JP6522863B1 - 積層シート、コーティング繊維、コーティング繊維束及び繊維強化プラスチック - Google Patents
積層シート、コーティング繊維、コーティング繊維束及び繊維強化プラスチック Download PDFInfo
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- JP6522863B1 JP6522863B1 JP2018549592A JP2018549592A JP6522863B1 JP 6522863 B1 JP6522863 B1 JP 6522863B1 JP 2018549592 A JP2018549592 A JP 2018549592A JP 2018549592 A JP2018549592 A JP 2018549592A JP 6522863 B1 JP6522863 B1 JP 6522863B1
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Abstract
Description
本発明に係る積層シート(以下、積層シート(1)と記載することがある)は、繊維基材と、該繊維基材の表面上に配置されている色調調整層(後述する第2の色調調整層と区別して、第1の色調調整層と呼ぶことがある)とを備える積層シートである。本発明に係る積層シート(1)は、第1の表面と、該第1の表面とは反対側に第2の表面とを有する。本発明に係る積層シート(1)では、上記積層シートの上記第1の表面側に上記繊維基材が配置されており、上記積層シートの上記第2の表面側に上記色調調整層が配置されている。本発明に係る積層シート(1)では、上記色調調整層は、上記積層シートの上記第2の表面の色調を、上記繊維基材の表面の色調とは異なるようにする性質を有する層である。本発明に係る積層シート(1)では、上記色調調整層は、光透過性を有する。
上記繊維基材は、上記積層シート中において、上記積層シートの上記第1の表面側に配置される。上記繊維基材は、1層であってもよく、多層であってもよい。
上記色調調整層は、上記繊維基材の表面上に配置される層である。上記色調調整層は、上記積層シート中において、上記積層シートの上記第2の表面側に配置される。上記色調調整層は、上記積層シートの上記第2の表面の色調を、上記繊維基材の表面の色調とは異なるようにする性質を有する層である。また、上記色調調整層は、光透過性を有する層である。
本発明に係るコーティング繊維は、繊維と、該繊維の表面上に配置されている色調調整層とを備える。本発明に係るコーティング繊維では、上記色調調整層は、MOx、又はMNxを含む層を有し、MOxの場合には、Mはn価の金属又は半金属を表し、かつxは0以上n/2未満の数を表し、MNxの場合には、Mはn価の金属又は半金属を表し、かつxは0以上n/3未満の数を表す。本発明に係るコーティング繊維では、上記色調調整層は、光透過性を有する。
本発明に係るコーティング繊維束は、複数の繊維を有し、上記繊維が上述したコーティング繊維を含む。
本発明に係る複合材料は、(1)上述した積層シートと、樹脂とを含むか、(2)上述したコーティング繊維と、樹脂とを含むか、(3)上述したコーティング繊維束と、樹脂とを含む。
繊維基材として、黒色のポリエステル(30デニール)が平織で織られた織物であるポリエステル繊維基材(マスダ社製「ひかるげんじTM−3001 E21」)を用いた。繊維基材を真空装置内に設置し、8.0×10−4Pa以下となるまで真空排気した。続いて、アルゴンガスを導入して、DCマグネトロンスパッタリング法により、繊維基材の表面上に、色調調整層(第1の色調調整層)としてSiO0.5層(平均厚み15nm)を形成して、積層シートを得た。
第2の色調調整層の形成:
参考例1における繊維基材(ポリエステル繊維基材)を用意した。繊維基材を真空装置内に設置し、8.0×10−4Pa以下となるまで真空排気した。続いて、アルゴンガスを導入して、DCマグネトロンスパッタリング法により、繊維基材の表面上に、第2の色調調整層としてTi層(平均厚み30nm)を形成して、繊維基材と第2の色調調整層との積層体を得た。
繊維基材と第2の色調調整層との積層体を真空装置内に設置し、8.0×10−4Pa以下となるまで真空排気した。続いて、アルゴンガスを導入して、DCマグネトロンスパッタリング法により、第2の色調調整層の繊維基材とは反対の表面上に、第1の色調調整層としてSiO0.5層(平均厚み35nm)を形成して、積層シートを得た。
第1の色調調整層(SiO0.5層)の平均厚みを、表1に示すように変更したこと以外は、実施例2と同様にして、積層シートを得た。
第1の色調調整層(SiO0.5層)及び第2の色調調整層の平均厚みを表1に示すように変更したこと、第2の色調調整層としてAg層を形成したこと以外は、実施例2と同様にして、積層シートを得た。
色調調整層(第1の色調調整層)としてTiO0.1層を形成したこと、色調調整層の平均厚みを表1に示すように変更したこと以外は、参考例1と同様にして積層シートを得た。
