JPS61281065A - 高温強度が優れたアルミナ・シリカ系セラミツクス焼結体の製造方法 - Google Patents
高温強度が優れたアルミナ・シリカ系セラミツクス焼結体の製造方法Info
- Publication number
- JPS61281065A JPS61281065A JP60123127A JP12312785A JPS61281065A JP S61281065 A JPS61281065 A JP S61281065A JP 60123127 A JP60123127 A JP 60123127A JP 12312785 A JP12312785 A JP 12312785A JP S61281065 A JPS61281065 A JP S61281065A
- Authority
- JP
- Japan
- Prior art keywords
- sintered body
- alumina
- strength
- raw material
- silica
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 title claims description 79
- 239000000377 silicon dioxide Substances 0.000 title claims description 49
- 239000000919 ceramic Substances 0.000 title claims description 19
- 238000004519 manufacturing process Methods 0.000 title claims description 19
- 239000000843 powder Substances 0.000 claims description 72
- 238000000034 method Methods 0.000 claims description 47
- 239000000203 mixture Substances 0.000 claims description 34
- 239000012535 impurity Substances 0.000 claims description 29
- AZDRQVAHHNSJOQ-UHFFFAOYSA-N alumane Chemical class [AlH3] AZDRQVAHHNSJOQ-UHFFFAOYSA-N 0.000 claims description 9
- 238000005245 sintering Methods 0.000 claims description 9
- 238000005118 spray pyrolysis Methods 0.000 claims description 8
- 230000002194 synthesizing effect Effects 0.000 claims description 5
- 125000000217 alkyl group Chemical group 0.000 claims description 3
- 238000001354 calcination Methods 0.000 claims description 2
- 238000007493 shaping process Methods 0.000 claims description 2
- 239000003021 water soluble solvent Substances 0.000 claims description 2
- 238000006116 polymerization reaction Methods 0.000 claims 1
- 239000002994 raw material Substances 0.000 description 60
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 27
- KZHJGOXRZJKJNY-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Si]=O.O=[Al]O[Al]=O.O=[Al]O[Al]=O.O=[Al]O[Al]=O KZHJGOXRZJKJNY-UHFFFAOYSA-N 0.000 description 24
- 229910052863 mullite Inorganic materials 0.000 description 24
- 239000011521 glass Substances 0.000 description 21
- 239000012071 phase Substances 0.000 description 19
- 229910052681 coesite Inorganic materials 0.000 description 18
- 229910052906 cristobalite Inorganic materials 0.000 description 18
- 230000007423 decrease Effects 0.000 description 18
- 229910052682 stishovite Inorganic materials 0.000 description 18
- 229910052905 tridymite Inorganic materials 0.000 description 18
- KKCBUQHMOMHUOY-UHFFFAOYSA-N Na2O Inorganic materials [O-2].[Na+].[Na+] KKCBUQHMOMHUOY-UHFFFAOYSA-N 0.000 description 17
- 235000012239 silicon dioxide Nutrition 0.000 description 14
- 238000012360 testing method Methods 0.000 description 14
- 229910052593 corundum Inorganic materials 0.000 description 11
- 239000000243 solution Substances 0.000 description 11
- 229910001845 yogo sapphire Inorganic materials 0.000 description 11
- -1 aluminum alkoxide Chemical class 0.000 description 10
- 238000005452 bending Methods 0.000 description 10
- 238000002156 mixing Methods 0.000 description 8
- 229910052710 silicon Inorganic materials 0.000 description 8
- BOTDANWDWHJENH-UHFFFAOYSA-N Tetraethyl orthosilicate Chemical compound CCO[Si](OCC)(OCC)OCC BOTDANWDWHJENH-UHFFFAOYSA-N 0.000 description 7
- 238000013001 point bending Methods 0.000 description 7
- 239000010703 silicon Substances 0.000 description 7
- 238000010438 heat treatment Methods 0.000 description 6
- 239000003513 alkali Substances 0.000 description 5
- 150000004703 alkoxides Chemical class 0.000 description 5
- 229910052782 aluminium Inorganic materials 0.000 description 5
