JPH02270975A - 表面処理鋼板用防錆油組成物 - Google Patents

表面処理鋼板用防錆油組成物

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Publication number
JPH02270975A
JPH02270975A JP1084262A JP8426289A JPH02270975A JP H02270975 A JPH02270975 A JP H02270975A JP 1084262 A JP1084262 A JP 1084262A JP 8426289 A JP8426289 A JP 8426289A JP H02270975 A JPH02270975 A JP H02270975A
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JP
Japan
Prior art keywords
oil
weight
parts
treated steel
rust
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
JP1084262A
Other languages
English (en)
Other versions
JP2764300B2 (ja
Inventor
Yukio Matsuzaki
松崎　幸雄
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Eneos Corp
Original Assignee
Nippon Oil Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Nippon Oil Corp filed Critical Nippon Oil Corp
Priority to JP1084262A priority Critical patent/JP2764300B2/ja
Priority to US07/577,011 priority patent/US5104558A/en
Publication of JPH02270975A publication Critical patent/JPH02270975A/ja
Application granted granted Critical
Publication of JP2764300B2 publication Critical patent/JP2764300B2/ja
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

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    • C10M2229/00—Organic macromolecular compounds containing atoms of elements not provided for in groups C10M2205/00, C10M2209/00, C10M2213/00, C10M2217/00, C10M2221/00 or C10M2225/00 as ingredients in lubricant compositions
    • C10M2229/04—Siloxanes with specific structure
    • C10M2229/05—Siloxanes with specific structure containing atoms other than silicon, hydrogen, oxygen or carbon
    • C10M2229/054—Siloxanes with specific structure containing atoms other than silicon, hydrogen, oxygen or carbon containing phosphorus
    • C10M2229/0545—Siloxanes with specific structure containing atoms other than silicon, hydrogen, oxygen or carbon containing phosphorus used as base material
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
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    • C—CHEMISTRY; METALLURGY
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    • C—CHEMISTRY; METALLURGY
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    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
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    • C—CHEMISTRY; METALLURGY
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    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2020/00—Specified physical or chemical properties or characteristics, i.e. function, of component of lubricating compositions
    • C10N2020/01—Physico-chemical properties
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    • C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/12—Inhibition of corrosion, e.g. anti-rust agents or anti-corrosives
    • C—CHEMISTRY; METALLURGY
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    • C—CHEMISTRY; METALLURGY
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Abstract

