JPS55160796A - Preparation of n6-alkyl cordycepin - Google Patents

Preparation of n6-alkyl cordycepin

Info

Publication number
JPS55160796A
JPS55160796A JP6753879A JP6753879A JPS55160796A JP S55160796 A JPS55160796 A JP S55160796A JP 6753879 A JP6753879 A JP 6753879A JP 6753879 A JP6753879 A JP 6753879A JP S55160796 A JPS55160796 A JP S55160796A
Authority
JP
Japan
Prior art keywords
alkyl
reacting
hydrogen halide
titled compound
cordycepin
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
JP6753879A
Other languages
Japanese (ja)
Other versions
JPS5710119B2 (en
Inventor
Susumu Shibuya
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Yamasa Shoyu KK
Original Assignee
Yamasa Shoyu KK
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Yamasa Shoyu KK filed Critical Yamasa Shoyu KK
Priority to JP6753879A priority Critical patent/JPS55160796A/en
Publication of JPS55160796A publication Critical patent/JPS55160796A/en
Publication of JPS5710119B2 publication Critical patent/JPS5710119B2/ja
Granted legal-status Critical Current

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  • Saccharide Compounds (AREA)

Abstract

PURPOSE: To prepare the titled compound having RNA-synthesis inhibiting activity and resistant to adenosinedeaminase, in high yield, by reacting an N1-alkylcordycepin (a novel compound) or its hydrogen halide salt with an alkali.
CONSTITUTION: The objective titled compound of formula III is prepared by reacting an N1-akylcordycepin of formula I (R is alkyl) or II (X⊖ is halogen anion) or its hydrogen halide alst in a solvent such as alcohol, under alkaline conditions of pH 7.5W14 (e.g. with NaOH) at a temperature between room temperature and 100°C for several minutes to several hours, thereby effecting the rearrangement reaction of the alkyl group from N1 to N6 position.
COPYRIGHT: (C)1980,JPO&Japio
JP6753879A 1979-06-01 1979-06-01 Preparation of n6-alkyl cordycepin Granted JPS55160796A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP6753879A JPS55160796A (en) 1979-06-01 1979-06-01 Preparation of n6-alkyl cordycepin

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP6753879A JPS55160796A (en) 1979-06-01 1979-06-01 Preparation of n6-alkyl cordycepin

Publications (2)

Publication Number Publication Date
JPS55160796A true JPS55160796A (en) 1980-12-13
JPS5710119B2 JPS5710119B2 (en) 1982-02-24

Family

ID=13347845

Family Applications (1)

Application Number Title Priority Date Filing Date
JP6753879A Granted JPS55160796A (en) 1979-06-01 1979-06-01 Preparation of n6-alkyl cordycepin

Country Status (1)

Country Link
JP (1) JPS55160796A (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2006516641A (en) * 2003-02-03 2006-07-06 シーブイ・セラピューティクス・インコーポレイテッド Full and partial agonists of adenosine receptors
CN103214533A (en) * 2013-04-19 2013-07-24 湖南农业大学 Method for continuously preparing cordycepin and cordyceps polysaccharide by using membrane separation technology

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2006516641A (en) * 2003-02-03 2006-07-06 シーブイ・セラピューティクス・インコーポレイテッド Full and partial agonists of adenosine receptors
CN103214533A (en) * 2013-04-19 2013-07-24 湖南农业大学 Method for continuously preparing cordycepin and cordyceps polysaccharide by using membrane separation technology

Also Published As

Publication number Publication date
JPS5710119B2 (en) 1982-02-24

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