- 230000015572 biosynthetic process Effects 0.000 description 5
- 238000007796 conventional method Methods 0.000 description 5
- 238000006073 displacement reaction Methods 0.000 description 5
- 239000011224 oxide ceramic Substances 0.000 description 5
- 229910052574 oxide ceramic Inorganic materials 0.000 description 5
- 238000003786 synthesis reaction Methods 0.000 description 5
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 4
- SMZOGRDCAXLAAR-UHFFFAOYSA-N aluminium isopropoxide Chemical compound [Al+3].CC(C)[O-].CC(C)[O-].CC(C)[O-] SMZOGRDCAXLAAR-UHFFFAOYSA-N 0.000 description 4
- 238000001879 gelation Methods 0.000 description 4
- 230000003301 hydrolyzing effect Effects 0.000 description 4
- 239000011259 mixed solution Substances 0.000 description 4
- 238000001308 synthesis method Methods 0.000 description 4
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
- 238000000975 co-precipitation Methods 0.000 description 3
- 239000013078 crystal Substances 0.000 description 3
- 238000010586 diagram Methods 0.000 description 3
- 239000000499 gel Substances 0.000 description 3
- 238000000465 moulding Methods 0.000 description 3
- 239000011734 sodium Substances 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- BNGXYYYYKUGPPF-UHFFFAOYSA-M (3-methylphenyl)methyl-triphenylphosphanium;chloride Chemical compound [Cl-].CC1=CC=CC(C[P+](C=2C=CC=CC=2)(C=2C=CC=CC=2)C=2C=CC=CC=2)=C1 BNGXYYYYKUGPPF-UHFFFAOYSA-M 0.000 description 2
- BPQQTUXANYXVAA-UHFFFAOYSA-N Orthosilicate Chemical compound [O-][Si]([O-])([O-])[O-] BPQQTUXANYXVAA-UHFFFAOYSA-N 0.000 description 2
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 2
- JLDSOYXADOWAKB-UHFFFAOYSA-N aluminium nitrate Chemical compound [Al+3].[O-][N+]([O-])=O.[O-][N+]([O-])=O.[O-][N+]([O-])=O JLDSOYXADOWAKB-UHFFFAOYSA-N 0.000 description 2
- BYFGZMCJNACEKR-UHFFFAOYSA-N aluminium(i) oxide Chemical compound [Al]O[Al] BYFGZMCJNACEKR-UHFFFAOYSA-N 0.000 description 2
- 229910021529 ammonia Inorganic materials 0.000 description 2
- 239000007864 aqueous solution Substances 0.000 description 2
- 239000012153 distilled water Substances 0.000 description 2
- 230000007062 hydrolysis Effects 0.000 description 2
- 238000006460 hydrolysis reaction Methods 0.000 description 2
- NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical compound O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 238000002844 melting Methods 0.000 description 2
- 230000008018 melting Effects 0.000 description 2
- 239000002245 particle Substances 0.000 description 2
- 238000012827 research and development Methods 0.000 description 2
- 239000000741 silica gel Substances 0.000 description 2
- 229910002027 silica gel Inorganic materials 0.000 description 2
- 239000002904 solvent Substances 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- FUJCRWPEOMXPAD-UHFFFAOYSA-N Li2O Inorganic materials [Li+].[Li+].[O-2] FUJCRWPEOMXPAD-UHFFFAOYSA-N 0.000 description 1
- 229910002651 NO3 Inorganic materials 0.000 description 1
- 239000004115 Sodium Silicate Substances 0.000 description 1
- 229910000272 alkali metal oxide Inorganic materials 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000010304 firing Methods 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- 239000008240 homogeneous mixture Substances 0.000 description 1
- 239000007791 liquid phase Substances 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 230000000704 physical effect Effects 0.000 description 1
- NOTVAPJNGZMVSD-UHFFFAOYSA-N potassium monoxide Inorganic materials [K]O[K] NOTVAPJNGZMVSD-UHFFFAOYSA-N 0.000 description 1