(57)【要約】本公報は電子出願前の出願データであるた
め要約のデータは記録されません。

Description

【発明の詳細な説明】 産業上の利用分野 本発明は亜鉛メッキ鋼板のような表面処理鋼板に用いら
れる、プレス、板金、引き抜き等の加工の際に問題とな
るフレーキング、ゴーリン、グ等の表面損傷を効果的に
防止しかつ防錆性に優れた表面処理鋼板用防錆油組成物
に関するものである。
従来の技術および 発明が解決しようとする課題 鋼板の表面上に、亜鉛、鉛、錫、クロム、ニッケル、ア
ルミニウムおよびこれらの合金などをメッキしたいわゆ
る表面処理鋼板は、その耐食性が表面処理を行っていな
い鋼板に比べて著しく向上するため、近年需要が増加し
ている。これら表面処理鋼板は、一般に成形加工され、
塗装されて最終製品となるが、この成形加工とはプレス
加工、板金加工、引き抜き加工等であり、この加工時に
パウダリング、フレーキング、ゴーリング等の表面Ｉｊ
ｉ傷の問題が生ずる。
表面処理鋼板の成形加工時に生ずる表面損傷の問題につ
いては、例えば日本塑性加工学界誌、第２４巻第２７５
号、１２４８〜１２５０ページ（１９８３年）、塑性と
加工　第２６巻第２９１号４１６〜４２３ページ（１９
８５年）に説明されている。これらの文献から明らかな
ようにメッキ層の表面損傷はパウダリング（粉化）、フ
レーキング（はくり）、ゴーリング（かじり）の三種に
大別できる。
パウダリングとは加工時にメッキ層が粉化し１、表面か
ら脱離する現象であり、フレーキングとはメッキ層が加
工時に巨視的薄片となって脱離する現象、またゴーリン
グとは工具表面に付着堆積した破片がメッキ層を掘り起
こしてクラックを生じさせる現象である。これらのうち
、パウダリングは表面メッキ層の延性が母材に比べ小さ
いため、母材の変形に追従できずに発生するものであり
、潤滑材でこれを減少させること困難である。しかし、
ゴーリング、フレーキングは潤滑油を用いて低減できる
ことは経験的に良く知られている。このような表面損傷
は表面処理鋼板の本来の性能である耐食性を著しく低下
させるのみならず、製品表面に修復困難な傷痕を残し、
さら塗装性をも劣化させるなど、完成品の商品価値を大
きく引き下げる原因となる。このような加工時の表面損
傷を防止するために、表面処理鋼板の加工業者は、加工
に先立って潤滑性に富む高粘度の潤滑油を塗油し、しか
るのち所定の加工処理を施すことが多い。
しかし、この塗油作業は煩雑であり、さらに加工後の脱
脂性が困難であるという問題がある。また、特開昭６１
−２６６９５号公報に開示されているように、表面処理
鋼板製造工場で出荷前に塗布される防錆油にワックスを
配合し、ワックス被膜の持つ特性で加工時の表面損傷を
防止することも可能であるが、ワックス皮膜は脱脂が極
度に困難である。さらに、表面処理鋼板の表面を薄い有
機ポリマー皮膜で被覆して加工時の表面損傷を防止した
ポリマー被覆鋼板は、すでに実用化されているが、コス
トが高いという欠点がある。
本発明者らはこれらの従来技術の持つ欠点を解決すべく
研究を重ねた結果、特定の組成を有する防錆油が、フレ
ーキング、ゴーリング等の表面損傷の防止に優れ、かつ
、防錆性も優れていることを見出し、本発明を完成する
に至った。
本発明は、表面処理鋼板製造工場で出荷前に塗布するこ
とにより、出荷時から使用時までの期間の発錆を完全に
防止し、かつ、その表面処理鋼板をそのまま成形加工し
た際にメッキ層の表面損傷を完全に防止し、さらに加工
後の脱脂もきわめて、　容易な表面処理鋼板用防錆油組
成物を提供することを目的とする。
課題を解決するための手段 本発明は、 ４０℃での動粘度が５〜５０ｃＳｔである鉱油および／
または合成油を基油とし、該基油１００重量部に対して （Ａ＞硫化エステル　２〜１５重量部 および （Ｂ）金属石けん　　２〜１５重量部 を必須の成分として配合してなる表面処理鋼板用防錆油
組成物を提供するものである。
また本発明は、 ４０℃での動粘度が５〜５０ｃＳｔである鉱油および／
または合成油を基油とし、該基油１００重二部に対して （Ａ、　）硫化エステル　　　２〜１５重量部および （Ｂ）金属スルホネート　２〜１５ｆｆｌ量部を必須の
成分として配合してなる表面処理鋼板用防錆油組成物を
提供してなるものである。
さらに本発明は、 ４０℃での動粘度が５〜５０ｃＳｔである鉱油および／
または合成油を基油とし、該基油１００重量部に対して （Ａ）硫化エステル　　　２〜１５重量部（Ｂ）金属石
けん　　　　２〜１５重量部および （Ｃ）金属スルホネート　２〜１５重量部を必須の成分
として配合してなる表面処理鋼板用防錆油組成物を提供
するものである。
以ド、本発明の内容をより詳細に説明する。
本発明における鉱油とは、減圧蒸留、溶剤脱れき、溶剤
