JPS61120833A - ポリフエニレンスルフイド樹脂の精製方法 - Google Patents
ポリフエニレンスルフイド樹脂の精製方法Info
- Publication number
- JPS61120833A JPS61120833A JP59242010A JP24201084A JPS61120833A JP S61120833 A JPS61120833 A JP S61120833A JP 59242010 A JP59242010 A JP 59242010A JP 24201084 A JP24201084 A JP 24201084A JP S61120833 A JPS61120833 A JP S61120833A
- Authority
- JP
- Japan
- Prior art keywords
- resin
- polyphenylene sulfide
- sulfide resin
- deionized water
- methylpyrrolidone
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000011347 resin Substances 0.000 title claims abstract description 55
- 229920005989 resin Polymers 0.000 title claims abstract description 55
- 239000004734 Polyphenylene sulfide Substances 0.000 title claims abstract description 44
- 229920000069 polyphenylene sulfide Polymers 0.000 title claims abstract description 44
- 238000000746 purification Methods 0.000 title description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 23
- 239000008367 deionised water Substances 0.000 claims abstract description 19
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 19
- SECXISVLQFMRJM-UHFFFAOYSA-N N-Methylpyrrolidone Chemical compound CN1CCCC1=O SECXISVLQFMRJM-UHFFFAOYSA-N 0.000 claims abstract description 16
- 239000000203 mixture Substances 0.000 claims abstract description 8
- 238000010438 heat treatment Methods 0.000 claims abstract description 7
- 238000000034 method Methods 0.000 claims description 21
- 239000012535 impurity Substances 0.000 abstract description 20
- 150000001450 anions Chemical class 0.000 abstract description 3
- 229960001545 hydrotalcite Drugs 0.000 abstract description 3
- 229910001701 hydrotalcite Inorganic materials 0.000 abstract description 3
- 229910021645 metal ion Inorganic materials 0.000 abstract description 3
- GDVKFRBCXAPAQJ-UHFFFAOYSA-A dialuminum;hexamagnesium;carbonate;hexadecahydroxide Chemical compound [OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[Mg+2].[Mg+2].[Mg+2].[Mg+2].[Mg+2].[Mg+2].[Al+3].[Al+3].[O-]C([O-])=O GDVKFRBCXAPAQJ-UHFFFAOYSA-A 0.000 abstract 2
- 229910052742 iron Inorganic materials 0.000 abstract 2
- 229910052782 aluminium Inorganic materials 0.000 abstract 1
- 229910052804 chromium Inorganic materials 0.000 abstract 1
- 229910052802 copper Inorganic materials 0.000 abstract 1
- 229910052749 magnesium Inorganic materials 0.000 abstract 1
- 229910052748 manganese Inorganic materials 0.000 abstract 1
- 239000003792 electrolyte Substances 0.000 description 12
- -1 Polyphenylene sulfite Polymers 0.000 description 10
- 239000000047 product Substances 0.000 description 9
- 230000000052 comparative effect Effects 0.000 description 7
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 6
- 150000002500 ions Chemical class 0.000 description 6
- 229920000642 polymer Polymers 0.000 description 5
- 238000006243 chemical reaction Methods 0.000 description 4
- PWZFXELTLAQOKC-UHFFFAOYSA-A dialuminum;hexamagnesium;carbonate;hexadecahydroxide;tetrahydrate Chemical compound O.O.O.O.[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[Mg+2].[Mg+2].[Mg+2].[Mg+2].[Mg+2].[Mg+2].[Al+3].[Al+3].[O-]C([O-])=O PWZFXELTLAQOKC-UHFFFAOYSA-A 0.000 description 4
- 239000000126 substance Substances 0.000 description 4
- 229910001868 water Inorganic materials 0.000 description 4
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
- 229920001577 copolymer Polymers 0.000 description 3
- 238000006116 polymerization reaction Methods 0.000 description 3
- 238000012545 processing Methods 0.000 description 3
- 239000011780 sodium chloride Substances 0.000 description 3
- XHKFBADIZIDYBU-UCMJJCQDSA-N 1-ethoxycarbonyloxyethyl (2s,5r,6r)-6-(azepan-1-ylmethylideneamino)-3,3-dimethyl-7-oxo-4-thia-1-azabicyclo[3.2.0]heptane-2-carboxylate Chemical compound N([C@H]1[C@@H]2N(C1=O)[C@H](C(S2)(C)C)C(=O)OC(C)OC(=O)OCC)=CN1CCCCCC1 XHKFBADIZIDYBU-UCMJJCQDSA-N 0.000 description 2
