JPH0231758B2 - - Google Patents
Info
- Publication number
- JPH0231758B2 JPH0231758B2 JP60121045A JP12104585A JPH0231758B2 JP H0231758 B2 JPH0231758 B2 JP H0231758B2 JP 60121045 A JP60121045 A JP 60121045A JP 12104585 A JP12104585 A JP 12104585A JP H0231758 B2 JPH0231758 B2 JP H0231758B2
- Authority
- JP
- Japan
- Prior art keywords
- weight
- diglyceride
- oil
- fat
- aqueous solution
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 claims description 39
- 239000003921 oil Substances 0.000 claims description 33
- 239000003925 fat Substances 0.000 claims description 28
- 238000000034 method Methods 0.000 claims description 18
- 239000002904 solvent Substances 0.000 claims description 18
- 238000007127 saponification reaction Methods 0.000 claims description 14
- 239000002253 acid Substances 0.000 claims description 12
- 239000007864 aqueous solution Substances 0.000 claims description 12
- 239000003513 alkali Substances 0.000 claims description 10
- 235000021588 free fatty acids Nutrition 0.000 claims description 9
- 238000006386 neutralization reaction Methods 0.000 claims description 9
- 239000002798 polar solvent Substances 0.000 claims description 9
- 239000000243 solution Substances 0.000 claims description 9
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims description 4
- IMNFDUFMRHMDMM-UHFFFAOYSA-N N-Heptane Chemical compound CCCCCCC IMNFDUFMRHMDMM-UHFFFAOYSA-N 0.000 claims description 4
- BKIMMITUMNQMOS-UHFFFAOYSA-N nonane Chemical compound CCCCCCCCC BKIMMITUMNQMOS-UHFFFAOYSA-N 0.000 claims description 4
- TVMXDCGIABBOFY-UHFFFAOYSA-N octane Chemical compound CCCCCCCC TVMXDCGIABBOFY-UHFFFAOYSA-N 0.000 claims description 2
- 239000003208 petroleum Substances 0.000 claims description 2
- 150000002430 hydrocarbons Chemical class 0.000 claims 1
- 239000012046 mixed solvent Substances 0.000 claims 1
- 235000019198 oils Nutrition 0.000 description 28
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 24
- 235000019197 fats Nutrition 0.000 description 23
- 238000005194 fractionation Methods 0.000 description 10
- 235000011121 sodium hydroxide Nutrition 0.000 description 8
- DCXXMTOCNZCJGO-UHFFFAOYSA-N tristearoylglycerol Chemical compound CCCCCCCCCCCCCCCCCC(=O)OCC(OC(=O)CCCCCCCCCCCCCCCCC)COC(=O)CCCCCCCCCCCCCCCCC DCXXMTOCNZCJGO-UHFFFAOYSA-N 0.000 description 8
- 235000014121 butter Nutrition 0.000 description 7
- 239000000203 mixture Substances 0.000 description 7
- 239000002994 raw material Substances 0.000 description 7
- 238000002844 melting Methods 0.000 description 6
- 238000003756 stirring Methods 0.000 description 6
- 238000011282 treatment Methods 0.000 description 6
- 230000000052 comparative effect Effects 0.000 description 5
- 239000013078 crystal Substances 0.000 description 5
- 230000008018 melting Effects 0.000 description 5
- 238000004458 analytical method Methods 0.000 description 4
- 230000000694 effects Effects 0.000 description 4
- 239000012535 impurity Substances 0.000 description 4
- 238000004809 thin layer chromatography Methods 0.000 description 4
- UFTFJSFQGQCHQW-UHFFFAOYSA-N triformin Chemical compound O=COCC(OC=O)COC=O UFTFJSFQGQCHQW-UHFFFAOYSA-N 0.000 description 4
- ZCYVEMRRCGMTRW-UHFFFAOYSA-N 7553-56-2 Chemical compound [I] ZCYVEMRRCGMTRW-UHFFFAOYSA-N 0.000 description 3
- 241000282693 Cercopithecidae Species 0.000 description 3
- 244000299461 Theobroma cacao Species 0.000 description 3
- 235000005764 Theobroma cacao ssp. cacao Nutrition 0.000 description 3
- 235000005767 Theobroma cacao ssp. sphaerocarpum Nutrition 0.000 description 3
- 230000002411 adverse Effects 0.000 description 3
- 235000001046 cacaotero Nutrition 0.000 description 3
- 238000000354 decomposition reaction Methods 0.000 description 3
- 210000002683 foot Anatomy 0.000 description 3
- 229910052740 iodine Inorganic materials 0.000 description 3
- 239000011630 iodine Substances 0.000 description 3
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 2
- 241001465754 Metazoa Species 0.000 description 2
- 239000003463 adsorbent Substances 0.000 description 2
- 239000010775 animal oil Substances 0.000 description 2
- 238000005119 centrifugation Methods 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 230000007423 decrease Effects 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 239000011259 mixed solution Substances 0.000 description 2
- 235000014593 oils and fats Nutrition 0.000 description 2
- 230000000704 physical effect Effects 0.000 description 2
