JPS61191518A - 誘電体磁器製造用低温焼結性原料粉末の製造法 - Google Patents
誘電体磁器製造用低温焼結性原料粉末の製造法Info
- Publication number
- JPS61191518A JPS61191518A JP60027942A JP2794285A JPS61191518A JP S61191518 A JPS61191518 A JP S61191518A JP 60027942 A JP60027942 A JP 60027942A JP 2794285 A JP2794285 A JP 2794285A JP S61191518 A JPS61191518 A JP S61191518A
- Authority
- JP
- Japan
- Prior art keywords
- raw material
- material powder
- powder
- low
- producing
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000000843 powder Substances 0.000 title claims abstract description 77
- 239000002994 raw material Substances 0.000 title claims abstract description 73
- 229910052573 porcelain Inorganic materials 0.000 title claims abstract description 13
- 238000004519 manufacturing process Methods 0.000 title claims description 31
- 239000000203 mixture Substances 0.000 claims abstract description 21
- 239000003960 organic solvent Substances 0.000 claims abstract description 17
- 239000002131 composite material Substances 0.000 claims abstract description 14
- 229910000464 lead oxide Inorganic materials 0.000 claims abstract description 12
- 238000001354 calcination Methods 0.000 claims abstract description 11
- 229910052725 zinc Inorganic materials 0.000 claims abstract description 8
- 229910052759 nickel Inorganic materials 0.000 claims abstract description 7
- 229910052749 magnesium Inorganic materials 0.000 claims abstract description 5
- 239000007795 chemical reaction product Substances 0.000 claims abstract description 4
- 229910052758 niobium Inorganic materials 0.000 claims abstract description 4
- 229910052719 titanium Inorganic materials 0.000 claims abstract description 4
- 229910052726 zirconium Inorganic materials 0.000 claims abstract description 4
- 229910052751 metal Inorganic materials 0.000 claims description 17
- 239000002184 metal Substances 0.000 claims description 17
- -1 amine compound Chemical class 0.000 claims description 12
- 239000002002 slurry Substances 0.000 claims description 12
- 239000002244 precipitate Substances 0.000 claims description 9
- 150000004703 alkoxides Chemical class 0.000 claims description 8
- 150000002902 organometallic compounds Chemical class 0.000 claims description 4
- 125000004432 carbon atom Chemical group C* 0.000 claims description 3
- 150000001735 carboxylic acids Chemical class 0.000 claims 1
- YEXPOXQUZXUXJW-UHFFFAOYSA-N oxolead Chemical compound [Pb]=O YEXPOXQUZXUXJW-UHFFFAOYSA-N 0.000 claims 1
- HTUMBQDCCIXGCV-UHFFFAOYSA-N lead oxide Chemical compound [O-2].[Pb+2] HTUMBQDCCIXGCV-UHFFFAOYSA-N 0.000 abstract description 12
- 238000005245 sintering Methods 0.000 abstract description 10
- 230000003301 hydrolyzing effect Effects 0.000 abstract description 7
- 239000010936 titanium Substances 0.000 abstract description 7
- ZMANZCXQSJIPKH-UHFFFAOYSA-N Triethylamine Chemical compound CCN(CC)CC ZMANZCXQSJIPKH-UHFFFAOYSA-N 0.000 abstract description 6
- 229910052748 manganese Inorganic materials 0.000 abstract description 6
- 150000003839 salts Chemical class 0.000 abstract description 3
- 150000007942 carboxylates Chemical class 0.000 abstract description 2
- 150000001732 carboxylic acid derivatives Chemical class 0.000 abstract description 2