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 2
- 229910052783 alkali metal Inorganic materials 0.000 description 2
- 150000003857 carboxamides Chemical class 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 239000011248 coating agent Substances 0.000 description 2
- 238000000576 coating method Methods 0.000 description 2
- 238000000605 extraction Methods 0.000 description 2
- 239000000835 fiber Substances 0.000 description 2
- 238000001914 filtration Methods 0.000 description 2
- 229910052751 metal Inorganic materials 0.000 description 2
- 239000002184 metal Substances 0.000 description 2
- 150000002739 metals Chemical class 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- 239000000843 powder Substances 0.000 description 2
- 239000012264 purified product Substances 0.000 description 2
- 229910001415 sodium ion Inorganic materials 0.000 description 2
- 239000000243 solution Substances 0.000 description 2
- 239000002904 solvent Substances 0.000 description 2
- 239000012085 test solution Substances 0.000 description 2
- NWUYHJFMYQTDRP-UHFFFAOYSA-N 1,2-bis(ethenyl)benzene;1-ethenyl-2-ethylbenzene;styrene Chemical compound C=CC1=CC=CC=C1.CCC1=CC=CC=C1C=C.C=CC1=CC=CC=C1C=C NWUYHJFMYQTDRP-UHFFFAOYSA-N 0.000 description 1
- OCJBOOLMMGQPQU-UHFFFAOYSA-N 1,4-dichlorobenzene Chemical compound ClC1=CC=C(Cl)C=C1 OCJBOOLMMGQPQU-UHFFFAOYSA-N 0.000 description 1
- JTPNRXUCIXHOKM-UHFFFAOYSA-N 1-chloronaphthalene Chemical compound C1=CC=C2C(Cl)=CC=CC2=C1 JTPNRXUCIXHOKM-UHFFFAOYSA-N 0.000 description 1
- MUBZPKHOEPUJKR-UHFFFAOYSA-L Oxalate Chemical compound [O-]C(=O)C([O-])=O MUBZPKHOEPUJKR-UHFFFAOYSA-L 0.000 description 1
- 125000003545 alkoxy group Chemical group 0.000 description 1
- 125000000217 alkyl group Chemical group 0.000 description 1
- 125000003277 amino group Chemical group 0.000 description 1
- 238000005349 anion exchange Methods 0.000 description 1
- 239000003957 anion exchange resin Substances 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 238000011088 calibration curve Methods 0.000 description 1
- 239000003990 capacitor Substances 0.000 description 1
- 125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 description 1
- 239000003729 cation exchange resin Substances 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 238000007334 copolymerization reaction Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000010292 electrical insulation Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 125000001033 ether group Chemical group 0.000 description 1
- 238000010304 firing Methods 0.000 description 1
- 238000007429 general method Methods 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 229910052736 halogen Inorganic materials 0.000 description 1
- 150000004679 hydroxides Chemical class 0.000 description 1
- 238000004255 ion exchange chromatography Methods 0.000 description 1
- 150000002576 ketones Chemical group 0.000 description 1
- 229910052744 lithium Inorganic materials 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000012778 molding material Substances 0.000 description 1
- 238000006386 neutralization reaction Methods 0.000 description 1
- 125000000449 nitro group Chemical group [O-][N+](*)=O 0.000 description 1
- 239000012299 nitrogen atmosphere Substances 0.000 description 1
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- YGSDEFSMJLZEOE-UHFFFAOYSA-M salicylate Chemical compound OC1=CC=CC=C1C([O-])=O YGSDEFSMJLZEOE-UHFFFAOYSA-M 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- 239000003566 sealing material Substances 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 229940079101 sodium sulfide Drugs 0.000 description 1
- 229910052979 sodium sulfide Inorganic materials 0.000 description 1
