JPH0362198B2 - - Google Patents
Info
- Publication number
- JPH0362198B2 JPH0362198B2 JP1617084A JP1617084A JPH0362198B2 JP H0362198 B2 JPH0362198 B2 JP H0362198B2 JP 1617084 A JP1617084 A JP 1617084A JP 1617084 A JP1617084 A JP 1617084A JP H0362198 B2 JPH0362198 B2 JP H0362198B2
- Authority
- JP
- Japan
- Prior art keywords
- pitch
- raw material
- solvent
- quinoline
- insoluble
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 239000002994 raw material Substances 0.000 claims description 34
- SMWDFEZZVXVKRB-UHFFFAOYSA-N Quinoline Chemical compound N1=CC=CC2=CC=CC=C21 SMWDFEZZVXVKRB-UHFFFAOYSA-N 0.000 claims description 32
- 229920000049 Carbon (fiber) Polymers 0.000 claims description 31
- 239000004917 carbon fiber Substances 0.000 claims description 31
- 239000002904 solvent Substances 0.000 claims description 27
- 238000000034 method Methods 0.000 claims description 24
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 claims description 21
- 239000000126 substance Substances 0.000 claims description 20
- 238000006243 chemical reaction Methods 0.000 claims description 19
- 238000000605 extraction Methods 0.000 claims description 18
- CXWXQJXEFPUFDZ-UHFFFAOYSA-N tetralin Chemical compound C1=CC=C2CCCCC2=C1 CXWXQJXEFPUFDZ-UHFFFAOYSA-N 0.000 claims description 17
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 claims description 15
- 238000002303 thermal reforming Methods 0.000 claims description 13
- 238000004821 distillation Methods 0.000 claims description 11
- 238000004519 manufacturing process Methods 0.000 claims description 11
- 238000009835 boiling Methods 0.000 claims description 10
- 239000012046 mixed solvent Substances 0.000 claims description 7
- 230000035484 reaction time Effects 0.000 claims description 6
- 239000006227 byproduct Substances 0.000 claims description 5
- 229910052799 carbon Inorganic materials 0.000 claims description 5
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 4
- 239000007795 chemical reaction product Substances 0.000 claims description 4
- 238000004231 fluid catalytic cracking Methods 0.000 claims description 4
- 239000003208 petroleum Substances 0.000 claims description 4
- 230000015572 biosynthetic process Effects 0.000 claims description 2
- 239000000463 material Substances 0.000 claims description 2
- 238000006011 modification reaction Methods 0.000 claims 1
- 239000004753 textile Substances 0.000 claims 1
- 239000011295 pitch Substances 0.000 description 47
- 239000003921 oil Substances 0.000 description 15
- 239000000835 fiber Substances 0.000 description 13
- 238000009987 spinning Methods 0.000 description 11
- 239000007788 liquid Substances 0.000 description 10
- 239000012530 fluid Substances 0.000 description 8
- 239000000047 product Substances 0.000 description 8
- 239000003054 catalyst Substances 0.000 description 7
- 239000000295 fuel oil Substances 0.000 description 6
- 238000005087 graphitization Methods 0.000 description 6
- 239000007789 gas Substances 0.000 description 5
- 238000000926 separation method Methods 0.000 description 5
- 239000007787 solid Substances 0.000 description 5
- 238000005292 vacuum distillation Methods 0.000 description 5
- 238000003763 carbonization Methods 0.000 description 4
- 238000010438 heat treatment Methods 0.000 description 4
- 239000002243 precursor Substances 0.000 description 4
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
- 230000003197 catalytic effect Effects 0.000 description 3
- 239000010419 fine particle Substances 0.000 description 3
- 230000005484 gravity Effects 0.000 description 3
- 239000002245 particle Substances 0.000 description 3
- 239000012071 phase Substances 0.000 description 3
- 238000004062 sedimentation Methods 0.000 description 3
- 238000000638 solvent extraction Methods 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- WYURNTSHIVDZCO-UHFFFAOYSA-N Tetrahydrofuran Chemical compound C1CCOC1 WYURNTSHIVDZCO-UHFFFAOYSA-N 0.000 description 2
- 125000003118 aryl group Chemical group 0.000 description 2
- 239000012298 atmosphere Substances 0.000 description 2
- 238000004523 catalytic cracking Methods 0.000 description 2
- 229910001873 dinitrogen Inorganic materials 0.000 description 2
- 238000007380 fibre production Methods 0.000 description 2
- 238000001914 filtration Methods 0.000 description 2
- 239000012634 fragment Substances 0.000 description 2
- 229930195733 hydrocarbon Natural products 0.000 description 2
- 150000002430 hydrocarbons Chemical class 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 239000012299 nitrogen atmosphere Substances 0.000 description 2
- 230000003287 optical effect Effects 0.000 description 2
- 239000011368 organic material Substances 0.000 description 2
- 239000003960 organic solvent Substances 0.000 description 2
- 229920002239 polyacrylonitrile Polymers 0.000 description 2
- 238000006068 polycondensation reaction Methods 0.000 description 2
- 239000007858 starting material Substances 0.000 description 2