- 150000001412 amines Chemical class 0.000 abstract 2
- 238000001556 precipitation Methods 0.000 abstract 2
- 239000011701 zinc Substances 0.000 abstract 2
- FIPWRIJSWJWJAI-UHFFFAOYSA-N Butyl carbitol 6-propylpiperonyl ether Chemical compound C1=C(CCC)C(COCCOCCOCCCC)=CC2=C1OCO2 FIPWRIJSWJWJAI-UHFFFAOYSA-N 0.000 abstract 1
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 abstract 1
- ZOIORXHNWRGPMV-UHFFFAOYSA-N acetic acid;zinc Chemical compound [Zn].CC(O)=O.CC(O)=O ZOIORXHNWRGPMV-UHFFFAOYSA-N 0.000 abstract 1
- 229960005235 piperonyl butoxide Drugs 0.000 abstract 1
- 239000000126 substance Substances 0.000 abstract 1
- 239000004246 zinc acetate Substances 0.000 abstract 1
- 239000000919 ceramic Substances 0.000 description 23
- 238000000034 method Methods 0.000 description 23
- 239000002245 particle Substances 0.000 description 18
- 239000000243 solution Substances 0.000 description 17
- 230000007062 hydrolysis Effects 0.000 description 11
- 238000006460 hydrolysis reaction Methods 0.000 description 11
- LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 description 10
- 230000000052 comparative effect Effects 0.000 description 9
- CPLXHLVBOLITMK-UHFFFAOYSA-N Magnesium oxide Chemical compound [Mg]=O CPLXHLVBOLITMK-UHFFFAOYSA-N 0.000 description 8
- CTQNGGLPUBDAKN-UHFFFAOYSA-N O-Xylene Chemical compound CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 description 6
- 239000000047 product Substances 0.000 description 6
- 239000008096 xylene Substances 0.000 description 6
- 238000006243 chemical reaction Methods 0.000 description 5
- 238000007796 conventional method Methods 0.000 description 5
- 239000002904 solvent Substances 0.000 description 5
- ROSDSFDQCJNGOL-UHFFFAOYSA-N Dimethylamine Chemical compound CNC ROSDSFDQCJNGOL-UHFFFAOYSA-N 0.000 description 4
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 4
- 125000003277 amino group Chemical group 0.000 description 4
- 239000012298 atmosphere Substances 0.000 description 4
- 239000000395 magnesium oxide Substances 0.000 description 4
- 238000000465 moulding Methods 0.000 description 4
- 239000007864 aqueous solution Substances 0.000 description 3
- 230000001186 cumulative effect Effects 0.000 description 3
- HPNMFZURTQLUMO-UHFFFAOYSA-N diethylamine Chemical compound CCNCC HPNMFZURTQLUMO-UHFFFAOYSA-N 0.000 description 3
- 238000001035 drying Methods 0.000 description 3
- 150000004679 hydroxides Chemical class 0.000 description 3
- 238000005259 measurement Methods 0.000 description 3
- 239000012071 phase Substances 0.000 description 3
- 238000010992 reflux Methods 0.000 description 3
- 238000010532 solid phase synthesis reaction Methods 0.000 description 3
- 239000006104 solid solution Substances 0.000 description 3
- 125000001424 substituent group Chemical group 0.000 description 3
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 2
- QUSNBJAOOMFDIB-UHFFFAOYSA-N Ethylamine Chemical compound CCN QUSNBJAOOMFDIB-UHFFFAOYSA-N 0.000 description 2
- BAVYZALUXZFZLV-UHFFFAOYSA-N Methylamine Chemical compound NC BAVYZALUXZFZLV-UHFFFAOYSA-N 0.000 description 2
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 2
- 244000309464 bull Species 0.000 description 2
- 150000001734 carboxylic acid salts Chemical class 0.000 description 2
