JP6949693B2 - 尿素、アンモニア及び二酸化炭素を含む水溶液の処理方法並びに処理設備 - Google Patents

尿素、アンモニア及び二酸化炭素を含む水溶液の処理方法並びに処理設備 Download PDF

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JP6949693B2
JP6949693B2 JP2017235912A JP2017235912A JP6949693B2 JP 6949693 B2 JP6949693 B2 JP 6949693B2 JP 2017235912 A JP2017235912 A JP 2017235912A JP 2017235912 A JP2017235912 A JP 2017235912A JP 6949693 B2 JP6949693 B2 JP 6949693B2
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urea
aqueous solution
ammonia
stripper
carbon dioxide
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JP2019098307A5 (enExample
JP2019098307A (ja
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啓伍 佐々木
啓伍 佐々木
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Toyo Engineering Corp
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Toyo Engineering Corp
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Priority to JP2017235912A priority Critical patent/JP6949693B2/ja
Priority to US16/208,332 priority patent/US10730761B2/en
Priority to GB1819924.0A priority patent/GB2571601B/en
Priority to CN201811496534.2A priority patent/CN109896534B/zh
Publication of JP2019098307A publication Critical patent/JP2019098307A/ja
Publication of JP2019098307A5 publication Critical patent/JP2019098307A5/ja
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00—Treatment of water, waste water, or sewage
    • C02F1/02—Treatment of water, waste water, or sewage by heating
    • C02F1/025—Thermal hydrolysis
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D19/00—Degasification of liquids
    • B01D19/0005—Degasification of liquids with one or more auxiliary substances
    • B01D19/001—Degasification of liquids with one or more auxiliary substances by bubbling steam through the liquid
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/009—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping in combination with chemical reactions
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14—Fractional distillation or use of a fractionation or rectification column
    • B01D3/143—Fractional distillation or use of a fractionation or rectification column by two or more of a fractionation, separation or rectification step
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/34—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping with one or more auxiliary substances
    • B01D3/38—Steam distillation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/34—Chemical or biological purification of waste gases
    • B01D53/46—Removing components of defined structure
    • B01D53/54—Nitrogen compounds
    • B01D53/58—Ammonia
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/34—Chemical or biological purification of waste gases
    • B01D53/74—General processes for purification of waste gases; Apparatus or devices specially adapted therefor
    • B01D53/77—Liquid phase processes
    • B01D53/78—Liquid phase processes with gas-liquid contact
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00—Treatment of water, waste water, or sewage
    • C02F1/20—Treatment of water, waste water, or sewage by degassing, i.e. liberation of dissolved gases
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00—Treatment of water, waste water, or sewage
    • C02F1/66—Treatment of water, waste water, or sewage by neutralisation; pH adjustment
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C273/00—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C273/00—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups
    • C07C273/02—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups of urea, its salts, complexes or addition compounds
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01C—AMMONIA; CYANOGEN; COMPOUNDS THEREOF
    • C01C1/00—Ammonia; Compounds thereof
    • C01C1/28—Methods of preparing ammonium salts in general
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F2101/00—Nature of the contaminant
    • C02F2101/10—Inorganic compounds
    • C02F2101/16—Nitrogen compounds, e.g. ammonia
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F2101/00—Nature of the contaminant
    • C02F2101/30—Organic compounds
    • C02F2101/38—Organic compounds containing nitrogen
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F2103/00—Nature of the water, waste water, sewage or sludge to be treated
    • C02F2103/34—Nature of the water, waste water, sewage or sludge to be treated from industrial activities not provided for in groups C02F2103/12 - C02F2103/32
    • C02F2103/36—Nature of the water, waste water, sewage or sludge to be treated from industrial activities not provided for in groups C02F2103/12 - C02F2103/32 from the manufacture of organic compounds
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F2209/00—Controlling or monitoring parameters in water treatment
    • C02F2209/02—Temperature
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F2209/00—Controlling or monitoring parameters in water treatment
    • C02F2209/03—Pressure
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F2301/00—General aspects of water treatment
    • C02F2301/08—Multistage treatments, e.g. repetition of the same process step under different conditions
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/10—Process efficiency
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/151—Reduction of greenhouse gas [GHG] emissions, e.g. CO2
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P70/00—Climate change mitigation technologies in the production process for final industrial or consumer products
    • Y02P70/10—Greenhouse gas [GHG] capture, material saving, heat recovery or other energy efficient measures, e.g. motor control, characterised by manufacturing processes, e.g. for rolling metal or metal working

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Environmental & Geological Engineering (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Hydrology & Water Resources (AREA)
  • Water Supply & Treatment (AREA)
  • General Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Biomedical Technology (AREA)
  • Analytical Chemistry (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Thermal Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Physical Water Treatments (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Degasification And Air Bubble Elimination (AREA)
  • Removal Of Specific Substances (AREA)
JP2017235912A 2017-12-08 2017-12-08 尿素、アンモニア及び二酸化炭素を含む水溶液の処理方法並びに処理設備 Active JP6949693B2 (ja)

Priority Applications (4)

