JPH0456775B2 - - Google Patents
Info
- Publication number
- JPH0456775B2 JPH0456775B2 JP61205632A JP20563286A JPH0456775B2 JP H0456775 B2 JPH0456775 B2 JP H0456775B2 JP 61205632 A JP61205632 A JP 61205632A JP 20563286 A JP20563286 A JP 20563286A JP H0456775 B2 JPH0456775 B2 JP H0456775B2
- Authority
- JP
- Japan
- Prior art keywords
- silica
- silica sol
- particle size
- silica particles
- particles
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- RMAQACBXLXPBSY-UHFFFAOYSA-N silicic acid Chemical compound O[Si](O)(O)O RMAQACBXLXPBSY-UHFFFAOYSA-N 0.000 claims description 130
- 239000002245 particle Substances 0.000 claims description 112
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 101
- 239000007788 liquid Substances 0.000 claims description 69
- 230000002378 acidificating effect Effects 0.000 claims description 45
- 235000012239 silicon dioxide Nutrition 0.000 claims description 44
- 238000000034 method Methods 0.000 claims description 35
- 229910004298 SiO 2 Inorganic materials 0.000 claims description 24
- 238000004519 manufacturing process Methods 0.000 claims description 16
- 239000002612 dispersion medium Substances 0.000 claims description 15
- 239000000377 silicon dioxide Substances 0.000 claims description 7
- 229910052910 alkali metal silicate Inorganic materials 0.000 claims description 6
- 239000003513 alkali Substances 0.000 claims description 4
- 229910052783 alkali metal Inorganic materials 0.000 claims description 4
- 150000001340 alkali metals Chemical class 0.000 claims description 4
- 239000000203 mixture Substances 0.000 claims description 3
- 239000000243 solution Substances 0.000 description 49
- 238000009826 distribution Methods 0.000 description 19
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 6
- 230000000052 comparative effect Effects 0.000 description 5
- 239000002253 acid Substances 0.000 description 3
- 238000000151 deposition Methods 0.000 description 3
- 239000004033 plastic Substances 0.000 description 3
- 229920003023 plastic Polymers 0.000 description 3
- 239000002994 raw material Substances 0.000 description 3
- NWUYHJFMYQTDRP-UHFFFAOYSA-N 1,2-bis(ethenyl)benzene;1-ethenyl-2-ethylbenzene;styrene Chemical compound C=CC1=CC=CC=C1.CCC1=CC=CC=C1C=C.C=CC1=CC=CC=C1C=C NWUYHJFMYQTDRP-UHFFFAOYSA-N 0.000 description 2
- 239000004115 Sodium Silicate Substances 0.000 description 2
- 239000003729 cation exchange resin Substances 0.000 description 2
- 239000011248 coating agent Substances 0.000 description 2
- 230000008021 deposition Effects 0.000 description 2
- 238000004090 dissolution Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000001704 evaporation Methods 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 230000001788 irregular Effects 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- 239000003960 organic solvent Substances 0.000 description 2
- 230000005070 ripening Effects 0.000 description 2
- 229910052911 sodium silicate Inorganic materials 0.000 description 2
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 description 2
- 238000000108 ultra-filtration Methods 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- 230000032683 aging Effects 0.000 description 1
- 239000012670 alkaline solution Substances 0.000 description 1
- 239000011230 binding agent Substances 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 229910052681 coesite Inorganic materials 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 229910052906 cristobalite Inorganic materials 0.000 description 1
- 238000007865 diluting Methods 0.000 description 1
- 238000000635 electron micrograph Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 238000001879 gelation Methods 0.000 description 1
- 238000010191 image analysis Methods 0.000 description 1
- 229910052914 metal silicate Inorganic materials 0.000 description 1
- 239000011259 mixed solution Substances 0.000 description 1
