JPH0118067B2 - - Google Patents
Info
- Publication number
- JPH0118067B2 JPH0118067B2 JP53094449A JP9444978A JPH0118067B2 JP H0118067 B2 JPH0118067 B2 JP H0118067B2 JP 53094449 A JP53094449 A JP 53094449A JP 9444978 A JP9444978 A JP 9444978A JP H0118067 B2 JPH0118067 B2 JP H0118067B2
- Authority
- JP
- Japan
- Prior art keywords
- isocyanate
- reaction
- reaction mixture
- solvent
- water
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
- B01J23/38—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
- B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
- B01J23/72—Copper
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C263/00—Preparation of derivatives of isocyanic acid
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C263/00—Preparation of derivatives of isocyanic acid
- C07C263/18—Separation; Purification; Stabilisation; Use of additives
- C07C263/20—Separation; Purification
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C2601/00—Systems containing only non-condensed rings
- C07C2601/12—Systems containing only non-condensed rings with a six-membered ring
- C07C2601/14—The ring being saturated
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Catalysts (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| NL7708510 | 1977-08-02 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS5439018A JPS5439018A (en) | 1979-03-24 |
| JPH0118067B2 true JPH0118067B2 (esLanguage) | 1989-04-03 |
Family
ID=19828957
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP9444978A Granted JPS5439018A (en) | 1977-08-02 | 1978-08-02 | Process for preparing isocyanate from formamide |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US4207251A (esLanguage) |
| EP (1) | EP0000602B1 (esLanguage) |
| JP (1) | JPS5439018A (esLanguage) |
| CA (1) | CA1117962A (esLanguage) |
| DE (1) | DE2860856D1 (esLanguage) |
| IT (1) | IT1097592B (esLanguage) |
Families Citing this family (20)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4430262A (en) * | 1981-06-05 | 1984-02-07 | Shell Oil Company | Preparation of isocyanates and/or derivatives thereof |
| DE3229323A1 (de) * | 1982-08-06 | 1984-02-09 | Basf Ag, 6700 Ludwigshafen | Verfahren zur herstellung aliphatischer isocyanate durch oxidative dehydrierung von formamiden |
| US4469640A (en) * | 1983-03-14 | 1984-09-04 | E. I. Du Pont De Nemours And Company | Catalytic conversion of formamides to isocyanates |
| US4824991A (en) * | 1984-08-09 | 1989-04-25 | E. I. Du Pont De Nemours And Company | Process for separating methyl isocyanate |
| US4694101A (en) * | 1984-08-09 | 1987-09-15 | E. I. Du Pont De Nemours And Company | Process for separating methyl isocyanate |
| US4537726A (en) * | 1984-11-09 | 1985-08-27 | E. I. Du Pont De Nemours And Company | Multi-stage process with adiabatic reactors for the preparation of isocyanates |
| US4698438A (en) * | 1985-04-26 | 1987-10-06 | E. I. Du Pont De Nemours And Company | Process for the preparation of methyl carbamates and thioimidates |
| US4603016A (en) * | 1985-11-14 | 1986-07-29 | E. I. Du Pont De Nemours And Company | Cryogenic brine separation of water and isocyanates |
| DE3573111D1 (en) * | 1985-12-12 | 1989-10-26 | Du Pont | Process for separating methyl isocyanate |
| US4683329A (en) * | 1986-04-16 | 1987-07-28 | E. I. Dupont De Nemours And Company | Beneficial use of water in catalytic conversion of formamides to isocyanates |
| US4795830A (en) * | 1986-09-02 | 1989-01-03 | E. I. Du Pont De Nemours And Company | Use of water to inhibit decomposition of monoalkylformamides |
| US5126480A (en) * | 1990-06-01 | 1992-06-30 | Arco Chemical Technology, L.P. | Isocyanate preparation |
| US5155267A (en) * | 1991-10-24 | 1992-10-13 | Arco Chemical Technology, L.P. | Synthesis of isocyanate precursors from primary formamides |
| JP2012509868A (ja) * | 2008-11-24 | 2012-04-26 | リライアンス ライフ サイエンシズ ピーヴィーティー リミティッド | テトラジン誘導体の製造方法 |
| WO2011067242A1 (de) * | 2009-12-01 | 2011-06-09 | Basf Se | Verfahren zur herstellung von isocyanaten durch thermische spaltung von carbamaten |
| US8835673B2 (en) * | 2009-12-04 | 2014-09-16 | Basf Se | Process for preparing isocyanates |
| PL2701841T3 (pl) * | 2011-04-26 | 2015-11-30 | Basf Se | Sposób utleniającego odwodorniania metanolu do formaldehydu na dzianinach zawierających srebro |
| CN107473989B (zh) * | 2016-06-08 | 2020-04-28 | 中国科学院大连化学物理研究所 | 一种催化甲醇转化制氨基甲酸甲酯的方法 |
| US20240336561A1 (en) | 2021-06-28 | 2024-10-10 | MAX-PLANCK-Gesellschaft zur Förderung der Wissenschaften e.V. | Catalytic synthesis of free isocyanates |
| KR102806436B1 (ko) * | 2024-03-29 | 2025-05-09 | 한화솔루션 주식회사 | 이소시아네이트 조성물, 이를 포함하는 광학렌즈 및 이를 이용한 이소시아네이트 조성물 보관방법 |
Family Cites Families (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3099673A (en) * | 1959-08-19 | 1963-07-30 | Bayer Ag | Process for the production of organic isocyanates |
| US3277140A (en) * | 1963-07-16 | 1966-10-04 | Air Prod & Chem | Preparation of aliphatic isocyanates |
| DE1277851B (de) | 1966-04-20 | 1968-09-19 | Bayer Ag | Verfahren zur Herstellung von 2-Chlorcarbonylphenylisocyanaten |
| US3929859A (en) * | 1974-11-18 | 1975-12-30 | Standard Oil Co Ohio | Manufacture of dinitriles from thiodinitriles |
| US3960914A (en) * | 1975-05-06 | 1976-06-01 | Sun Ventures, Inc. | Conversion of formamides to isocyanates |
| DE2520219C3 (de) | 1975-05-07 | 1983-02-24 | Basf Ag, 6700 Ludwigshafen | Verfahren zur Herstellung von Formaldehyd |
-
1978
- 1978-07-10 US US05/923,278 patent/US4207251A/en not_active Expired - Lifetime
- 1978-07-14 DE DE7878200097T patent/DE2860856D1/de not_active Expired
- 1978-07-14 EP EP78200097A patent/EP0000602B1/en not_active Expired
- 1978-07-31 IT IT26324/78A patent/IT1097592B/it active
- 1978-08-01 CA CA000308524A patent/CA1117962A/en not_active Expired
- 1978-08-02 JP JP9444978A patent/JPS5439018A/ja active Granted
Also Published As
| Publication number | Publication date |
|---|---|
| EP0000602A1 (en) | 1979-02-07 |
| JPS5439018A (en) | 1979-03-24 |
| DE2860856D1 (en) | 1981-10-29 |
| IT7826324A0 (it) | 1978-07-31 |
| US4207251A (en) | 1980-06-10 |
| CA1117962A (en) | 1982-02-09 |
| EP0000602B1 (en) | 1981-07-22 |
| IT1097592B (it) | 1985-08-31 |
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