JP7533875B2 - ピロリジジンアルカロイドの分析方法 - Google Patents

ピロリジジンアルカロイドの分析方法 Download PDF

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JP7533875B2
JP7533875B2 JP2020212915A JP2020212915A JP7533875B2 JP 7533875 B2 JP7533875 B2 JP 7533875B2 JP 2020212915 A JP2020212915 A JP 2020212915A JP 2020212915 A JP2020212915 A JP 2020212915A JP 7533875 B2 JP7533875 B2 JP 7533875B2
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sample
analytical method
group
analysis
pyrrolizidine
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JP2021110738A (ja
JP2021110738A5 (https=
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ヂェンホー チェン
シャオドン リー
尚樹 濱田
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Shimadzu China Co Ltd
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N27/00Investigating or analysing materials by the use of electric, electrochemical, or magnetic means
    • G01N27/62Investigating or analysing materials by the use of electric, electrochemical, or magnetic means by investigating the ionisation of gases, e.g. aerosols; by investigating electric discharges, e.g. emission of cathode
    • G01N27/68Investigating or analysing materials by the use of electric, electrochemical, or magnetic means by investigating the ionisation of gases, e.g. aerosols; by investigating electric discharges, e.g. emission of cathode using electric discharge to ionise a gas

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Electrochemistry (AREA)
  • Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
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  • Other Investigation Or Analysis Of Materials By Electrical Means (AREA)
JP2020212915A 2020-01-07 2020-12-22 ピロリジジンアルカロイドの分析方法 Active JP7533875B2 (ja)

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CN202010013660.9 2020-01-07
CN202010013660.9A CN113155944B (zh) 2020-01-07 2020-01-07 吡咯里西啶类生物碱的分析方法

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JP2021110738A5 JP2021110738A5 (https=) 2023-07-20
JP7533875B2 true JP7533875B2 (ja) 2024-08-14

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Families Citing this family (7)

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Publication number Priority date Publication date Assignee Title
CN114778725B (zh) * 2022-04-18 2023-08-25 安徽农业大学 一种基于QuEChERS法结合UPLC-MS/MS的吡咯里西啶碱检测方法及应用
CN114894927B (zh) * 2022-04-28 2023-11-21 广西壮族自治区食品药品检验所 瑶药白背三七中吡咯里西啶生物碱的含量测定方法
CN115561298A (zh) * 2022-09-21 2023-01-03 广西农业职业技术大学 一种检测肿节风中稀土元素含量的方法
CN116026947B (zh) * 2022-11-16 2025-02-28 上海理工大学 一种测定甘草中吡咯里西啶生物碱的方法
TW202508684A (zh) 2023-08-16 2025-03-01 農業部農業藥物試驗所 適用於農產品的殘留農藥萃取組合液、及使用該殘留農藥萃取組合液的農產品檢液原液快速萃取方法與農產品農藥殘留檢測方法
CN117761192B (zh) * 2023-12-22 2025-03-11 广州海关技术中心 一种化妆品中吡咯里西啶生物碱的检测方法
CN120195323B (zh) * 2025-05-27 2025-08-05 中国测试技术研究院 食品中吡咯里西啶类生物碱的检测方法

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2008195696A (ja) 2007-02-16 2008-08-28 Okayama Univ N−アセチルグルコサミニダーゼ阻害活性を有する化合物
CN109169387A (zh) 2018-09-10 2019-01-11 南宁利腾农业科技有限公司 乳鸽垫

Family Cites Families (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CA2393726A1 (en) * 2002-07-16 2004-01-16 Steven J. Locke Quantitative proteomics via isotopically differentiated derivatization
US8110797B2 (en) * 2009-02-06 2012-02-07 Florida State University Research Foundation, Inc. Electrospray ionization mass spectrometry methodology
JP2011027429A (ja) * 2009-07-21 2011-02-10 Kirin Holdings Co Ltd 液体クロマトグラフィーを用いたグリコアルカロイド類の精製および分析法
CN103792278B (zh) * 2014-01-26 2017-01-11 南昌大学 莲子中生物碱的电喷雾萃取电离质谱快速检测方法
US10121644B2 (en) * 2014-02-10 2018-11-06 Shimadzu Corporation Mass spectrometer and mass spectrometry method
CN104134606B (zh) * 2014-07-30 2017-04-19 中山大学 一种微萃取探针电喷雾离子源及其制备方法和应用
EP3265822B1 (en) * 2015-03-06 2021-04-28 Micromass UK Limited Tissue analysis by mass spectrometry or ion mobility spectrometry
CN105259273B (zh) * 2015-11-01 2017-05-24 中国科学院成都生物研究所 耐盐液相色谱电喷雾质谱联用接口装置及其使用方法
KR20170142673A (ko) * 2016-06-20 2017-12-28 한국과학기술연구원 종이분무이온화 및 질량분석기를 이용한 생체 뇨 시료 내 에페드린류의 직접 정량 분석 방법
CN106404945A (zh) * 2016-08-30 2017-02-15 中山大学 一种段塞流微萃取‑纸基电喷雾质谱联用技术
CN108169387A (zh) * 2016-12-07 2018-06-15 中国科学院大连化学物理研究所 一种中药制剂中吡咯里西啶生物碱的液/质分析样品前处理法
KR20190087900A (ko) * 2018-01-17 2019-07-25 한미약품 주식회사 도네페질 및 메만틴의 동시 분석방법
CN110187016A (zh) * 2019-05-07 2019-08-30 司法鉴定科学研究院 一种干血样品中的卡西酮类物质的分析方法
CN110208358A (zh) * 2019-05-21 2019-09-06 暨南大学 一种高频振动雾化电离探针装置及方法
CN110161143A (zh) * 2019-06-12 2019-08-23 厦门出入境检验检疫局检验检疫技术中心 一种同时检测食品中20种生物碱的色谱-质谱联用方法

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2008195696A (ja) 2007-02-16 2008-08-28 Okayama Univ N−アセチルグルコサミニダーゼ阻害活性を有する化合物
CN109169387A (zh) 2018-09-10 2019-01-11 南宁利腾农业科技有限公司 乳鸽垫

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CN113155944A (zh) 2021-07-23
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