抽出、水素化分解、溶剤脱ろう、水素化脱ろう、硫酸洗
浄、白土精製、水素化精製等、適宜組み合わせて精製し
たものであり、具体的には例えば、７０ベール油、ＳＡ
Ｅ　１０．５ＡＥ２０．５ＡＥ３０．５ＡＥ４０．５Ａ
Ｅ５０、ブライトストックなど、各種の油が挙げられる
。また、合成油としては、具体的には例えば、ポリブテ
ン、α−オレフィンオリゴマー、アルキルベンゼン、ア
ルキルナフタレン、ジエステル、ポリオールエステル、
ポリグリコール、ポリフェニルエーテル、トリクレジル
ホスフェート、シリコーン油、パーフルオロアルキルエ
ーテル、ノルマルパラフィン、イソパラフィンなど、各
種の油が挙げられる。
本発明の基油である、４０℃における動粘度が５〜５０
ｃＳｔである鉱油および／または合成油とは、上記のよ
うな鉱油、合成油を単独で、あるいは混合したもので、
４０℃における動粘度が５〜５０ｃＳｔ、好ましくは５
〜２０ｃＳｔのものをいう。５ｃＳｔ未満の場合は、鋼
板に塗布して長期間保管した場合、蒸発揮散するために
防錆性、表面損傷防止性が著しく低下し、また、５０ｃ
Ｓｔを超える場合には、成形加工後の脱脂性が悪いため
、それぞれ好ましくない。
本発明における硫化エステルは、通常、１分子中に１個
以上の不飽和結合を有するカルボン酸エステルと、硫黄
、−塩化硫黄、二塩化硫黄、メルカプタン類などの硫黄
化合物とを高温で反応させて得られる。
ここでいうカルボン酸エステルとしては、炭素数３〜２
０の不飽和酸、例えばアクリル酸、プロピオル酸、メタ
クリル酸、クロトン酸、イソクロトン酸、オレイン酸、
エライジン酸、リシノール酸、リノール酸、リルン酸な
どの不飽和酸の炭素数１〜２０のアルキルエステル、例
えば、メチル、エチル、プロピル、ブチル、ペンチル、
ヘキシル、ヘプチル、オクチル、ノニル、デシル、ウン
デシル、ドデシル、トリデシル、テトラデシル、ペンタ
デシル、ヘキサデシル、ヘプタデシル、オクタデシル、
ノナデシル、エイコシルなどのエステルが好ましく用い
られる。また、魚油、牛脂、豚脂、まっこう鯨油、トー
ル油、亜麻仁油、オリーブ池、大豆油、なたね油、ひま
し油、落下主油、米ぬか油などの動物油脂あるいは植物
油脂も好ましく用いられる。これらの不飽和カルボン酸
エステルと、硫黄、−塩化硫黄、二塩化硫黄、メルカプ
タン類などの硫黄化合物とを高温で反応させて硫化エス
テルが得られる。この硫化エステルの製法の詳細は、例
えば、特開昭５９−１５９８９６号公報に記載されてい
る。
この硫化エステルの配合量は、基油１００重量部に対し
、２〜１５重量部、好ましくは５〜１０重量部である。
配合量が２重量部未満の場合には効果が不十分であり、
１５重量部を超える場合には添加量に見合った効果がな
く、経済的に好ましくない。
本発明の組成物は、基油に前記の硫化エステルを配合し
、さらに金属石けんおよび金属スルホネートのうちいず
れか一方または両方を配合することを特徴とする。
この金属石けんとは、バルミチン酸、ステアリン酸、オ
レイン酸などの脂肪酸、ナフテン酸、樹脂酸、ラノリン
脂肪酸、酸化パラフィン、アルケニルコハク酸、アミノ
酸等の金属塩である。この金属としては、リチウム、ナ
トリウム、カリウムなどのアルカリ金属、マグネシウム
、カルシウム、バリウムなどのアルカリ土類金属、その
他、アルミニウム、亜鉛、鉛などの金属が挙げられる。
これらの金属石けんの配合量は基油１００重量部に対し
２〜１５重量部、好ましくは５〜１０重量部である。配
合量が２重量部未満の場合は、効果が十分でなく、１５
重量部を超える場合には配合量に見合った効果が得られ
ず、経済的に好ましくない。
また本発明の金属スルホネートとは、石油スルホン酸、
ジノニルナフタレンスルホン酸、アルキルベンゼンスル
ホン酸等各種の鉱油系、合成系スルホン酸の金属塩であ
る。この金属としては、リチウム、ナトリウム、カリウ
ムなどのアルカリ金属、マグネシウム、カルシウム、バ
リウムなどのアルカリ土類金属、その他亜鉛などの金属
が挙げられる。また、これらの金属スルホネートは、中
性、塩基性、過塩基性のいずれのものでも使用できる。
これらの金属スルホネートの配合量は、基油１００重量
部に対し、２〜１５重量部、好ましくは３〜１０重量部
である。配合量が２重量部未満の場合には十分な効果が
得られず、また１５重量部を超える場合には配合量に見
合った効果が得られず、経済的に好ましくない。
本発明の組成物は、単独でも、優れた表面損傷防止機能
および防錆力を有するが、必要に応じて通常使用されて
いる公知の添加剤、例えば、酸化防止剤、粘度指数向上
剤、流動点降下剤、油性剤、極圧剤、腐食防止剤、さび
止め剤などを添加してもよい。
本発明でいう表面処理鋼板とは、冷間圧延鋼板、熱間圧