- 238000010899 nucleation Methods 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 239000012798 spherical particle Substances 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 229910052682 stishovite Inorganic materials 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 239000000758 substrate Substances 0.000 description 1
- 230000008719 thickening Effects 0.000 description 1
- 229910052905 tridymite Inorganic materials 0.000 description 1
Landscapes
- Silicon Compounds (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP20563286A JPS6364911A (ja) | 1986-09-01 | 1986-09-01 | 大粒径のシリカ粒子を含むシリカゾルの製造方法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP20563286A JPS6364911A (ja) | 1986-09-01 | 1986-09-01 | 大粒径のシリカ粒子を含むシリカゾルの製造方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS6364911A JPS6364911A (ja) | 1988-03-23 |
| JPH0456775B2 true JPH0456775B2 (ko) | 1992-09-09 |
Family
ID=16510104
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP20563286A Granted JPS6364911A (ja) | 1986-09-01 | 1986-09-01 | 大粒径のシリカ粒子を含むシリカゾルの製造方法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS6364911A (ko) |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP4493320B2 (ja) | 2002-12-12 | 2010-06-30 | 日揮触媒化成株式会社 | シリカゾルの製造方法およびシリカゾル |
| US20100146864A1 (en) * | 2005-08-10 | 2010-06-17 | Catalysts & Chemicals Industries Co., Ltd | Nodular Silica Sol and Method of Producing the Same |
| JP5089312B2 (ja) * | 2007-09-28 | 2012-12-05 | 日揮触媒化成株式会社 | ハードコート膜付基材およびハードコート膜形成用塗布液 |
| KR101955184B1 (ko) | 2016-03-28 | 2019-03-08 | 주식회사 엘지화학 | 저분진 고단열 에어로겔 블랭킷의 제조방법 |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3440174A (en) * | 1965-04-26 | 1969-04-22 | Nalco Chemical Co | Method of making silica sols containing large particle size silica |
| US3538015A (en) * | 1967-12-07 | 1970-11-03 | Nalco Chemical Co | Large particle silica sols and method of production |
| US3789009A (en) * | 1971-07-15 | 1974-01-29 | Du Pont | Process for the preparation of large particle silica sols |
-
1986
- 1986-09-01 JP JP20563286A patent/JPS6364911A/ja active Granted
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3440174A (en) * | 1965-04-26 | 1969-04-22 | Nalco Chemical Co | Method of making silica sols containing large particle size silica |
| US3538015A (en) * | 1967-12-07 | 1970-11-03 | Nalco Chemical Co | Large particle silica sols and method of production |
| US3789009A (en) * | 1971-07-15 | 1974-01-29 | Du Pont | Process for the preparation of large particle silica sols |
Also Published As
| Publication number | Publication date |
|---|---|
| JPS6364911A (ja) | 1988-03-23 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| JP5334385B2 (ja) | ポリシリケート粒子状材料の製造および使用 | |
| US5221497A (en) | Elongated-shaped silica sol and method for preparing the same | |
| US5066420A (en) | Production of silica colloids | |
| JP2012503586A (ja) | 制御可能な幅広い粒径分布及び最小粒径を有するシリカゾルの製造方法 | |
| JPH0159974B2 (ko) | ||
| JP3584485B2 (ja) | シリカゾルの製造方法 | |
| JPH085657B2 (ja) | シリカゾルとその製法 | |
| CN114956101B (zh) | 一种高分散微米尺寸二氧化硅微球及其制备方法 | |
| US5236623A (en) | Process for the production of a silica colloid | |
| US20070034116A1 (en) | Silica sols with controlled minimum particle size and preparation thereof | |
| JP2001048520A (ja) | 細長い形状のシリカゾル及びその製造方法 | |
| JP4493320B2 (ja) | シリカゾルの製造方法およびシリカゾル | |
| JPH0456775B2 (ko) | ||
| JPH02288B2 (ko) | ||
| US3538015A (en) | Large particle silica sols and method of production | |
| JPH0455125B2 (ko) | ||
| JP3330984B2 (ja) | 単分散球状シリカの製造方法 | |
| JP2000178020A (ja) | 高純度シリカ水性ゾル及びその製造方法 | |
| JPH0455124B2 (ko) | ||
| JP6041668B2 (ja) | シリカ微粒子の製造方法 | |
| JPH02167813A (ja) | コロイダルシリカメタノールゾルの製造方法 | |
| JPS62275005A (ja) | 単分散された粒子の製造方法 | |
| CN112978737A (zh) | 一种粒径均一的纳米氧化硅颗粒的制备方法 | |
| CN115594186B (zh) | 一种小粒径的醇溶剂型硅溶胶的制备方法 | |
| CN112703170A (zh) | 制备可以控制粒度的丝光沸石的方法 |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
| R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
| EXPY | Cancellation because of completion of term |