参考例1におけるポリエステル繊維基材(マスダ社製「ひかるげんじTM−3001 E21」)を、比較例1の評価対象とした。比較例1では、第1の色調調整層及び第2の色調調整層の双方を形成しなかった。
参考例1における繊維基材(ポリエステル繊維基材)を用意した。この繊維基材の一方の面に、青色顔料を含む塗料を塗布して、着色層(光透過性を有しない色調調整層、平均厚み15μm)を形成し、第2の表面側に着色層が配置されている積層シートを得た。なお、比較例2の着色層(光透過性を有しない色調調整層)の可視光透過率は、1%未満であった。着色層は、光透過性を有していなかった。
炭素質基材として、炭素繊維(目付量200g/m2、フィラメント径7μm、密度12.5本/インチ)が綾織で織られた織物である炭素繊維基材(三菱ケミカル社製「TR3523 M」、厚さ0.21mm)を用いた。炭素質基材を真空装置内に設置し、5.0×10−4Pa以下となるまで真空排気した。続いて、アルゴンガスを導入して、DCマグネトロンスパッタリング法により、炭素質基材の表面上に、第1の色調調整層としてSiO0.5層(平均厚み15nm)を形成して、積層シートを得た。
第2の色調調整層の形成:
参考例6における炭素質基材を用意した。炭素質基材を真空装置内に設置し、5.0×10−4Pa以下となるまで真空排気した。続いて、アルゴンガスを導入して、DCマグネトロンスパッタリング法により、炭素質基材の表面上に、第2の色調調整層としてTi層(平均厚み30nm)を形成して、炭素質基材と第2の色調調整層との積層体を得た。
炭素質基材と第2の色調調整層との積層体を真空装置内に設置し、5.0×10−4Pa以下となるまで真空排気した。続いて、アルゴンガスを導入して、DCマグネトロンスパッタリング法により、第2の色調調整層の炭素質基材とは反対の表面上に、第1の色調調整層としてSiO0.5層(平均厚み35nm)を形成して、積層シートを得た。
第1の色調調整層(SiO0.5層)の厚みを、表2,3に示すように変更したこと以外は、実施例7と同様にして、積層シートを得た。
参考例6における炭素質基材を用意した。この基材の表面上に、参考例6と同様にして、第1の色調調整層としてTiO0.1層(平均厚み30nm)を形成して、積層シートを得た。参考例14では、第2の色調調整層を形成しなかった。
参考例6における炭素質基材(三菱ケミカル社製「TR3523 M」、厚さ0.21mm)を、比較例3の評価対象とした。比較例3では、第1の色調調整層及び第2の色調調整層の双方を形成しなかった。
参考例6における炭素質基材を用意した。この炭素質基材の一方の面に、青色顔料を含む塗料を塗布して、着色層(光透過性を有しない色調調整層、平均厚み15μm)を形成し、第2の表面側に着色層が配置されている積層シートを得た。なお、比較例4の着色層(光透過性を有しない色調調整層)の可視光透過率は、1%未満であった。着色層は、光透過性を有していなかった。
参考例6における炭素質基材を用意した。この炭素質基材の一方の面に、赤色染料(Pigment Red 254)を含む塗料を塗布して、着色層(光透過性を有しない色調調整層、平均厚み10μm)を形成し、第2の表面側に着色層が配置されている積層シートを得た。なお、比較例5の着色層(光透過性を有しない色調調整層)の可視光透過率は、1%未満であった。着色層は、光透過性を有していなかった。
(1)色差
分光光度計(日立ハイテク社製「U−4100」)を用いて、JIS Z8781−4:2013に準拠して、積層シート(参考例1、実施例2〜4、参考例5,6、実施例7〜13、参考例14及び比較例2,4,5)の第2の表面、及び繊維基材(比較例1,3)の表面のL*a*b*表色系におけるL*、a*、b*を求めた。
上記(1)の測定において、明度L*を評価した。JIS Z8781−4:2013に準拠して、積層シートの第2の表面の明度L*と積層シートの繊維基材の表面の明度L*との差を求めた。
参考例1、実施例2〜4、参考例5,6、実施例7〜13、参考例14及び比較例2,4,5の、積層シートの第2の表面の可視光反射率と、繊維基材表面の可視光反射率との差を求めた。
積層シートの第2の表面(参考例1、実施例2〜4、参考例5,6、実施例7〜13、参考例14及び比較例2,4,5)、及び繊維基材の表面(比較例1,3)の色目を目視にて確認した。色目は、JIS Z8102:2001に準拠して、分類した。
参考例1、実施例2〜4、参考例5及び比較例2では、積層シートの第2の表面を観察したときに、繊維基材に用いたポリエステル繊維が有する凹凸形状が損なわれていないか及び表面模様が視認されるか、目視にて確認した。参考例6、実施例7〜13、参考例14及び比較例4,5では、積層シートの第2の表面を観察したときに、炭素質基材に用いた炭素繊維が有する凹凸形状が損なわれていないか及び表面模様が視認されるか、目視にて確認した。
○:凹凸形状が損なわれていない
×:凹凸形状が損なわれている
○:表面模様が視認される
×:表面模様が視認されない
