JPH044260B2 - - Google Patents
Info
- Publication number
- JPH044260B2 JPH044260B2 JP7091784A JP7091784A JPH044260B2 JP H044260 B2 JPH044260 B2 JP H044260B2 JP 7091784 A JP7091784 A JP 7091784A JP 7091784 A JP7091784 A JP 7091784A JP H044260 B2 JPH044260 B2 JP H044260B2
- Authority
- JP
- Japan
- Prior art keywords
- microcrystals
- heat treatment
- fluorine
- fluorine phlogopite
- glass
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 229910052731 fluorine Inorganic materials 0.000 claims description 25
- YCKRFDGAMUMZLT-UHFFFAOYSA-N Fluorine atom Chemical compound [F] YCKRFDGAMUMZLT-UHFFFAOYSA-N 0.000 claims description 23
- 239000011737 fluorine Substances 0.000 claims description 23
- 239000002241 glass-ceramic Substances 0.000 claims description 23
- 238000010438 heat treatment Methods 0.000 claims description 22
- 229910052628 phlogopite Inorganic materials 0.000 claims description 22
- 239000013081 microcrystal Substances 0.000 claims description 17
- 238000004519 manufacturing process Methods 0.000 claims description 9
- 238000006460 hydrolysis reaction Methods 0.000 claims description 8
- 239000000203 mixture Substances 0.000 claims description 7
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 5
- -1 alkoxide compounds Chemical class 0.000 claims description 4
- 238000005245 sintering Methods 0.000 claims description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 4
- 238000001035 drying Methods 0.000 claims description 3
- 150000002222 fluorine compounds Chemical class 0.000 claims description 3
- 239000002798 polar solvent Substances 0.000 claims description 3
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims description 2
- 229910052593 corundum Inorganic materials 0.000 claims description 2
- 230000018044 dehydration Effects 0.000 claims description 2
- 238000006297 dehydration reaction Methods 0.000 claims description 2
- 229910052751 metal Inorganic materials 0.000 claims description 2
- 239000002184 metal Substances 0.000 claims description 2
- 239000007858 starting material Substances 0.000 claims description 2
- 229910001845 yogo sapphire Inorganic materials 0.000 claims description 2
- 229910052681 coesite Inorganic materials 0.000 claims 1
- 229910052906 cristobalite Inorganic materials 0.000 claims 1
- 239000000377 silicon dioxide Substances 0.000 claims 1
- 235000012239 silicon dioxide Nutrition 0.000 claims 1
- 229910052682 stishovite Inorganic materials 0.000 claims 1
- 229910052905 tridymite Inorganic materials 0.000 claims 1
- 239000013078 crystal Substances 0.000 description 14
- 239000011159 matrix material Substances 0.000 description 12
- 239000000047 product Substances 0.000 description 9
- 239000000463 material Substances 0.000 description 8
- 238000000034 method Methods 0.000 description 7
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 6
- 230000007062 hydrolysis Effects 0.000 description 6
- 239000000843 powder Substances 0.000 description 5
- 229910004298 SiO 2 Inorganic materials 0.000 description 4
- 239000012467 final product Substances 0.000 description 4
- 239000011521 glass Substances 0.000 description 4
- 238000002844 melting Methods 0.000 description 4
- 230000008018 melting Effects 0.000 description 4
- 239000000126 substance Substances 0.000 description 4
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
- 150000004703 alkoxides Chemical class 0.000 description 3
- 239000011777 magnesium Substances 0.000 description 3
- 239000010445 mica Substances 0.000 description 3
- 229910052618 mica group Inorganic materials 0.000 description 3
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 2
- KWOLFJPFCHCOCG-UHFFFAOYSA-N Acetophenone Chemical compound CC(=O)C1=CC=CC=C1 KWOLFJPFCHCOCG-UHFFFAOYSA-N 0.000 description 2
- 229910004283 SiO 4 Inorganic materials 0.000 description 2
- 230000002411 adverse Effects 0.000 description 2
- 125000000217 alkyl group Chemical group 0.000 description 2
- 239000011230 binding agent Substances 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 239000006227 byproduct Substances 0.000 description 2
- 230000000052 comparative effect Effects 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 238000007796 conventional method Methods 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- 230000007423 decrease Effects 0.000 description 2
- 238000000635 electron micrograph Methods 0.000 description 2
- 238000010304 firing Methods 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- JBXYCUKPDAAYAS-UHFFFAOYSA-N methanol;trifluoroborane Chemical compound OC.FB(F)F JBXYCUKPDAAYAS-UHFFFAOYSA-N 0.000 description 2
- 239000012454 non-polar solvent Substances 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 150000003839 salts Chemical class 0.000 description 2
- ZWEHNKRNPOVVGH-UHFFFAOYSA-N 2-Butanone Chemical compound CCC(C)=O ZWEHNKRNPOVVGH-UHFFFAOYSA-N 0.000 description 1
- 229910018072 Al 2 O 3 Inorganic materials 0.000 description 1
- 229910019142 PO4 Inorganic materials 0.000 description 1