延鋼板などの鋼板の表面上に亜鉛、鉛、錫、クロム、ニ
ッケル、アルミニウムなどの金属およびこれらの合金類
をメッキしたものをいう。また、特に、亜鉛メッキ鋼板
は、冷間圧延鋼板、熱間圧延鋼板などの鋼板の表面上に
電気亜鉛メッキ法あるいは溶融亜鉛メッキ法により、亜
鉛、亜鉛−鉄合金、亜鉛−ニッケル合金、亜鉛−アルミ
ニウム合金等をメッキしたもの、あるいは、亜鉛や亜鉛
合金をメッキしたのち熱処理を行ってメッキ層と素材鉄
との合金化処理を行った、いわゆる合金化亜鉛メッキ鋼
板が好ましい。本発明の防錆油組成物は、上記した全て
の表面処理鋼板に好ましく使用できる。
実施例 以下、本発明を実施例および比較例によりさらに具体的
に説明する。
実施例１〜１４および比較例１〜１１ 本発明による表面処理鋼板用防錆油組成物（実施例１〜
１４）および比較のための組成物（比較例１〜１１）を
製造し、その組成を第１表に示した。なお、使用した各
成分および表面処理鋼板は以下の通りである。
鉱油 中東原油を蒸留し、得られた潤滑油留分をフルフラール
処理、水素精製、ＭＥＫ脱ろう処理することにより得ら
れたパラフィン系精製鉱油Ａ：４０℃の動粘度　　６．
５４ｃＳｔＢ：４０℃の動粘度　４８．８　　ｃｓｔＣ
：４０℃の動粘度　８５．３　　ｃＳｔ合成油 Ａ：弗化水素酸を触媒としてプロピレンポリマーをベン
ゼンにアルキル化することによりて得られた分枝）Ｊ１
ｙルキルベンゼン混合物４０℃の動粘度　１５．８　　
ｃＳｔ Ｂ：ポリ−α−オレフィン ４０℃の動粘度　１８．１　　ｃＳｔ Ｃ：ポリエステル ４０℃の動粘度　１９．９　　ｃｓｔ 硫化エステル Ａ；硫化ラード Ｂ：硫化植物油エステル Ｃ：硫化米ヌカメチルエステル 金属石けん Ａ：酸化パラフィンのバリウム石けん Ｂ：酸化パラフィンのナトリウム石けんＣ；ラノリン脂
肪酸のバリウム石けん 金属スルホネート Ａ：鉱油系スルホン酸のバリウム塩（中性Ｂ：アルキル
ベンゼンスルホン酸のカルシウム塩（塩基性） Ｃニジノニルナフタレンスルホン酸の ナトリウム塩 表面処理鋼板 Ａ：電気メッキ法により鋼板の両側の３０　ｇ　／　ｔ
ｒｒの亜鉛をメッキしたもの Ｂ：溶融メッキ法により片面に４５ｇ／ｎｆの亜鉛をメ
ッキし、熱処理によりメッキ層を合金化した、合金化溶
融亜鉛メッキ鋼板 これらの組成物につき、以下に示す試験によって性能評
価を行い、その結果を第１表に併記した。
・表面損傷防止性試験 表面処理鋼板試験片に組成物を塗布し、ビード引き抜き
試験を行い、試験後の試験片の表面メッキ層のフレーキ
ング、ゴーリングの発生状況を評価した。鉱油Ａと鉱油
Ｂを各５０重量％の割合で混合した４０℃粘度１５．４
ｃＳｔの無添加油を塗布して試験を行った場合の表面損
傷の状態を０、全く損傷のない鋼板の表面状態を１０と
した段階法で評価した。
・塩水噴霧による防錆性能評価 ＪＩＳ　　Ｋ　　２２４６に準拠して実施した。評点Ａ
はさび発生なし。評点Ｅは全面さび発生を表わし、Ａ−
Ｈの５段階で評価した。
・脱脂性評価試験 市販の脱脂剤を用いて脱脂性を評価した。表１中の０印
は脱脂性良好なことを、Ｘ印は脱脂性不良なことを、ま
たΔ印はその中間にあることを表す。
第１表の結果から明らかなように、鉱油に硫化エステル
および金属スルホネートを配合した組成物（実施例１〜
３）、鉱油に硫化エステルおよび金属石けんを配合した
組成物（実施例４〜６）はいずれも表面損傷防止性、さ
び止め性、脱脂性に優れている。また、金属スルホネー
トおよび金属石けんを併用した組成物（実施例７〜１４
）については°さび止め性がさらに向上している。実施
例１２および１４の組成物の脱脂性がやや低下している
が、実用上問題ない程度であり、いずれも表面損傷防止
性１、さび止め性、共に優れた表面処理鋼板用防錆油で
ある。
それに対して、基油に硫化エステルを単独で配合した組
成物（比較例１，２および９）は、表面損傷防止性が本
発明品に劣り、また、全くさび止め能力がない。また、
基油に金属石けんまたは金属スルホネートを単独で配合
した組成物（比較例３〜６）は、さび止め性は向上する
ものの、表面損傷防止能力がほとんどない。また、硫化
エステ少を用いずに、金属石けんおよび金属スルホネー
トを併用した組成物（比較例７，８．および１０）は、
さび止め性はさらに向上するが、やはり表面損傷防止能
力がほとんどない。さらに、硫化エステル、金属石けん
、および金属スルホネートの王者を配合した場合でも、
基油粘度が本発明の範囲外の組成物（比較例１１）は脱
脂性が悪く、実用は困難である。
発明の効果 以上のように、本発明の表面処理鋼板用防錆油は、各成
分の相乗効果により表面損傷防止能力に優れ、しかもさ
び止め性、脱脂性に優れた防錆油である。
特許出願人　　　日本石油株式会社