- 238000010992 reflux Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 150000003626 triacylglycerols Chemical class 0.000 description 2
- 235000015112 vegetable and seed oil Nutrition 0.000 description 2
- 239000008158 vegetable oil Substances 0.000 description 2
- VZSRBBMJRBPUNF-UHFFFAOYSA-N 2-(2,3-dihydro-1H-inden-2-ylamino)-N-[3-oxo-3-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)propyl]pyrimidine-5-carboxamide Chemical group C1C(CC2=CC=CC=C12)NC1=NC=C(C=N1)C(=O)NCCC(N1CC2=C(CC1)NN=N2)=O VZSRBBMJRBPUNF-UHFFFAOYSA-N 0.000 description 1
- 235000019482 Palm oil Nutrition 0.000 description 1
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 1
- 239000012670 alkaline solution Substances 0.000 description 1
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 238000004042 decolorization Methods 0.000 description 1
- 238000004332 deodorization Methods 0.000 description 1
- 238000003795 desorption Methods 0.000 description 1
- 230000006866 deterioration Effects 0.000 description 1
- 230000002542 deteriorative effect Effects 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 238000011049 filling Methods 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 238000004128 high performance liquid chromatography Methods 0.000 description 1
- 230000007062 hydrolysis Effects 0.000 description 1
- 238000006460 hydrolysis reaction Methods 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 150000002632 lipids Chemical class 0.000 description 1
- 239000002540 palm oil Substances 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 230000009257 reactivity Effects 0.000 description 1
- 238000007670 refining Methods 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 239000000741 silica gel Substances 0.000 description 1
- 229910002027 silica gel Inorganic materials 0.000 description 1
- 238000001179 sorption measurement Methods 0.000 description 1
- 238000005496 tempering Methods 0.000 description 1
Landscapes
- Fats And Perfumes (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP12104585A JPS61278595A (ja) | 1985-06-03 | 1985-06-03 | 油脂中のジグリセリド成分除去法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP12104585A JPS61278595A (ja) | 1985-06-03 | 1985-06-03 | 油脂中のジグリセリド成分除去法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS61278595A JPS61278595A (ja) | 1986-12-09 |
| JPH0231758B2 true JPH0231758B2 (es) | 1990-07-16 |
Family
ID=14801458
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP12104585A Granted JPS61278595A (ja) | 1985-06-03 | 1985-06-03 | 油脂中のジグリセリド成分除去法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS61278595A (es) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPWO2010110232A1 (ja) * | 2009-03-26 | 2012-09-27 | 不二製油株式会社 | チョコレート添加剤及びその製造方法 |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPWO2011055732A1 (ja) * | 2009-11-06 | 2013-03-28 | 不二製油株式会社 | グリセリド油脂中のクロロプロパノール類及びその形成物質を低減する方法 |
-
1985
- 1985-06-03 JP JP12104585A patent/JPS61278595A/ja active Granted
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPWO2010110232A1 (ja) * | 2009-03-26 | 2012-09-27 | 不二製油株式会社 | チョコレート添加剤及びその製造方法 |
Also Published As
| Publication number | Publication date |
|---|---|
| JPS61278595A (ja) | 1986-12-09 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| JP6698704B2 (ja) | 塩基性第四級アンモニウム塩処理を含む、グリセリド油精製法 | |
| US5225580A (en) | Process for separating fatty acids and triglycerides | |
| MXPA06005533A (es) | Proceso para la preparacion de una composicion que comprende compuestos insaturados. | |
| NZ532126A (en) | Chemical process for the production of 1,3-Diglyceride oils | |
| AU2002334783A1 (en) | Chemical process for the production of 1,3-diglyceride oils | |
| WO2019087894A1 (ja) | 飽和炭化水素の含量の低減方法及び精製パーム系油脂 | |
| JPH0633086A (ja) | 吸着法により油脂材料から硫黄化合物を除去する方法 | |
| JP6581715B2 (ja) | 精製パーム系油脂の製造方法、並びに、精製パーム系油脂中のグリシドール、３−クロロプロパン−１，２−ジオール、及びこれらの脂肪酸エステル、及び／又はジグリセリドの低減方法 | |
| CN114144506A (zh) | 精制油脂的制造方法 | |
| JP2583660B2 (ja) | パーム油の精製分別方法 | |
| WO2011138957A1 (ja) | 食用油脂の精製方法 | |
| JP2005530018A (ja) | 植物油の精製の副生物から植物ステロールを回収する方法 | |
| EP0079799B1 (en) | Fat refining | |
| JP6396399B2 (ja) | 飽和炭化水素含有量が低減されたパーム油 | |
| JPH0231758B2 (es) | ||
| JPS62209029A (ja) | ヘキサメチルテトラコサン類の製造法 | |
| WO2014109313A1 (ja) | 油脂の製造方法 | |
| JP6832317B2 (ja) | 飽和炭化水素含有量が低減されたパーム油 | |
| JP2004298041A (ja) | チョコレート及びハードバターの製造方法 | |
| GB2578478A (en) | Chloropropanol removal process | |
| JP2014530258A (ja) | トリアシルグリセロール油製造方法 | |
| WO1982001720A1 (en) | Fat refining | |
| JP6652588B2 (ja) | トリグリセリド油から脂肪酸を抽出する方法 | |
| JP3656863B2 (ja) | 高度不飽和脂肪酸残基含量の高い油脂の製造方法 | |
| GB2144143A (en) | Refining of palm oils |