New! View global litigation for patent families

JPS5511538A - Production of methoxysilane - Google Patents

Production of methoxysilane

Info

Publication number
JPS5511538A
JPS5511538A JP8434878A JP8434878A JPS5511538A JP S5511538 A JPS5511538 A JP S5511538A JP 8434878 A JP8434878 A JP 8434878A JP 8434878 A JP8434878 A JP 8434878A JP S5511538 A JPS5511538 A JP S5511538A
Authority
JP
Grant status
Application
Patent type
Prior art keywords
methanol
azeotropic
mixture
methoxysilane
distillation
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP8434878A
Other versions
JPS6139955B2 (en )
Inventor
Sunao Imaki
Tetsuyoshi Suzuki
Takahisa Yamaura
Original Assignee
Mitsubishi Chem Ind Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date

Links

Abstract

PURPOSE: A mixture of methoxysilane and unreacted methanol resulting from the reaction between silicon and methanol is subjected to azeotropic distillation to remove rapidly methanol, thus preventing the formation of tetramethoxy silane and producing title compound in high yield.
CONSTITUTION: The reaction between silicon or its compound and methanol in the presence of cuprous chloride is conducted in a solvent as cumene. Then, the unreacted methanol is removed by the azeotropic distillation of the reaction mixture containing methoxysilane and methanol to give title compound. The azeotropic distillation is effected by adding a substance that forms an azeotropic mixture with methanol and gives difference in boiling point between trimethoxysilane and the azeotropic mixture by more than 1°C.
COPYRIGHT: (C)1980,JPO&Japio
JP8434878A 1978-07-11 1978-07-11 Expired JPS6139955B2 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP8434878A JPS6139955B2 (en) 1978-07-11 1978-07-11

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP8434878A JPS6139955B2 (en) 1978-07-11 1978-07-11

Publications (2)

Publication Number Publication Date
JPS5511538A true true JPS5511538A (en) 1980-01-26
JPS6139955B2 JPS6139955B2 (en) 1986-09-06

Family

ID=13828000

Family Applications (1)

Application Number Title Priority Date Filing Date
JP8434878A Expired JPS6139955B2 (en) 1978-07-11 1978-07-11

Country Status (1)

Country Link
JP (1) JPS6139955B2 (en)

Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4487949A (en) * 1983-11-22 1984-12-11 Union Carbide Corporation Process for the preparation of alkyl silicates
US4727173A (en) * 1987-03-31 1988-02-23 Union Carbide Corporation Process for producing trialkoxysilanes from the reaction of silicon metal and alcohol
JPS63156793A (en) * 1986-12-19 1988-06-29 Mitsubishi Kasei Corp Production of alkoxysilanes
JPH02160792A (en) * 1988-12-14 1990-06-20 Shin Etsu Chem Co Ltd Preparation of tetraalkoxysilane
US4999446A (en) * 1990-06-21 1991-03-12 Union Carbide Chemicals And Plastics Company Inc. Trimethoxysilane preparation via the methanol-silicon reaction with recycle
US5084590A (en) * 1991-06-24 1992-01-28 Union Carbide Chemicals & Plastics Technology Corporation Trimethoxysilane preparation via the methanol-silicon reaction using a continuous process and multiple reactors
JPH06115431A (en) * 1992-09-30 1994-04-26 Investigacion Y Accesoramiento Technico Sa Bogie for railway vehicle
JP2008500305A (en) * 2004-05-26 2008-01-10 デグサ ゲーエムベーハーDegussa GmbH Preparation of organosilane ester

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS501692A (en) * 1973-05-07 1975-01-09
JPS5034539A (en) * 1973-07-28 1975-04-02

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS501692A (en) * 1973-05-07 1975-01-09
JPS5034539A (en) * 1973-07-28 1975-04-02

Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4487949A (en) * 1983-11-22 1984-12-11 Union Carbide Corporation Process for the preparation of alkyl silicates
JPH0723383B2 (en) * 1986-12-19 1995-03-15 三菱化学株式会社 Manufacturing method of alkoxysilanes
JPS63156793A (en) * 1986-12-19 1988-06-29 Mitsubishi Kasei Corp Production of alkoxysilanes
US4727173A (en) * 1987-03-31 1988-02-23 Union Carbide Corporation Process for producing trialkoxysilanes from the reaction of silicon metal and alcohol
JPH02160792A (en) * 1988-12-14 1990-06-20 Shin Etsu Chem Co Ltd Preparation of tetraalkoxysilane
US4999446A (en) * 1990-06-21 1991-03-12 Union Carbide Chemicals And Plastics Company Inc. Trimethoxysilane preparation via the methanol-silicon reaction with recycle
US5084590A (en) * 1991-06-24 1992-01-28 Union Carbide Chemicals & Plastics Technology Corporation Trimethoxysilane preparation via the methanol-silicon reaction using a continuous process and multiple reactors
JPH06115431A (en) * 1992-09-30 1994-04-26 Investigacion Y Accesoramiento Technico Sa Bogie for railway vehicle
JP2008500305A (en) * 2004-05-26 2008-01-10 デグサ ゲーエムベーハーDegussa GmbH Preparation of organosilane ester

Also Published As

Publication number Publication date Type
JPS6139955B2 (en) 1986-09-06 grant
JP1454476C (en) grant

Similar Documents

Publication Publication Date Title
JPS57156318A (en) Production of trichlorosilane
JPH01132542A (en) Method for optically resolving gossypol racemic modification
Miller et al. The addition of trimethylsilyl iodide to some α, β-unsaturated ketones
JPH0267230A (en) Purification of organometallic compound
JPS5660447A (en) Forming method of organic photoconductive film
JPS5740420A (en) Preparation of 1,1,3,4,4,6-hexamethyl-1,2,3,4- tetrahydronaphthalene
JPS58198460A (en) Preparation of beta-mercaptopropionic acid
JPH03291247A (en) Production of high-purity metallic alkoxide
JPS5528928A (en) Preparation of methoxysilane
JPS57108094A (en) Preparation of alkoxysilane
JPS5721341A (en) Preparation of substituted acetic ester
JPS588045A (en) Preparation of alpha-phenylpropionic ester
JPH03127795A (en) Production of alkylmetallic compound
JPS56150026A (en) Preparation of methyl chloride
JPS5929633A (en) Method for recovering acetic acid from aqueous solution of acetate
JPS5251331A (en) Process for preparation of unsaturated compounds
JPS56104891A (en) Preparation of (n-aminoethyl)aminoalkylsilane
JPS5884814A (en) Preparation of novolak type phenolic resin
JPS5235192A (en) Process for the production of a catalyst for copolymerization
JPS54128531A (en) Preparation of polyglycidyl compound
JPS5581818A (en) Method of fluorination
JPS527911A (en) Process for preparation of ethers
JPS5610135A (en) Preparation of di-n-propylmalonic acid
JPS6193165A (en) Method of separating and purifying quinaldine
JPS6270326A (en) Production of diarylbutane