Claims (1)

  1. 【特許請求の範囲】 〔１〕４０℃での動粘度が５〜５０ｃＳｔである鉱油お
    よび／または合成油を基油とし、該基油１００重量部に
    対して （Ａ）硫化エステル２〜１５重量部 および （Ｂ）金属石けん２〜１５重量部 を必須の成分として配合してなる表面処理鋼板用防錆油
    組成物。 〔２〕４０℃での動粘度が５〜５０ｃＳｔである鉱油お
    よび／または合成油を基油とし、該基油１００重量部に
    対して （Ａ）硫化エステル２〜１５重量部 および （Ｂ）金属スルホネート２〜１５重量部 を必須の成分として配合してなる表面処理鋼板用防錆油
    組成物。 〔３〕４０℃での動粘度が５〜５０ｃＳｔである鉱油お
    よび／または合成油を基油とし、該基油１００重量部に
    対して （Ａ）硫化エステル２〜１５重量部 （Ｂ）金属石けん２〜１５重量部 および （Ｃ）金属スルホネート２〜１５重量部 を必須の成分として配合してなる表面処理鋼板用防錆油
    組成物。 〔４〕表面処理鋼板が亜鉛メッキ鋼板である請求項１か
    ら３のいずれか一項記載の表面処理鋼板用防錆油組成物
    。
JP1084262A 1988-12-27 1989-04-03 表面処理鋼板用成形加工兼防錆油組成物 Expired - Lifetime JP2764300B2 (ja)

