JPS59144727A - フエニルアセトアルデヒドの製造法 - Google Patents
フエニルアセトアルデヒドの製造法Info
- Publication number
- JPS59144727A JPS59144727A JP58019133A JP1913383A JPS59144727A JP S59144727 A JPS59144727 A JP S59144727A JP 58019133 A JP58019133 A JP 58019133A JP 1913383 A JP1913383 A JP 1913383A JP S59144727 A JPS59144727 A JP S59144727A
- Authority
- JP
- Japan
- Prior art keywords
- alumina
- catalyst
- silica
- styrene oxide
- surface area
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- DTUQWGWMVIHBKE-UHFFFAOYSA-N phenylacetaldehyde Chemical compound O=CCC1=CC=CC=C1 DTUQWGWMVIHBKE-UHFFFAOYSA-N 0.000 title claims description 20
- 229940100595 phenylacetaldehyde Drugs 0.000 title claims description 10
- 239000003054 catalyst Substances 0.000 claims abstract description 25
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims abstract description 16
- AWMVMTVKBNGEAK-UHFFFAOYSA-N Styrene oxide Chemical compound C1OC1C1=CC=CC=C1 AWMVMTVKBNGEAK-UHFFFAOYSA-N 0.000 claims abstract description 15
- 238000004519 manufacturing process Methods 0.000 claims description 3
- 238000006555 catalytic reaction Methods 0.000 claims description 2
- 230000002194 synthesizing effect Effects 0.000 claims 1
- 238000006243 chemical reaction Methods 0.000 abstract description 18
- 239000007788 liquid Substances 0.000 abstract description 3
- 239000008122 artificial sweetener Substances 0.000 abstract description 2
- 235000021311 artificial sweeteners Nutrition 0.000 abstract description 2
- 150000001875 compounds Chemical class 0.000 abstract description 2
- 229940079593 drug Drugs 0.000 abstract description 2
- 239000003814 drug Substances 0.000 abstract description 2
- 239000000126 substance Substances 0.000 abstract description 2
- 239000007792 gaseous phase Substances 0.000 abstract 3
- 239000003905 agrochemical Substances 0.000 abstract 1
- 239000002304 perfume Substances 0.000 abstract 1
- 238000000034 method Methods 0.000 description 5
- 239000007864 aqueous solution Substances 0.000 description 4
- 238000006317 isomerization reaction Methods 0.000 description 4
- 239000000203 mixture Substances 0.000 description 4
- WRMNZCZEMHIOCP-UHFFFAOYSA-N 2-phenylethanol Chemical compound OCCC1=CC=CC=C1 WRMNZCZEMHIOCP-UHFFFAOYSA-N 0.000 description 3
- 230000007423 decrease Effects 0.000 description 3
- 230000003647 oxidation Effects 0.000 description 3
- 238000007254 oxidation reaction Methods 0.000 description 3
- VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 description 2
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 description 2
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
- 239000003513 alkali Substances 0.000 description 2
- 239000004927 clay Substances 0.000 description 2
- 238000006297 dehydration reaction Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000010304 firing Methods 0.000 description 2
- PWMWNFMRSKOCEY-UHFFFAOYSA-N 1-Phenyl-1,2-ethanediol Chemical compound OCC(O)C1=CC=CC=C1 PWMWNFMRSKOCEY-UHFFFAOYSA-N 0.000 description 1
- 238000004438 BET method Methods 0.000 description 1
- 241001474791 Proboscis Species 0.000 description 1
- 239000004115 Sodium Silicate Substances 0.000 description 1
- DIZPMCHEQGEION-UHFFFAOYSA-H aluminium sulfate (anhydrous) Chemical compound [Al+3].[Al+3].[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O DIZPMCHEQGEION-UHFFFAOYSA-H 0.000 description 1
- 235000011114 ammonium hydroxide Nutrition 0.000 description 1
- 238000001354 calcination Methods 0.000 description 1
- 230000003197 catalytic effect Effects 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 230000018044 dehydration Effects 0.000 description 1
- 239000003205 fragrance Substances 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- -1 phenyl glycide ester Chemical class 0.000 description 1
- 229940067107 phenylethyl alcohol Drugs 0.000 description 1
- 238000006116 polymerization reaction Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 230000005070 ripening Effects 0.000 description 1
- 238000007086 side reaction Methods 0.000 description 1
- 239000002002 slurry Substances 0.000 description 1
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 description 1
- 229910052911 sodium silicate Inorganic materials 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 238000001179 sorption measurement Methods 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 238000001256 steam distillation Methods 0.000 description 1
- 239000000725 suspension Substances 0.000 description 1
- 238000005292 vacuum distillation Methods 0.000 description 1
Classifications
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/52—Improvements relating to the production of bulk chemicals using catalysts, e.g. selective catalysts
Landscapes
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Catalysts (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP58019133A JPS59144727A (ja) | 1983-02-08 | 1983-02-08 | フエニルアセトアルデヒドの製造法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP58019133A JPS59144727A (ja) | 1983-02-08 | 1983-02-08 | フエニルアセトアルデヒドの製造法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS59144727A true JPS59144727A (ja) | 1984-08-18 |
| JPS6312455B2 JPS6312455B2 (enrdf_load_stackoverflow) | 1988-03-18 |
Family
ID=11990961
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP58019133A Granted JPS59144727A (ja) | 1983-02-08 | 1983-02-08 | フエニルアセトアルデヒドの製造法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS59144727A (enrdf_load_stackoverflow) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0728837A1 (en) * | 1995-02-23 | 1996-08-28 | Tokuyama Corporation | Amorphous sodium silicate-metal sulfate composite powder |
| WO2010070659A3 (en) * | 2008-11-06 | 2012-08-30 | Shasun Chemicals And Drugs Limited | A novel heterogeneous catalyst for the preparation of arylacetaldehydes |
-
1983
- 1983-02-08 JP JP58019133A patent/JPS59144727A/ja active Granted
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0728837A1 (en) * | 1995-02-23 | 1996-08-28 | Tokuyama Corporation | Amorphous sodium silicate-metal sulfate composite powder |
| US5707960A (en) * | 1995-02-23 | 1998-01-13 | Tokuyama Corporation | Amorphous sodium silicate-metal sulfate composite powder |
| AU689367B2 (en) * | 1995-02-23 | 1998-03-26 | Tokuyama Corporation | Amorphous sodium silicate-metal sulfate composite powder |
| WO2010070659A3 (en) * | 2008-11-06 | 2012-08-30 | Shasun Chemicals And Drugs Limited | A novel heterogeneous catalyst for the preparation of arylacetaldehydes |
Also Published As
| Publication number | Publication date |
|---|---|
| JPS6312455B2 (enrdf_load_stackoverflow) | 1988-03-18 |
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