JP2021110738A5 - - Google Patents
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- Publication number
- JP2021110738A5 JP2021110738A5 JP2020212915A JP2020212915A JP2021110738A5 JP 2021110738 A5 JP2021110738 A5 JP 2021110738A5 JP 2020212915 A JP2020212915 A JP 2020212915A JP 2020212915 A JP2020212915 A JP 2020212915A JP 2021110738 A5 JP2021110738 A5 JP 2021110738A5
- Authority
- JP
- Japan
- Prior art keywords
- oxide
- seneciphylline
- senecionine
- senkiruquin
- retrolucine
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- HKODIGSRFALUTA-ZJQCNOOHSA-N Integerrimine Natural products CC=C1C[C@H](C)[C@@](C)(O)C(=O)OCC2=CCN3CC[C@@H](OC1=O)[C@H]23 HKODIGSRFALUTA-ZJQCNOOHSA-N 0.000 description 1
- PHMRVSMVJKXEEJ-UHFFFAOYSA-N Seneciphylline Natural products CC=C/1CC(=C)C(C)(O)C(=O)OCC2CCN3C=CC(OC1=O)C23 PHMRVSMVJKXEEJ-UHFFFAOYSA-N 0.000 description 1
- CTCKXBIRQMSUIU-UHFFFAOYSA-N Seneciphyllinine Natural products O1C(=O)C(=CC)CC(=C)C(C)(OC(C)=O)C(=O)OCC2=CCN3C2C1CC3 CTCKXBIRQMSUIU-UHFFFAOYSA-N 0.000 description 1
- FCEVNJIUIMLVML-IIDMSEBBSA-N alpha-longilobine Natural products O1C(=O)C(=CC)CC(=C)[C@@](C)(O)C(=O)OCC2=CCN3[C@H]2[C@H]1CC3 FCEVNJIUIMLVML-IIDMSEBBSA-N 0.000 description 1
- LHVAZUAALQTANZ-ANYXPJNNSA-N chembl469442 Chemical compound C1OC(=O)[C@](C)(O)[C@@](O)(C)[C@@H](C)C(=O)O[C@@H]2CC[N+]3([O-])[C@@H]2C1=CC3 LHVAZUAALQTANZ-ANYXPJNNSA-N 0.000 description 1
- -1 laciocarpine Chemical compound 0.000 description 1
- BTHCJHQOYFUIMG-UHFFFAOYSA-N platyphylline Natural products O1C(=O)C(=CC)CC(C)C(C)(O)C(=O)OCC2CCN3C2C1CC3 BTHCJHQOYFUIMG-UHFFFAOYSA-N 0.000 description 1
- ADRDEXBBJTUCND-UHFFFAOYSA-N pyrrolizidine Chemical class C1CCN2CCCC21 ADRDEXBBJTUCND-UHFFFAOYSA-N 0.000 description 1
- 229930002356 pyrrolizidine alkaloid Natural products 0.000 description 1
- HKODIGSRFALUTA-JTLQZVBZSA-N senecionine Chemical compound O1C(=O)C(=C/C)\C[C@@H](C)[C@@](C)(O)C(=O)OCC2=CCN3[C@H]2[C@H]1CC3 HKODIGSRFALUTA-JTLQZVBZSA-N 0.000 description 1
- OZPMZVHQAUHYCP-UHFFFAOYSA-N senecionine Natural products CC=C/1CC(C)C(C)(O)C(=O)OC2=CCN3CCC(OC1=O)C23 OZPMZVHQAUHYCP-UHFFFAOYSA-N 0.000 description 1
- PLGBHVNNYDZWGZ-GPUZEBNTSA-N senecionine N-oxide Chemical compound O1C(=O)C(=C/C)\C[C@@H](C)[C@@](C)(O)C(=O)OCC2=CC[N+]3([O-])[C@H]2[C@H]1CC3 PLGBHVNNYDZWGZ-GPUZEBNTSA-N 0.000 description 1
- FCEVNJIUIMLVML-QPSVUOIXSA-N seneciphylline Chemical compound O1C(=O)C(=C/C)\CC(=C)[C@@](C)(O)C(=O)OCC2=CCN3[C@H]2[C@H]1CC3 FCEVNJIUIMLVML-QPSVUOIXSA-N 0.000 description 1
- FCEVNJIUIMLVML-UHFFFAOYSA-N spartioidine Natural products O1C(=O)C(=CC)CC(=C)C(C)(O)C(=O)OCC2=CCN3C2C1CC3 FCEVNJIUIMLVML-UHFFFAOYSA-N 0.000 description 1
- COHUFMBRBUPZPA-HPHFTHPTSA-N spartioidine N-oxide Chemical compound O1C(=O)C(=C/C)/CC(=C)[C@@](C)(O)C(=O)OCC2=CC[N+]3([O-])[C@H]2[C@H]1CC3 COHUFMBRBUPZPA-HPHFTHPTSA-N 0.000 description 1
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202010013660.9 | 2020-01-07 | ||
| CN202010013660.9A CN113155944B (zh) | 2020-01-07 | 2020-01-07 | 吡咯里西啶类生物碱的分析方法 |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2021110738A JP2021110738A (ja) | 2021-08-02 |