- ZGHLCBJZQLNUAZ-UHFFFAOYSA-N sodium sulfide nonahydrate Chemical compound O.O.O.O.O.O.O.O.O.[Na+].[Na+].[S-2] ZGHLCBJZQLNUAZ-UHFFFAOYSA-N 0.000 description 1
- 229940048181 sodium sulfide nonahydrate Drugs 0.000 description 1
- WMDLZMCDBSJMTM-UHFFFAOYSA-M sodium;sulfanide;nonahydrate Chemical compound O.O.O.O.O.O.O.O.O.[Na+].[SH-] WMDLZMCDBSJMTM-UHFFFAOYSA-M 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000000638 solvent extraction Methods 0.000 description 1
- 239000012086 standard solution Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 150000004763 sulfides Chemical group 0.000 description 1
- 125000001174 sulfone group Chemical group 0.000 description 1
- 150000003457 sulfones Chemical group 0.000 description 1
- 238000003809 water extraction Methods 0.000 description 1
Landscapes
- Compositions Of Macromolecular Compounds (AREA)
- Polymers With Sulfur, Phosphorus Or Metals In The Main Chain (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP59242010A JPS61120833A (ja) | 1984-11-15 | 1984-11-15 | ポリフエニレンスルフイド樹脂の精製方法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP59242010A JPS61120833A (ja) | 1984-11-15 | 1984-11-15 | ポリフエニレンスルフイド樹脂の精製方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS61120833A true JPS61120833A (ja) | 1986-06-07 |
| JPH0240251B2 JPH0240251B2 (enrdf_load_stackoverflow) | 1990-09-11 |
Family
ID=17082915
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP59242010A Granted JPS61120833A (ja) | 1984-11-15 | 1984-11-15 | ポリフエニレンスルフイド樹脂の精製方法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS61120833A (enrdf_load_stackoverflow) |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH10265574A (ja) * | 1997-03-25 | 1998-10-06 | Idemitsu Petrochem Co Ltd | 残留ハロゲン化リチウムの変性方法 |
| JP2000034407A (ja) * | 1998-07-17 | 2000-02-02 | Matsushita Electric Works Ltd | 電子部品封止用樹脂組成物およびその製造方法、ならびにこの電子部品封止用樹脂組成物を用いた封止電子部品 |
| JP2003096298A (ja) * | 2001-09-25 | 2003-04-03 | Toray Ind Inc | ポリフェニレンスルフィド樹脂組成物およびコンデンサー用部品 |
| JP2007321032A (ja) * | 2006-05-31 | 2007-12-13 | Dainippon Ink & Chem Inc | 耐熱性樹脂組成物、及び表面実装用電子部品 |
| JP2018110108A (ja) * | 2016-12-12 | 2018-07-12 | 東レ株式会社 | 高分子電解質組成物、それを用いた高分子電解質膜、触媒層付電解質膜、膜電極複合体、固体高分子形燃料電池、固体高分子形水電解式水素発生装置および電気化学式水素圧縮装置、ならびに高分子電解質組成物の製造方法 |
| JP2020015843A (ja) * | 2018-07-26 | 2020-01-30 | Dic株式会社 | ポリアリーレンスルフィド樹脂の製造方法及び分離方法 |
| WO2023089962A1 (ja) * | 2021-11-18 | 2023-05-25 | Dic株式会社 | ポリアリーレンスルフィド樹脂混合物、樹脂組成物及び成形品ならびにそれらの製造方法 |
-
1984
- 1984-11-15 JP JP59242010A patent/JPS61120833A/ja active Granted
Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH10265574A (ja) * | 1997-03-25 | 1998-10-06 | Idemitsu Petrochem Co Ltd | 残留ハロゲン化リチウムの変性方法 |
| JP2000034407A (ja) * | 1998-07-17 | 2000-02-02 | Matsushita Electric Works Ltd | 電子部品封止用樹脂組成物およびその製造方法、ならびにこの電子部品封止用樹脂組成物を用いた封止電子部品 |
| JP2003096298A (ja) * | 2001-09-25 | 2003-04-03 | Toray Ind Inc | ポリフェニレンスルフィド樹脂組成物およびコンデンサー用部品 |
| JP2007321032A (ja) * | 2006-05-31 | 2007-12-13 | Dainippon Ink & Chem Inc | 耐熱性樹脂組成物、及び表面実装用電子部品 |
| JP2018110108A (ja) * | 2016-12-12 | 2018-07-12 | 東レ株式会社 | 高分子電解質組成物、それを用いた高分子電解質膜、触媒層付電解質膜、膜電極複合体、固体高分子形燃料電池、固体高分子形水電解式水素発生装置および電気化学式水素圧縮装置、ならびに高分子電解質組成物の製造方法 |
| JP2020015843A (ja) * | 2018-07-26 | 2020-01-30 | Dic株式会社 | ポリアリーレンスルフィド樹脂の製造方法及び分離方法 |
| WO2023089962A1 (ja) * | 2021-11-18 | 2023-05-25 | Dic株式会社 | ポリアリーレンスルフィド樹脂混合物、樹脂組成物及び成形品ならびにそれらの製造方法 |
| JP7334873B1 (ja) * | 2021-11-18 | 2023-08-29 | Dic株式会社 | ポリアリーレンスルフィド樹脂混合物、樹脂組成物及び成形品ならびにそれらの製造方法 |
| EP4435056A4 (en) * | 2021-11-18 | 2025-03-19 | DIC Corporation | POLY(ARYLENE SULFIDE) RESIN BLEND, RESIN COMPOSITION, MOULDED ARTICLES AND MANUFACTURING METHOD THEREOF |
Also Published As
| Publication number | Publication date |
|---|---|
| JPH0240251B2 (enrdf_load_stackoverflow) | 1990-09-11 |
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