- 238000000975 co-precipitation Methods 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 239000007772 electrode material Substances 0.000 description 2
- 230000001747 exhibiting effect Effects 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 239000012456 homogeneous solution Substances 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 description 2
- XMFOQHDPRMAJNU-UHFFFAOYSA-N lead(ii,iv) oxide Chemical compound O1[Pb]O[Pb]11O[Pb]O1 XMFOQHDPRMAJNU-UHFFFAOYSA-N 0.000 description 2
- 238000009766 low-temperature sintering Methods 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 150000002736 metal compounds Chemical class 0.000 description 2
- 229910044991 metal oxide Inorganic materials 0.000 description 2
- 150000004706 metal oxides Chemical class 0.000 description 2
- 150000002739 metals Chemical class 0.000 description 2
- 125000002524 organometallic group Chemical group 0.000 description 2
- 229910052760 oxygen Inorganic materials 0.000 description 2
- 238000011160 research Methods 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- 238000002441 X-ray diffraction Methods 0.000 description 1
- 150000001242 acetic acid derivatives Chemical class 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 150000001298 alcohols Chemical class 0.000 description 1
- 239000004411 aluminium Substances 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 239000011230 binding agent Substances 0.000 description 1
- 239000003990 capacitor Substances 0.000 description 1
- 150000004649 carbonic acid derivatives Chemical class 0.000 description 1
- 239000013256 coordination polymer Substances 0.000 description 1
- NKZSPGSOXYXWQA-UHFFFAOYSA-N dioxido(oxo)titanium;lead(2+) Chemical compound [Pb+2].[O-][Ti]([O-])=O NKZSPGSOXYXWQA-UHFFFAOYSA-N 0.000 description 1
- 238000011549 displacement method Methods 0.000 description 1
- 230000005684 electric field Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 238000010304 firing Methods 0.000 description 1
- 230000001788 irregular Effects 0.000 description 1
- 229910052745 lead Inorganic materials 0.000 description 1
- VJPLIHZPOJDHLB-UHFFFAOYSA-N lead titanium Chemical compound [Ti].[Pb] VJPLIHZPOJDHLB-UHFFFAOYSA-N 0.000 description 1
- 125000000956 methoxy group Chemical group [H]C([H])([H])O* 0.000 description 1
- 239000011259 mixed solution Substances 0.000 description 1
- 239000012046 mixed solvent Substances 0.000 description 1
- 239000012299 nitrogen atmosphere Substances 0.000 description 1
- 239000012454 non-polar solvent Substances 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 239000002798 polar solvent Substances 0.000 description 1
- 239000002243 precursor Substances 0.000 description 1
- 238000004062 sedimentation Methods 0.000 description 1
- 229920002545 silicone oil Polymers 0.000 description 1
- 239000007790 solid phase Substances 0.000 description 1
- 238000000638 solvent extraction Methods 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 229910052715 tantalum Inorganic materials 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 description 1
- XQQWBPOEMYKKBY-UHFFFAOYSA-H trimagnesium;dicarbonate;dihydroxide Chemical compound [OH-].[OH-].[Mg+2].[Mg+2].[Mg+2].[O-]C([O-])=O.[O-]C([O-])=O XQQWBPOEMYKKBY-UHFFFAOYSA-H 0.000 description 1