| JP2021110738A5 true JP2021110738A5 (https=) | 2023-07-20 |
| JP7533875B2 JP7533875B2 (ja) | 2024-08-14 |
Family
ID=76881354
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2020212915A Active JP7533875B2 (ja) | 2020-01-07 | 2020-12-22 | ピロリジジンアルカロイドの分析方法 |
Country Status (2)
| Country | Link |
|---|---|
| JP (1) | JP7533875B2 (https=) |
| CN (1) | CN113155944B (https=) |
Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114778725B (zh) * | 2022-04-18 | 2023-08-25 | 安徽农业大学 | 一种基于QuEChERS法结合UPLC-MS/MS的吡咯里西啶碱检测方法及应用 |
| CN114894927B (zh) * | 2022-04-28 | 2023-11-21 | 广西壮族自治区食品药品检验所 | 瑶药白背三七中吡咯里西啶生物碱的含量测定方法 |
| CN115561298A (zh) * | 2022-09-21 | 2023-01-03 | 广西农业职业技术大学 | 一种检测肿节风中稀土元素含量的方法 |
| CN116026947B (zh) * | 2022-11-16 | 2025-02-28 | 上海理工大学 | 一种测定甘草中吡咯里西啶生物碱的方法 |
| TW202508684A (zh) | 2023-08-16 | 2025-03-01 | 農業部農業藥物試驗所 | 適用於農產品的殘留農藥萃取組合液、及使用該殘留農藥萃取組合液的農產品檢液原液快速萃取方法與農產品農藥殘留檢測方法 |
| CN117761192B (zh) * | 2023-12-22 | 2025-03-11 | 广州海关技术中心 | 一种化妆品中吡咯里西啶生物碱的检测方法 |
| CN120195323B (zh) * | 2025-05-27 | 2025-08-05 | 中国测试技术研究院 | 食品中吡咯里西啶类生物碱的检测方法 |
Family Cites Families (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CA2393726A1 (en) * | 2002-07-16 | 2004-01-16 | Steven J. Locke | Quantitative proteomics via isotopically differentiated derivatization |
| JP4636623B2 (ja) | 2007-02-16 | 2011-02-23 | 国立大学法人 岡山大学 | Ｎ−アセチルグルコサミニダーゼ阻害活性を有する化合物 |
| US8110797B2 (en) * | 2009-02-06 | 2012-02-07 | Florida State University Research Foundation, Inc. | Electrospray ionization mass spectrometry methodology |
| JP2011027429A (ja) * | 2009-07-21 | 2011-02-10 | Kirin Holdings Co Ltd | 液体クロマトグラフィーを用いたグリコアルカロイド類の精製および分析法 |
| CN103792278B (zh) * | 2014-01-26 | 2017-01-11 | 南昌大学 | 莲子中生物碱的电喷雾萃取电离质谱快速检测方法 |
| US10121644B2 (en) * | 2014-02-10 | 2018-11-06 | Shimadzu Corporation | Mass spectrometer and mass spectrometry method |
| CN104134606B (zh) * | 2014-07-30 | 2017-04-19 | 中山大学 | 一种微萃取探针电喷雾离子源及其制备方法和应用 |
| EP3265822B1 (en) * | 2015-03-06 | 2021-04-28 | Micromass UK Limited | Tissue analysis by mass spectrometry or ion mobility spectrometry |
| CN105259273B (zh) * | 2015-11-01 | 2017-05-24 | 中国科学院成都生物研究所 | 耐盐液相色谱电喷雾质谱联用接口装置及其使用方法 |
| KR20170142673A (ko) * | 2016-06-20 | 2017-12-28 | 한국과학기술연구원 | 종이분무이온화 및 질량분석기를 이용한 생체 뇨 시료 내 에페드린류의 직접 정량 분석 방법 |
| CN106404945A (zh) * | 2016-08-30 | 2017-02-15 | 中山大学 | 一种段塞流微萃取‑纸基电喷雾质谱联用技术 |
| CN108169387A (zh) * | 2016-12-07 | 2018-06-15 | 中国科学院大连化学物理研究所 | 一种中药制剂中吡咯里西啶生物碱的液/质分析样品前处理法 |
| KR20190087900A (ko) * | 2018-01-17 | 2019-07-25 | 한미약품 주식회사 | 도네페질 및 메만틴의 동시 분석방법 |
| CN109169387B (zh) | 2018-09-10 | 2023-10-13 | 南宁利腾农业科技有限公司 | 乳鸽垫 |
| CN110187016A (zh) * | 2019-05-07 | 2019-08-30 | 司法鉴定科学研究院 | 一种干血样品中的卡西酮类物质的分析方法 |
| CN110208358A (zh) * | 2019-05-21 | 2019-09-06 | 暨南大学 | 一种高频振动雾化电离探针装置及方法 |
| CN110161143A (zh) * | 2019-06-12 | 2019-08-23 | 厦门出入境检验检疫局检验检疫技术中心 | 一种同时检测食品中20种生物碱的色谱-质谱联用方法 |
-
2020
- 2020-01-07 CN CN202010013660.9A patent/CN113155944B/zh active Active
- 2020-12-22 JP JP2020212915A patent/JP7533875B2/ja active Active
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