05 |
| JPH0581239B2 (enExample) | 1993-11-11 |
| EP0168095B1 (fr) | 1988-01-20 |
| EP0168095A1 (fr) | 1986-01-15 |
| US4705604A (en) | 1987-11-10 |
| ATE32102T1 (de) | 1988-02-15 |
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