- BOTDANWDWHJENH-UHFFFAOYSA-N Tetraethyl orthosilicate Chemical compound CCO[Si](OCC)(OCC)OCC BOTDANWDWHJENH-UHFFFAOYSA-N 0.000 description 1
- 238000002441 X-ray diffraction Methods 0.000 description 1
- 150000001298 alcohols Chemical class 0.000 description 1
- SMZOGRDCAXLAAR-UHFFFAOYSA-N aluminium isopropoxide Chemical compound [Al+3].CC(C)[O-].CC(C)[O-].CC(C)[O-] SMZOGRDCAXLAAR-UHFFFAOYSA-N 0.000 description 1
- 238000005452 bending Methods 0.000 description 1
- 239000000919 ceramic Substances 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
- 230000008025 crystallization Effects 0.000 description 1
- 238000005520 cutting process Methods 0.000 description 1
- 238000005553 drilling Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- HHFAWKCIHAUFRX-UHFFFAOYSA-N ethoxide Chemical compound CC[O-] HHFAWKCIHAUFRX-UHFFFAOYSA-N 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 150000002576 ketones Chemical class 0.000 description 1
- CRGZYKWWYNQGEC-UHFFFAOYSA-N magnesium;methanolate Chemical compound [Mg+2].[O-]C.[O-]C CRGZYKWWYNQGEC-UHFFFAOYSA-N 0.000 description 1
- 239000011259 mixed solution Substances 0.000 description 1
- 239000012768 molten material Substances 0.000 description 1
- 238000000465 moulding Methods 0.000 description 1
- 239000010452 phosphate Substances 0.000 description 1
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 description 1
- 229920001296 polysiloxane Polymers 0.000 description 1
- BDAWXSQJJCIFIK-UHFFFAOYSA-N potassium methoxide Chemical compound [K+].[O-]C BDAWXSQJJCIFIK-UHFFFAOYSA-N 0.000 description 1
- 238000010298 pulverizing process Methods 0.000 description 1
- 230000009257 reactivity Effects 0.000 description 1
- 230000035939 shock Effects 0.000 description 1
- 238000007711 solidification Methods 0.000 description 1
- 230000008023 solidification Effects 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- WRECIMRULFAWHA-UHFFFAOYSA-N trimethyl borate Chemical compound COB(OC)OC WRECIMRULFAWHA-UHFFFAOYSA-N 0.000 description 1
Landscapes
- Glass Melting And Manufacturing (AREA)
- Glass Compositions (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP7091784A JPS60215548A (ja) | 1984-04-11 | 1984-04-11 | ガラスセラミツクスの製造法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP7091784A JPS60215548A (ja) | 1984-04-11 | 1984-04-11 | ガラスセラミツクスの製造法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS60215548A JPS60215548A (ja) | 1985-10-28 |
| JPH044260B2 true JPH044260B2 (enExample) | 1992-01-27 |
Family
ID=13445331
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP7091784A Granted JPS60215548A (ja) | 1984-04-11 | 1984-04-11 | ガラスセラミツクスの製造法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS60215548A (enExample) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP4582028B2 (ja) * | 2006-03-13 | 2010-11-17 | 石川県 | 快削性ガラスセラミックスの製造方法 |
| JP2008109018A (ja) * | 2006-10-27 | 2008-05-08 | Kyocera Corp | 配線基板 |
-
1984
- 1984-04-11 JP JP7091784A patent/JPS60215548A/ja active Granted
Also Published As
| Publication number | Publication date |
|---|---|
| JPS60215548A (ja) | 1985-10-28 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| US3006775A (en) | Ceramic material and method of making the same | |
| US3940255A (en) | Process for making cordierite glass-ceramic having nucleating agent and increased percent cordierite crystallinity | |
| US3022179A (en) | Ceramic material and method of making the same | |
| Zhu et al. | Sintering behavior and properties of MgTiO3/CaO-B2O3-SiO2 ceramic composites for LTCC applications | |
| US3883337A (en) | Method of manufacturing a glass object by molding and sintering glass powder | |
| JPS6331422B2 (enExample) | ||
| CN111908797B (zh) | 一种低热膨胀堇青石基微晶玻璃材料及其制备方法 | |
| JPH02149415A (ja) | フッ素雲母の製造方法 | |
| US5132253A (en) | Sol-gel method for making ceramic materials | |
| US4835298A (en) | Method for producing liquid alkoxides of mixed metals | |
| US4777151A (en) | Glass-ceramic product and method of making the same | |
| US5173455A (en) | Low sintering cordierite powder composition | |
| US3365314A (en) | Method of producing articles containing predominantly cordierite, anorthite, spinel and/or forsterite | |
| JPH0269335A (ja) | アルカリ土類金属アルミノホウ酸塩ガラスセラミックおよびその製造方法 | |
| JPS62187139A (ja) | リチウム−アルミニウム−珪酸塩ガラス、ガラスセラミツク粉末およびそれらの製造方法 | |
| JPS636499B2 (enExample) | ||
| US5320792A (en) | Process for the preparation of LAS ceramic sintered bodies | |
| JPH044260B2 (enExample) | ||
| DE69516408T2 (de) | Gesinterde quarzglasprodukte und verfahren zur herstellung | |
| US3325265A (en) | Method of making synthetic mica bodies | |
| Hogan et al. | Gel-derived amorphous cesium-aluminosilicate powders useful for formation of pollucite glass-ceramics | |
| JPS61178425A (ja) | フツ素金雲母セラミツクス焼結体の製造方法 | |
| JP2606851B2 (ja) | ガラスセラミックスの製造方法 | |
| CN120157467B (zh) | 一种堇青石陶瓷材料及其制备方法和应用 | |
| JPH0249259B2 (ja) | Ketsushokagarasutosonoseizohoho |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| EXPY | Cancellation because of completion of term |