積層シート(参考例1、実施例2〜4、参考例5,6、実施例7〜13、参考例14及び比較例2,4,5)の第2の表面、及び繊維基材(比較例1,3)の表面を観察したときに、金属光沢感を有するか、目視にて確認した。
○○:金属光沢感がかなりある
○:金属光沢感がある
△:金属光沢感がわずかにある
×:金属光沢感がない
積層シート(参考例1、実施例2〜4、参考例5,6、実施例7〜13、参考例14及び比較例2,4,5)の第2の表面、及び繊維基材(比較例1,3)の表面を観察したときに、繊維基材に用いたポリエステル繊維又は炭素繊維が有する光沢感が損なわれていないか、目視にて確認した。
○:光沢感がある
×:光沢感がない
分光光度計(日立ハイテク社製「U−4100」)を用いて、第1の色調調整層(参考例1、実施例2〜4、参考例5,6、実施例7〜13、参考例14)、及び着色層(比較例2,4,5)の可視光透過率を求めた。
積層シート(参考例1、実施例2〜4、参考例5,6、実施例7〜13、参考例14及び比較例2,4,5)の第2の表面に幅15mm、長さ30mmの粘着テープ(積水化学工業製「セキスイセロテープNo252」)を貼り、2kgの圧着ローラーを一往復させ、貼りで張り合わせたのち、粘着テープを剥がした。剥がした粘着テープ上に第1の色調調整層又は第2の色調調整層が付着しているか否かを確認した。
○:粘着テープに第1の色調調整層又は第2の色調調整層が付着していない
×:粘着テープに第1の色調調整層又は第2の色調調整層が付着している
1a…第1の表面
1b…第2の表面
2…繊維基材
3…第1の色調調整層
4…第2の色調調整層
Claims (15)
- 繊維基材と、該繊維基材の表面上に配置されている第2の色調調整層と、該第2の色調調整層の該繊維基材側とは反対の表面上に配置されている第1の色調調整層とを備える積層シートであり、
前記積層シートは、第1の表面と、該第1の表面とは反対側に第2の表面とを有し、
前記積層シートの前記第1の表面側に前記繊維基材が配置されており、前記積層シートの前記第2の表面側に前記第1の色調調整層が配置されており、
前記第1の色調調整層は、前記積層シートの前記第2の表面の色調を、前記繊維基材の表面の色調とは異なるようにする性質を有する層であり、
前記第1の色調調整層は、MOx、又はMNxを含む層を有し、
MOxの場合には、Mはケイ素を表し、かつxは0以上0.5以下の数を表すか、又は、Mはチタンを表し、かつxは0以上0.1以下の数を表し、
MNxの場合には、Mはn価の金属又は半金属を表し、かつxは0以上n/3未満の数を表し、
前記第1の色調調整層は、光透過性を有する、積層シート。 - 繊維基材と、該繊維基材の表面上に配置されている第2の色調調整層と、該第2の色調調整層の該繊維基材側とは反対の表面上に配置されている第1の色調調整層とを備える積層シートであり、
前記積層シートは、第1の表面と、該第1の表面とは反対側に第2の表面とを有し、
前記積層シートの前記第1の表面側に前記繊維基材が配置されており、前記積層シートの前記第2の表面側に前記第1の色調調整層が配置されており、
前記第1の色調調整層は、MOx、又はMNxを含む層を有し、
MOxの場合には、Mはケイ素を表し、かつxは0以上0.5以下の数を表すか、又は、Mはチタンを表し、かつxは0以上0.1以下の数を表し、
MNxの場合には、Mはn価の金属又は半金属を表し、かつxは0以上n/3未満の数を表し、
前記第1の色調調整層は、光透過性を有する、積層シート。 - 前記第1の色調調整層は顔料を含まず、かつ、前記第1の色調調整層は染料を含まない、請求項1又は2に記載の積層シート。
- 前記繊維基材は合成繊維基材である、請求項1〜3のいずれか1項に記載の積層シート。
- MNxにおけるMは、ケイ素、ゲルマニウム、ガリウム、亜鉛、銀、金、チタン、アルミニウム、スズ、銅、鉄、モリブデン、ニオブ、又はインジウムである、請求項1〜4のいずれか1項に記載の積層シート。
- 前記第1の色調調整層の平均厚みが1nm以上200nm以下である、請求項1〜5のいずれか1項に記載の積層シート。
- 前記第1の色調調整層の可視光透過率が8%以上である、請求項1〜6のいずれか1項に記載の積層シート。
- 前記積層シートの前記第2の表面と、前記繊維基材の表面との、JIS Z8781−4:2013に準拠して測定されるL*a*b*表色系における色差ΔE*abが10以上である、請求項1〜7のいずれか1項に記載の積層シート。
- JIS Z8781−4:2013に準拠したL*a*b*表色系における明度の測定において、前記積層シートの前記第2の表面の明度L*が、前記繊維基材の表面の明度L*よりも5以上高い、請求項1〜8のいずれか1項に記載の積層シート。
- 前記第1の色調調整層に最も多く含まれる金属元素又は半金属元素が、ケイ素であり、
前記第2の色調調整層に最も多く含まれる金属元素又は半金属元素が、ゲルマニウム、ガリウム、亜鉛、銀、金、チタン、アルミニウム、スズ、銅、鉄、モリブデン、ニオブ、又はインジウムである、請求項1〜9のいずれか1項に記載の積層シート。 - 繊維と、該繊維の表面上に配置されている第2の色調調整層と、該第2の色調調整層の該繊維側とは反対の表面上に配置されている第1の色調調整層とを備えるコーティング繊維であり、