- RMAQACBXLXPBSY-UHFFFAOYSA-N silicic acid Chemical compound O[Si](O)(O)O RMAQACBXLXPBSY-UHFFFAOYSA-N 0.000 description 1
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 description 1
- 229910052911 sodium silicate Inorganic materials 0.000 description 1
- RPACBEVZENYWOL-XFULWGLBSA-M sodium;(2r)-2-[6-(4-chlorophenoxy)hexyl]oxirane-2-carboxylate Chemical compound [Na+].C=1C=C(Cl)C=CC=1OCCCCCC[C@]1(C(=O)[O-])CO1 RPACBEVZENYWOL-XFULWGLBSA-M 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 239000000725 suspension Substances 0.000 description 1
- 239000011345 viscous material Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/01—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
- C04B35/16—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on silicates other than clay
- C04B35/18—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on silicates other than clay rich in aluminium oxide
Landscapes
- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Ceramic Engineering (AREA)
- Manufacturing & Machinery (AREA)
- Materials Engineering (AREA)
- Structural Engineering (AREA)
- Organic Chemistry (AREA)
- Compositions Of Oxide Ceramics (AREA)
Priority Applications (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP60123127A JPS61281065A (ja) | 1985-06-06 | 1985-06-06 | 高温強度が優れたアルミナ・シリカ系セラミツクス焼結体の製造方法 |
| DE19863618758 DE3618758A1 (de) | 1985-06-06 | 1986-06-04 | Verfahren zur herstellung von gesinterten tonerde-silika-keramiken mit verbesserter hochtemperaturfestigkeit |
| GB8613829A GB2177390B (en) | 1985-06-06 | 1986-06-05 | Process for producing alumina silica sintered ceramics having improved high-temperature strength |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP60123127A JPS61281065A (ja) | 1985-06-06 | 1985-06-06 | 高温強度が優れたアルミナ・シリカ系セラミツクス焼結体の製造方法 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| JPS61281065A true JPS61281065A (ja) | 1986-12-11 |
Family
ID=14852847
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP60123127A Pending JPS61281065A (ja) | 1985-06-06 | 1985-06-06 | 高温強度が優れたアルミナ・シリカ系セラミツクス焼結体の製造方法 |
Country Status (3)
| Country | Link |
|---|---|
| JP (1) | JPS61281065A (enrdf_load_stackoverflow) |
| DE (1) | DE3618758A1 (enrdf_load_stackoverflow) |
| GB (1) | GB2177390B (enrdf_load_stackoverflow) |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE4228711A1 (de) * | 1992-08-28 | 1994-03-03 | Degussa | Silicium-Aluminium-Mischoxid |
| DE10117776B4 (de) * | 2001-04-09 | 2004-08-26 | The Morgan Crucible Co. Plc., Windsor | Hochtemperaturbeständiger feinkeramischer gesinterter Werkstoff |
| EP2778144A1 (de) * | 2013-03-11 | 2014-09-17 | Keramik Holding AG Laufen | Keramisches Material |
| CN116639957B (zh) * | 2023-05-19 | 2024-07-02 | 萍乡市石化填料有限责任公司 | 一种强耐碱的瓷球及其制备方法 |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS58199711A (ja) * | 1982-05-18 | 1983-11-21 | Dainippon Ink & Chem Inc | アルミノ・シリケ−ト粉末の製造方法 |
| US4427785A (en) * | 1982-05-25 | 1984-01-24 | General Electric Company | Optically translucent ceramic |
-
1985
- 1985-06-06 JP JP60123127A patent/JPS61281065A/ja active Pending
-
1986
- 1986-06-04 DE DE19863618758 patent/DE3618758A1/de active Granted
- 1986-06-05 GB GB8613829A patent/GB2177390B/en not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| GB2177390A (en) | 1987-01-21 |
| DE3618758C2 (enrdf_load_stackoverflow) | 1990-02-01 |
| DE3618758A1 (de) | 1987-01-02 |
| GB8613829D0 (en) | 1986-07-09 |
| GB2177390B (en) | 1989-02-22 |
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