JPS5885874A - イソシアヌル酸エステルの製造方法 - Google Patents
イソシアヌル酸エステルの製造方法Info
- Publication number
- JPS5885874A JPS5885874A JP57191964A JP19196482A JPS5885874A JP S5885874 A JPS5885874 A JP S5885874A JP 57191964 A JP57191964 A JP 57191964A JP 19196482 A JP19196482 A JP 19196482A JP S5885874 A JPS5885874 A JP S5885874A
- Authority
- JP
- Japan
- Prior art keywords
- carbon atoms
- catalyst
- ester
- group
- reaction
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 238000004519 manufacturing process Methods 0.000 title claims description 4
- ZFSLODLOARCGLH-UHFFFAOYSA-N isocyanuric acid Natural products OC1=NC(O)=NC(O)=N1 ZFSLODLOARCGLH-UHFFFAOYSA-N 0.000 title 1
- -1 isocyanuric acid ester Chemical class 0.000 title 1
- 238000000034 method Methods 0.000 claims description 26
- 239000003054 catalyst Substances 0.000 claims description 25
- 150000002148 esters Chemical class 0.000 claims description 25
- 238000006317 isomerization reaction Methods 0.000 claims description 13
- 239000002904 solvent Substances 0.000 claims description 12
- 239000002253 acid Substances 0.000 claims description 11
- 125000004432 carbon atom Chemical group C* 0.000 claims description 11
- 238000006243 chemical reaction Methods 0.000 claims description 8
- 125000003342 alkenyl group Chemical group 0.000 claims description 7
- 125000000217 alkyl group Chemical group 0.000 claims description 6
- 239000007864 aqueous solution Substances 0.000 claims description 5
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 claims description 5
- 229910052739 hydrogen Inorganic materials 0.000 claims description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 4
- 239000007795 chemical reaction product Substances 0.000 claims description 2
- 239000001257 hydrogen Substances 0.000 claims description 2
- 229910052757 nitrogen Inorganic materials 0.000 claims description 2
- JUJWROOIHBZHMG-UHFFFAOYSA-N Pyridine Chemical group C1=CC=NC=C1 JUJWROOIHBZHMG-UHFFFAOYSA-N 0.000 claims 1
- 125000001797 benzyl group Chemical group [H]C1=C([H])C([H])=C(C([H])=C1[H])C([H])([H])* 0.000 claims 1
- 230000003197 catalytic effect Effects 0.000 claims 1
- 125000004435 hydrogen atom Chemical group [H]* 0.000 claims 1
- 239000000203 mixture Substances 0.000 description 4
- 238000006116 polymerization reaction Methods 0.000 description 4
- 239000007858 starting material Substances 0.000 description 4
- 150000001875 compounds Chemical class 0.000 description 3
- 239000000243 solution Substances 0.000 description 3
- 238000003756 stirring Methods 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- 239000003513 alkali Substances 0.000 description 2
- XXROGKLTLUQVRX-UHFFFAOYSA-N allyl alcohol Chemical compound OCC=C XXROGKLTLUQVRX-UHFFFAOYSA-N 0.000 description 2
- 229910052799 carbon Inorganic materials 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 238000011065 in-situ storage Methods 0.000 description 2
- 239000003112 inhibitor Substances 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 229920000642 polymer Polymers 0.000 description 2
- 239000011541 reaction mixture Substances 0.000 description 2
- 150000003839 salts Chemical class 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 150000005691 triesters Chemical class 0.000 description 2
- 238000005406 washing Methods 0.000 description 2
- 125000006702 (C1-C18) alkyl group Chemical group 0.000 description 1
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
- 101100192880 Neosartorya fumigata (strain ATCC MYA-4609 / Af293 / CBS 101355 / FGSC A1100) pyr7 gene Proteins 0.000 description 1
- BHELZAPQIKSEDF-UHFFFAOYSA-N allyl bromide Chemical compound BrCC=C BHELZAPQIKSEDF-UHFFFAOYSA-N 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 150000001721 carbon Chemical group 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 229910052802 copper Inorganic materials 0.000 description 1
- 239000010949 copper Substances 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000012065 filter cake Substances 0.000 description 1
- 150000004820 halides Chemical class 0.000 description 1
- 229910052736 halogen Inorganic materials 0.000 description 1
- 150000002367 halogens Chemical group 0.000 description 1
- MNWFXJYAOYHMED-UHFFFAOYSA-N heptanoic acid Chemical compound CCCCCCC(O)=O MNWFXJYAOYHMED-UHFFFAOYSA-N 0.000 description 1
- 239000008240 homogeneous mixture Substances 0.000 description 1
- 238000000265 homogenisation Methods 0.000 description 1