- 238000005979 thermal decomposition reaction Methods 0.000 description 2
- CTQNGGLPUBDAKN-UHFFFAOYSA-N O-Xylene Chemical compound CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 description 1
- 229920000297 Rayon Polymers 0.000 description 1
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 1
- 229910021536 Zeolite Inorganic materials 0.000 description 1
- 230000032683 aging Effects 0.000 description 1
- 239000011337 anisotropic pitch Substances 0.000 description 1
- 239000012296 anti-solvent Substances 0.000 description 1
- 239000012300 argon atmosphere Substances 0.000 description 1
- 239000003575 carbonaceous material Substances 0.000 description 1
- 229920002678 cellulose Polymers 0.000 description 1
- 239000001913 cellulose Substances 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 239000010779 crude oil Substances 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
- 230000008025 crystallization Effects 0.000 description 1
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 238000010304 firing Methods 0.000 description 1
- 239000000446 fuel Substances 0.000 description 1
- 230000004927 fusion Effects 0.000 description 1
- 239000012770 industrial material Substances 0.000 description 1
- 229920005610 lignin Polymers 0.000 description 1
- 239000004973 liquid crystal related substance Substances 0.000 description 1
- 239000007791 liquid phase Substances 0.000 description 1
- 238000002074 melt spinning Methods 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 150000002739 metals Chemical class 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 229910017464 nitrogen compound Inorganic materials 0.000 description 1
- 150000002830 nitrogen compounds Chemical class 0.000 description 1
- 150000002902 organometallic compounds Chemical class 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 150000002927 oxygen compounds Chemical class 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 230000008092 positive effect Effects 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 239000002964 rayon Substances 0.000 description 1
- 230000009257 reactivity Effects 0.000 description 1
- 238000002407 reforming Methods 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 238000005464 sample preparation method Methods 0.000 description 1
- 239000007790 solid phase Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 229910052717 sulfur Inorganic materials 0.000 description 1
- 239000011593 sulfur Substances 0.000 description 1
- 150000003464 sulfur compounds Chemical class 0.000 description 1
- 229920003002 synthetic resin Polymers 0.000 description 1
- 239000000057 synthetic resin Substances 0.000 description 1
- YLQBMQCUIZJEEH-UHFFFAOYSA-N tetrahydrofuran Natural products C=1C=COC=1 YLQBMQCUIZJEEH-UHFFFAOYSA-N 0.000 description 1
- 238000004804 winding Methods 0.000 description 1
- 239000008096 xylene Substances 0.000 description 1
- 239000010457 zeolite Substances 0.000 description 1
Landscapes
- Working-Up Tar And Pitch (AREA)
- Inorganic Fibers (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP1617084A JPS60163992A (ja) | 1984-02-02 | 1984-02-02 | 炭素繊維用原料ピツチの製造法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP1617084A JPS60163992A (ja) | 1984-02-02 | 1984-02-02 | 炭素繊維用原料ピツチの製造法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS60163992A JPS60163992A (ja) | 1985-08-26 |
| JPH0362198B2 true JPH0362198B2 (es) | 1991-09-25 |
Family
ID=11909032
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP1617084A Granted JPS60163992A (ja) | 1984-02-02 | 1984-02-02 | 炭素繊維用原料ピツチの製造法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS60163992A (es) |
-
1984
- 1984-02-02 JP JP1617084A patent/JPS60163992A/ja active Granted
Also Published As
| Publication number | Publication date |
|---|---|
| JPS60163992A (ja) | 1985-08-26 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| JPH0258317B2 (es) | ||
| JPS621990B2 (es) | ||
| JPH048472B2 (es) | ||
| JPS635433B2 (es) | ||
| JPH0255476B2 (es) | ||
| US4503026A (en) | Spinnable precursors from petroleum pitch, fibers spun therefrom and method of preparation thereof | |
| JPS59216921A (ja) | 炭素繊維の製造方法 | |
| JPH0456077B2 (es) | ||
| US4522701A (en) | Process for preparing an anisotropic aromatic pitch | |
| JPS59196390A (ja) | 炭素繊維用ピツチの製造方法 | |
| JPH0150272B2 (es) | ||
| JPS58196292A (ja) | プリメソフエ−ス炭素質の製造方法 | |
| JPH0362198B2 (es) | ||
| JPH0260712B2 (es) | ||
| JPH0475273B2 (es) | ||
| JPH01247487A (ja) | メソフェースピッチの製造方法 | |
| US5540905A (en) | Optically anisotropic pitch for manufacturing high compressive strength carbon fibers and method of manufacturing high compressive strength carbon fibers | |
| JPS61287961A (ja) | 炭素繊維用前駆体ピツチ | |
| JPS59189188A (ja) | 高強度、高弾性率炭素繊維用原料ピツチの製造方法 | |
| JPH0150271B2 (es) | ||
| JPH0455237B2 (es) | ||
| JPS58145782A (ja) | ピツチの製造法 | |
| JPH0324516B2 (es) | ||
| JPS5947426A (ja) | 高弾性炭素繊維の製造法 | |
| JP3016089B2 (ja) | 超低軟化点、低粘度のメソフェーズピッチ及びその製造方法並びに高強度、高弾性率炭素繊維の製造方法 |