Landscapes
- Compositions Of Oxide Ceramics (AREA)
- Inorganic Compounds Of Heavy Metals (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP60027942A JPS61191518A (ja) | 1985-02-15 | 1985-02-15 | 誘電体磁器製造用低温焼結性原料粉末の製造法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP60027942A JPS61191518A (ja) | 1985-02-15 | 1985-02-15 | 誘電体磁器製造用低温焼結性原料粉末の製造法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS61191518A true JPS61191518A (ja) | 1986-08-26 |
| JPH0542371B2 JPH0542371B2 (enrdf_load_stackoverflow) | 1993-06-28 |
Family
ID=12234942
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP60027942A Granted JPS61191518A (ja) | 1985-02-15 | 1985-02-15 | 誘電体磁器製造用低温焼結性原料粉末の製造法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS61191518A (enrdf_load_stackoverflow) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2004005194A1 (ja) * | 2002-07-09 | 2004-01-15 | Daihatsu Motor Co., Ltd. | ペロブスカイト型複合酸化物の製造方法 |
| US7205257B2 (en) | 2002-07-09 | 2007-04-17 | Daihatsu Motor Co., Ltd. | Catalyst for clarifying exhaust gas |
-
1985
- 1985-02-15 JP JP60027942A patent/JPS61191518A/ja active Granted
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2004005194A1 (ja) * | 2002-07-09 | 2004-01-15 | Daihatsu Motor Co., Ltd. | ペロブスカイト型複合酸化物の製造方法 |
| US7205257B2 (en) | 2002-07-09 | 2007-04-17 | Daihatsu Motor Co., Ltd. | Catalyst for clarifying exhaust gas |
| US7381394B2 (en) | 2002-07-09 | 2008-06-03 | Daihatsu Motor Co., Ltd. | Method for producing perovskite-type composite oxide |
| CN100393629C (zh) * | 2002-07-09 | 2008-06-11 | 大发工业株式会社 | 钙钛矿型复合氧化物的制造方法 |
| US7622418B2 (en) | 2002-07-09 | 2009-11-24 | Daihatsu Motor Company, Ltd. | Method for producing exhaust gas purifying catalyst |
Also Published As
| Publication number | Publication date |
|---|---|
| JPH0542371B2 (enrdf_load_stackoverflow) | 1993-06-28 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| Gu et al. | Single‐Calcination Synthesis of Pyrochlore‐Free 0.9 Pb (Mg1/3Nb2/3) O3–0.1 PbTiO3 and Pb (Mg1/3Nb2/3) O3 Ceramics Using a Coating Method | |
| KR101786056B1 (ko) | 코어쉘 구조를 갖는 저온소성용 무연압전 세라믹 및 그 제조 방법 | |
| JPS61191518A (ja) | 誘電体磁器製造用低温焼結性原料粉末の製造法 | |
| JPS63236713A (ja) | ペロブスカイト型化合物の無機微粉体の製造方法 | |
| JPS61191519A (ja) | 誘電体磁器製造用低温焼結性原料粉末の製法 | |
| JPS61232217A (ja) | 誘電体磁器製造用の低温焼結性原料粉末の製造方法 | |
| JPS61174116A (ja) | ペロブスカイト型酸化物の製造法 | |
| JP3710100B2 (ja) | 酸化物圧電材料の製造方法 | |
| JPS62241825A (ja) | 赤外線センサー用焦電体磁器の製法 | |
| JPS6259529A (ja) | チタン含有易焼結性ペロブスカイトおよびその固溶体の原料粉末の製造方法 | |
| JPS61232218A (ja) | 誘電体磁器製造用原料粉末の製造方法 | |
| KR101249585B1 (ko) | 복합금속산화물 분말의 제조방법 | |
| JP2841344B2 (ja) | 圧電体セラミックス組成物 | |
| JPH05330908A (ja) | 緩和型強誘電体磁器原料粉末の製造方法 | |
| JPH0354120A (ja) | 誘電体磁器組成物を製造するための原料粉末の製法 | |
| JPH0433383A (ja) | 圧電体セラミックスの製造方法 | |
| JPH0457615B2 (enrdf_load_stackoverflow) | ||
| JPS62162670A (ja) | チタン酸ジルコン酸鉛焼結体の製法 | |
| JPH0354122A (ja) | 誘電体磁器組成物を製造するための原料粉末の新規な製造方法 | |
| JPH0193419A (ja) | 圧電セラミックス原料粉末の製造方法 | |
| JPS63190717A (ja) | 低温焼結用複合ペロブスカイトの原料粉末の製造方法 | |
| JPS63225523A (ja) | ペロブスカイト原料粉末の製法 | |
| JPH02279523A (ja) | 鉛含有酸化物の製造方法 | |
| JP2000001369A (ja) | 高性能電歪セラミックス | |
| JPH08239268A (ja) | 圧電磁器組成物及びその粉末の製造方法 |