JPH0256408B2 - - Google Patents
Info
- Publication number
- JPH0256408B2 JPH0256408B2 JP708683A JP708683A JPH0256408B2 JP H0256408 B2 JPH0256408 B2 JP H0256408B2 JP 708683 A JP708683 A JP 708683A JP 708683 A JP708683 A JP 708683A JP H0256408 B2 JPH0256408 B2 JP H0256408B2
- Authority
- JP
- Japan
- Prior art keywords
- chamber
- reduction
- mgcl
- lid
- metal
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 238000006722 reduction reaction Methods 0.000 claims description 70
- 230000009467 reduction Effects 0.000 claims description 69
- 238000001704 evaporation Methods 0.000 claims description 59
- 230000008020 evaporation Effects 0.000 claims description 58
- 238000001816 cooling Methods 0.000 claims description 39
- 238000009833 condensation Methods 0.000 claims description 35
- 230000005494 condensation Effects 0.000 claims description 35
- 229910052751 metal Inorganic materials 0.000 claims description 28
- 239000002184 metal Substances 0.000 claims description 28
- 238000010438 heat treatment Methods 0.000 claims description 22
- 229910001510 metal chloride Inorganic materials 0.000 claims description 13
- 238000006243 chemical reaction Methods 0.000 claims description 11
- 238000000746 purification Methods 0.000 claims description 11
- 239000006227 byproduct Substances 0.000 claims description 10
- TWRXJAOTZQYOKJ-UHFFFAOYSA-L Magnesium chloride Chemical compound [Mg+2].[Cl-].[Cl-] TWRXJAOTZQYOKJ-UHFFFAOYSA-L 0.000 claims description 8
- 238000007670 refining Methods 0.000 claims description 5
- 239000007791 liquid phase Substances 0.000 claims description 4
- 229910001629 magnesium chloride Inorganic materials 0.000 claims description 4
- 239000007790 solid phase Substances 0.000 claims description 3
- 230000008016 vaporization Effects 0.000 claims description 3
- 230000008018 melting Effects 0.000 claims 1
- 238000002844 melting Methods 0.000 claims 1
- 239000002244 precipitate Substances 0.000 claims 1
- 230000001376 precipitating effect Effects 0.000 claims 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 16
- 238000011946 reduction process Methods 0.000 description 15
- 239000007789 gas Substances 0.000 description 12
- 238000000034 method Methods 0.000 description 12
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 7
- 150000002739 metals Chemical class 0.000 description 7
- 230000008569 process Effects 0.000 description 7
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 6
- 239000000567 combustion gas Substances 0.000 description 6
- 238000000926 separation method Methods 0.000 description 6
- 238000005192 partition Methods 0.000 description 4
- 238000010276 construction Methods 0.000 description 3
- 230000007423 decrease Effects 0.000 description 3
- 238000007599 discharging Methods 0.000 description 3
- 229910052742 iron Inorganic materials 0.000 description 3
- 230000007246 mechanism Effects 0.000 description 3
- 239000000155 melt Substances 0.000 description 3
- 238000003303 reheating Methods 0.000 description 3
- 229910001220 stainless steel Inorganic materials 0.000 description 3
- 239000010935 stainless steel Substances 0.000 description 3
- 238000005292 vacuum distillation Methods 0.000 description 3
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 description 2
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 2
- 229910000831 Steel Inorganic materials 0.000 description 2
- 239000012300 argon atmosphere Substances 0.000 description 2
- 239000012298 atmosphere Substances 0.000 description 2
- 150000001805 chlorine compounds Chemical class 0.000 description 2
- 238000004821 distillation Methods 0.000 description 2
- 238000002347 injection Methods 0.000 description 2
- 239000007924 injection Substances 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 239000012071 phase Substances 0.000 description 2
- 238000012545 processing Methods 0.000 description 2
- 239000010959 steel Substances 0.000 description 2
- 229910052719 titanium Inorganic materials 0.000 description 2
- 238000012546 transfer Methods 0.000 description 2
- 229910052726 zirconium Inorganic materials 0.000 description 2