前記第1の色調調整層は、MOx、又はMNxを含む層を有し、
MOxの場合には、Mはケイ素を表し、かつxは0以上0.5以下の数を表すか、又は、Mはチタンを表し、かつxは0以上0.1以下の数を表し、
MNxの場合には、Mはn価の金属又は半金属を表し、かつxは0以上n/3未満の数を表し、
前記第1の色調調整層は、光透過性を有する、コーティング繊維。 - 複数の繊維を有し、
前記繊維が請求項11に記載のコーティング繊維を含む、コーティング繊維束。 - 請求項1〜10のいずれか1項に記載の積層シートを含む、繊維強化プラスチック。
- 請求項11に記載のコーティング繊維を含む、繊維強化プラスチック。
- 請求項12に記載のコーティング繊維束を含む、繊維強化プラスチック。
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US (1) | US20200247088A1 (ja) |
JP (2) | JP6522863B1 (ja) |
KR (1) | KR20200039663A (ja) |
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EP3756881A4 (en) * | 2018-02-22 | 2021-12-29 | Sekisui Chemical Co., Ltd. | Laminate sheet |
JPWO2020059725A1 (ja) * | 2018-09-18 | 2021-08-30 | 積水化学工業株式会社 | 繊維シート |
US11376812B2 (en) | 2020-02-11 | 2022-07-05 | Helicoid Industries Inc. | Shock and impact resistant structures |
DE102020128724A1 (de) | 2020-11-02 | 2022-05-05 | Bayerische Motoren Werke Aktiengesellschaft | Sichtbauteil für ein Kraftfahrzeug |
US11852297B2 (en) | 2021-06-01 | 2023-12-26 | Helicoid Industries Inc. | Containers and methods for protecting pressure vessels |
US11346499B1 (en) | 2021-06-01 | 2022-05-31 | Helicoid Industries Inc. | Containers and methods for protecting pressure vessels |
WO2024006078A1 (en) | 2022-06-27 | 2024-01-04 | Helicoid Industries Inc. | High impact-resistant, reinforced fiber for leading edge protection of aerodynamic structures |
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- 2018-08-09 CN CN201880051582.2A patent/CN110997311A/zh active Pending
- 2018-08-09 KR KR1020207002154A patent/KR20200039663A/ko not_active Application Discontinuation
- 2018-08-09 US US16/637,253 patent/US20200247088A1/en not_active Abandoned
- 2018-08-09 JP JP2018549592A patent/JP6522863B1/ja active Active
- 2018-08-09 WO PCT/JP2018/029952 patent/WO2019031589A1/ja active Application Filing
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KR20200039663A (ko) | 2020-04-16 |
JPWO2019031589A1 (ja) | 2019-11-07 |
US20200247088A1 (en) | 2020-08-06 |
WO2019031589A1 (ja) | 2019-02-14 |
CN110997311A (zh) | 2020-04-10 |
JP2019162879A (ja) | 2019-09-26 |
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