- 150000002431 hydrogen Chemical group 0.000 description 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 239000003444 phase transfer catalyst Substances 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 238000007086 side reaction Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000001308 synthesis method Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D251/00—Heterocyclic compounds containing 1,3,5-triazine rings
- C07D251/02—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings
- C07D251/12—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members
- C07D251/26—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members with only hetero atoms directly attached to ring carbon atoms
- C07D251/30—Only oxygen atoms
- C07D251/34—Cyanuric or isocyanuric esters
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Plural Heterocyclic Compounds (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Catalysts (AREA)
- Nitrogen Condensed Heterocyclic Rings (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| NL8104978 | 1981-11-04 | ||
| NL8104978 | 1981-11-04 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS5885874A true JPS5885874A (ja) | 1983-05-23 |
| JPH0465070B2 JPH0465070B2 (en, 2012) | 1992-10-16 |
Family
ID=19838309
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP57191964A Granted JPS5885874A (ja) | 1981-11-04 | 1982-11-02 | イソシアヌル酸エステルの製造方法 |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US4451651A (en, 2012) |
| EP (1) | EP0078567B1 (en, 2012) |
| JP (1) | JPS5885874A (en, 2012) |
| AT (1) | ATE20744T1 (en, 2012) |
| CA (1) | CA1183844A (en, 2012) |
| DE (1) | DE3272037D1 (en, 2012) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2009542755A (ja) * | 2006-07-12 | 2009-12-03 | エボニック デグサ ゲーエムベーハー | トリアリルイソシアヌレート（ｔａｉｃ）の製造方法 |
| EP2270103A2 (en) | 2000-12-27 | 2011-01-05 | Kaneka Corporation | Curing agent, curable compositions, compositions for optical materials, optical materials, their production, and liquid crystal displays and LED's made by using the materials |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102438997B (zh) | 2009-05-25 | 2016-05-04 | 日本化成株式会社 | 异氰尿酸三烯丙酯、氰尿酸三烯丙酯和异氰尿酸三烯丙酯的制造方法 |
| ES2632783T3 (es) | 2014-12-19 | 2017-09-15 | Evonik Degussa Gmbh | Sistemas de redes de cubierta para láminas de encapsulación que comprenden compuestos de bis-(alquenilamidas) |
| EP3034528B1 (de) | 2014-12-19 | 2017-06-21 | Evonik Degussa GmbH | Covernetzersysteme für Verkapselungsfolien umfassend Harnstoffverbindungen |
Family Cites Families (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3088948A (en) * | 1963-05-07 | Production of tris | ||
| US3037979A (en) * | 1962-06-05 | Process for manufacturing iso- | ||
| GB858810A (en) * | 1957-09-09 | 1961-01-18 | Kenichi Fukui | Process for manufacturing cyanuric and isocyanuric acid derivatives |
| FR1402888A (fr) * | 1964-01-24 | 1965-06-18 | Azote Office Nat Ind | nu-dérivés bis- ou tris (carbamyle nu- substitués) de l'acide isocyanurique et leur préparation |
| JPS6030675B2 (ja) * | 1976-01-19 | 1985-07-17 | 花王株式会社 | イソシアヌル酸トリエステルの製造方法 |
| US4326057A (en) * | 1980-12-22 | 1982-04-20 | Monsanto Company | Adducts of acrolein and isocyanuric acid |
-
1982
- 1982-10-25 DE DE8282201326T patent/DE3272037D1/de not_active Expired
- 1982-10-25 AT AT82201326T patent/ATE20744T1/de not_active IP Right Cessation
- 1982-10-25 EP EP82201326A patent/EP0078567B1/en not_active Expired
- 1982-11-02 JP JP57191964A patent/JPS5885874A/ja active Granted
- 1982-11-03 CA CA000414732A patent/CA1183844A/en not_active Expired
- 1982-11-04 US US06/439,140 patent/US4451651A/en not_active Expired - Lifetime
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP2270103A2 (en) | 2000-12-27 | 2011-01-05 | Kaneka Corporation | Curing agent, curable compositions, compositions for optical materials, optical materials, their production, and liquid crystal displays and LED's made by using the materials |
| JP2009542755A (ja) * | 2006-07-12 | 2009-12-03 | エボニック デグサ ゲーエムベーハー | トリアリルイソシアヌレート（ｔａｉｃ）の製造方法 |
Also Published As
| Publication number | Publication date |
|---|---|
| EP0078567B1 (en) | 1986-07-16 |
| CA1183844A (en) | 1985-03-12 |
| ATE20744T1 (de) | 1986-08-15 |
| US4451651A (en) | 1984-05-29 |
| EP0078567A1 (en) | 1983-05-11 |
| JPH0465070B2 (en, 2012) | 1992-10-16 |
| DE3272037D1 (en) | 1986-08-21 |
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