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US07/577,011 US5104558A (en) 1988-12-27 1990-09-04 Rust-proofing oil composition

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JP63-330687 1988-12-27
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JPH0680978A (ja) * 1992-09-04 1994-03-22 Idemitsu Kosan Co Ltd 鋼のスズまたはスズ−亜鉛熱拡散処理材用潤滑剤組成物およびそれを用いた潤滑方法
JPH07179879A (ja) * 1993-11-11 1995-07-18 Nippon Seiko Kk 防錆潤滑油及びその防錆潤滑油が塗布された玉軸受
JPH0987648A (ja) * 1995-09-22 1997-03-31 Mitsubishi Oil Co Ltd 冷延鋼板及び亜鉛めっき鋼板用プレス加工兼洗浄防錆油組成物
JPH1190323A (ja) * 1997-09-24 1999-04-06 Nisshin Steel Co Ltd 防錆処理金属材およびその製造法
CN106520258A (zh) * 2016-08-31 2017-03-22 江苏龙蟠科技股份有限公司 一种乳化剂及其制备方法与应用

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JP3601634B2 (ja) * 1996-04-12 2004-12-15 新日本石油株式会社 さび止め剤組成物
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ATE557078T1 (de) * 2001-04-06 2012-05-15 Nippon Oil Corp Rostverhindernde ölzusammensetzung
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KR20060001022A (ko) * 2004-06-30 2006-01-06 고려용접봉 주식회사 용접와이어용 표면처리유 및 이로부터 표면처리된 용접용와이어
US7732386B2 (en) 2005-10-25 2010-06-08 Chevron U.S.A. Inc. Rust inhibitor for highly paraffinic lubricating base oil
JP4619266B2 (ja) * 2005-10-31 2011-01-26 トヨタ紡織株式会社 自動車用高張力鋼板のプレス加工用の潤滑油
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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH0680978A (ja) * 1992-09-04 1994-03-22 Idemitsu Kosan Co Ltd 鋼のスズまたはスズ−亜鉛熱拡散処理材用潤滑剤組成物およびそれを用いた潤滑方法
JPH07179879A (ja) * 1993-11-11 1995-07-18 Nippon Seiko Kk 防錆潤滑油及びその防錆潤滑油が塗布された玉軸受
JPH0987648A (ja) * 1995-09-22 1997-03-31 Mitsubishi Oil Co Ltd 冷延鋼板及び亜鉛めっき鋼板用プレス加工兼洗浄防錆油組成物
JPH1190323A (ja) * 1997-09-24 1999-04-06 Nisshin Steel Co Ltd 防錆処理金属材およびその製造法
CN106520258A (zh) * 2016-08-31 2017-03-22 江苏龙蟠科技股份有限公司 一种乳化剂及其制备方法与应用

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