- KPZGRMZPZLOPBS-UHFFFAOYSA-N 1,3-dichloro-2,2-bis(chloromethyl)propane Chemical compound ClCC(CCl)(CCl)CCl KPZGRMZPZLOPBS-UHFFFAOYSA-N 0.000 description 1
- 229910007926 ZrCl Inorganic materials 0.000 description 1
- 229910052786 argon Inorganic materials 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 239000000498 cooling water Substances 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 238000005485 electric heating Methods 0.000 description 1
- 238000005265 energy consumption Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 238000011049 filling Methods 0.000 description 1
- 229910052735 hafnium Inorganic materials 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 238000009776 industrial production Methods 0.000 description 1
- 239000011261 inert gas Substances 0.000 description 1
- 239000011810 insulating material Substances 0.000 description 1
- 238000009413 insulation Methods 0.000 description 1
- OHZZTXYKLXZFSZ-UHFFFAOYSA-I manganese(3+) 5,10,15-tris(1-methylpyridin-1-ium-4-yl)-20-(1-methylpyridin-4-ylidene)porphyrin-22-ide pentachloride Chemical compound [Cl-].[Cl-].[Cl-].[Cl-].[Cl-].[Mn+3].C1=CN(C)C=CC1=C1C(C=C2)=NC2=C(C=2C=C[N+](C)=CC=2)C([N-]2)=CC=C2C(C=2C=C[N+](C)=CC=2)=C(C=C2)N=C2C(C=2C=C[N+](C)=CC=2)=C2N=C1C=C2 OHZZTXYKLXZFSZ-UHFFFAOYSA-I 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000001465 metallisation Methods 0.000 description 1
- 239000012768 molten material Substances 0.000 description 1
- 229910052758 niobium Inorganic materials 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000007711 solidification Methods 0.000 description 1
- 230000008023 solidification Effects 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 230000007704 transition Effects 0.000 description 1
- 238000009736 wetting Methods 0.000 description 1
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP708683A JPS59133335A (ja) | 1983-01-18 | 1983-01-18 | 金属塩化物の還元精製装置 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP708683A JPS59133335A (ja) | 1983-01-18 | 1983-01-18 | 金属塩化物の還元精製装置 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS59133335A JPS59133335A (ja) | 1984-07-31 |
| JPH0256408B2 true JPH0256408B2 (zh) | 1990-11-30 |
Family
ID=11656275
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP708683A Granted JPS59133335A (ja) | 1983-01-18 | 1983-01-18 | 金属塩化物の還元精製装置 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS59133335A (zh) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2761485B2 (ja) * | 1989-10-26 | 1998-06-04 | 株式会社住友シチックス尼崎 | 高融点高靭性金属の製造装置および製造方法 |
| CN101812601B (zh) * | 2010-04-13 | 2011-08-31 | 洛阳双瑞万基钛业有限公司 | 一种用于海绵钛生产的防堵管加热装置 |
| CN104711425A (zh) * | 2013-12-12 | 2015-06-17 | 贵阳铝镁设计研究院有限公司 | 一种海绵钛、海绵锆还原蒸馏设备 |
-
1983
- 1983-01-18 JP JP708683A patent/JPS59133335A/ja active Granted
Also Published As
| Publication number | Publication date |
|---|---|
| JPS59133335A (ja) | 1984-07-31 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| US6824585B2 (en) | Low cost high speed titanium and its alloy production | |
| US4565354A (en) | Apparatus for producing purified refractory metal from a chloride thereof | |
| JPH059497B2 (zh) | ||
| US2337042A (en) | Apparatus and method for manufacture of magnesium metal | |
| JPH0256408B2 (zh) | ||
| JPH0255490B2 (zh) | ||
| JPS6112838A (ja) | スポンジチタン製造装置 | |
| EP0091414B1 (en) | Apparatus and method for production of refractory metal from a chloride thereof | |
| JPS591646A (ja) | 金属Ｔｉの製造方法 | |
| RU2205241C1 (ru) | Способ получения кальция и устройство для его осуществления (варианты) | |
| JPS6112837A (ja) | 金属チタンの製造法 | |
| JPS59226127A (ja) | 高融点高靭性金属の製造装置 | |
| JPS5934218B2 (ja) | 金属チタニウム製造装置 | |
| JPS6137338B2 (zh) | ||
| JPH0445571B2 (zh) | ||
| JPS6144124B2 (zh) | ||
| JP3515541B2 (ja) | スポンジチタン製造装置 | |
| JPS58189340A (ja) | 金属塩化物から金属を得る方法 | |
| JPS6112836A (ja) | スポンジチタンの製造法 | |
| RU2261286C2 (ru) | Магниетермический способ получения губчатого циркония и устройство для его осуществления | |
| JPS6137339B2 (zh) | ||
| JPS5817245B2 (ja) | 蒸留亜鉛精製装置 | |
| JPS6131168B2 (zh) | ||
| JPS6131167B2 (zh) | ||
| JPS61217539A (ja) | 耐火金属からＭｇ及びＭｇＣｌ↓２を分離する方法及びそのための装置 |