JPS5598176A - Novel phthalide derivative - Google Patents
Novel phthalide derivativeInfo
- Publication number
- JPS5598176A JPS5598176A JP473679A JP473679A JPS5598176A JP S5598176 A JPS5598176 A JP S5598176A JP 473679 A JP473679 A JP 473679A JP 473679 A JP473679 A JP 473679A JP S5598176 A JPS5598176 A JP S5598176A
- Authority
- JP
- Japan
- Prior art keywords
- formula
- derivative
- compound
- diester
- phthalide derivative
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Landscapes
- Furan Compounds (AREA)
Abstract
NEW MATERIAL:A phthalide derivative of formula I (R1, R2, and R3 may be the same or different alkyl groups).
EXAMPLE: 6-Ethoxycarbonyl-5,7-dimethylphthalide.
USE: An intermediate for the synthesis of 2-phenyl-1-phthalazone derivatives having thromboxane biosynthesis inhibitory and antithrombotic actions.
PROCESS: A reactive derivative of the carboxylic acid compound of formula I is reduced with a boron hydride complex, preferably sodium borohydride, in the presence of a dehydrochlorinating agent, e.g. triethylamine, in a solvent, e.g. tetrahydrofuran, to give the compound of formula I. The starting compound of formula II can be obtained by partial hydrolysis of a phthalic diester derivative prepared through the Dieles-Alder reaction of an isodehydroacetate with an acetylenedicarboxylic diester.
COPYRIGHT: (C)1980,JPO&Japio
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP473679A JPS5598176A (en) | 1979-01-22 | 1979-01-22 | Novel phthalide derivative |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP473679A JPS5598176A (en) | 1979-01-22 | 1979-01-22 | Novel phthalide derivative |
Publications (1)
Publication Number | Publication Date |
---|---|
JPS5598176A true JPS5598176A (en) | 1980-07-25 |
Family
ID=11592185
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP473679A Pending JPS5598176A (en) | 1979-01-22 | 1979-01-22 | Novel phthalide derivative |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS5598176A (en) |
-
1979
- 1979-01-22 JP JP473679A patent/JPS5598176A/en active Pending
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