Application Number Priority Date Filing Date Title
JP2017235912A JP6949693B2 (ja) 2017-12-08 2017-12-08 尿素、アンモニア及び二酸化炭素を含む水溶液の処理方法並びに処理設備
US16/208,332 US10730761B2 (en) 2017-12-08 2018-12-03 Treatment method of an aqueous solution containing urea, ammonia and carbon dioxide and treatment equipment therefor
GB1819924.0A GB2571601B (en) 2017-12-08 2018-12-06 Treatment method
CN201811496534.2A CN109896534B (zh) 2017-12-08 2018-12-07 含有尿素、氨和二氧化碳的水溶液的处理方法及其处理设备

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP2017235912A JP6949693B2 (ja) 2017-12-08 2017-12-08 尿素、アンモニア及び二酸化炭素を含む水溶液の処理方法並びに処理設備

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JP2019098307A JP2019098307A (ja) 2019-06-24
JP2019098307A5 JP2019098307A5 (enExample) 2020-12-03
JP6949693B2 true JP6949693B2 (ja) 2021-10-13

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US (1) US10730761B2 (enExample)
JP (1) JP6949693B2 (enExample)
CN (1) CN109896534B (enExample)
GB (1) GB2571601B (enExample)

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102019208859A1 (de) * 2019-06-18 2020-12-24 Skw Stickstoffwerke Piesteritz Gmbh Verfahren zur kontinuierlichen Herstellung reiner Harnstofflösungen durch Verwertung von Prozesswasser
EP3782979A1 (en) * 2019-08-20 2021-02-24 Yara International ASA Preparation of urea solution and facility to do so
CN113426153B (zh) * 2021-06-25 2024-06-21 中国成达工程有限公司 生产液体车用尿素及脱硝用尿素溶液的生产装置及方法
WO2023156360A1 (de) 2022-02-18 2023-08-24 Thyssenkrupp Industrial Solutions Ag Optimierte prozesskondensataufbereitung
LU102914B1 (de) 2022-02-18 2023-08-18 Thyssenkrupp Ind Solutions Ag Optimierte Prozesskondensataufbereitung

Family Cites Families (15)

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Publication number Priority date Publication date Assignee Title
JPS555977B2 (enExample) * 1974-05-14 1980-02-12
JPS5352274A (en) * 1976-10-25 1978-05-12 Mitsui Toatsu Chem Inc Treating method for aqueous solution containing urea, ammonia and carbondioxide
NL8102391A (nl) * 1981-05-15 1982-12-01 Unie Van Kunstmestfab Bv Werkwijze voor het winnen van waardevolle bestanddelen uit de afvalstromen verkregen bij de ureumbereiding.
NL8702530A (nl) * 1987-10-23 1989-05-16 Stamicarbon Werkwijze voor de bereiding van ureum en water uitgaande van ammoniak en kooldioxide.
DE69326881D1 (de) * 1993-01-07 1999-12-02 Urea Casale Sa Verbessertes Verfahren zur Produktion von Harnstoff unter Verwendung eines Schrittes zur Kohlendioxidentfernung
ES2119071T3 (es) * 1994-11-18 1998-10-01 Norsk Hydro As Procedimiento para preparar urea.
JPH09227493A (ja) * 1996-02-27 1997-09-02 Toyo Eng Corp 排ガス中からの尿素ダスト及びアンモニアの回収方法
JP2000001466A (ja) * 1998-06-12 2000-01-07 Toyo Eng Corp 排ガス中の尿素ダスト及びアンモニアの回収・利用方法
JP2000279736A (ja) * 1999-03-29 2000-10-10 Toyo Eng Corp 尿素ダスト及びアンモニアを含有する流体の処理装置、それを用いた処理方法及びそれを付設した尿素製造装置
CN100556503C (zh) * 2006-08-01 2009-11-04 智胜化工股份有限公司 一种净化尿素造粒塔粉尘的方法
ITMI20072206A1 (it) * 2007-11-21 2009-05-22 Snam Progetti Metodo per il recupero di ammoniaca da una corrente gassosa in un processo di sintesi di urea
EP2119489A1 (en) * 2008-05-14 2009-11-18 Uhde Fertilizer Technology B.V. Method for reducing aerosol emissions in a urea granulation plant
CN103011366B (zh) * 2012-12-14 2013-12-25 太原理工大学 一种固体催化剂催化水解低浓度尿素废水的方法
EA201890452A1 (ru) * 2015-09-08 2018-08-31 Тойо Инджиниринг Корпорейшн Способ получения мочевины и установка для получения мочевины
JP6634342B2 (ja) * 2016-05-24 2020-01-22 東洋エンジニアリング株式会社 尿素水溶液の処理方法および装置

Also Published As

Publication number Publication date
GB2571601B (en) 2022-04-27
CN109896534A (zh) 2019-06-18
CN109896534B (zh) 2024-03-01
US10730761B2 (en) 2020-08-04
US20190177180A1 (en) 2019-06-13
GB2571601A (en) 2019-09-04
GB201819924D0 (en) 2019-01-23
JP2019098307A (ja) 2019-06-24

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