JP6138463B2 - 乳化剤とグルテンを反応させてなる組成物の製造方法 - Google Patents
乳化剤とグルテンを反応させてなる組成物の製造方法 Download PDFInfo
- Publication number
- JP6138463B2 JP6138463B2 JP2012255605A JP2012255605A JP6138463B2 JP 6138463 B2 JP6138463 B2 JP 6138463B2 JP 2012255605 A JP2012255605 A JP 2012255605A JP 2012255605 A JP2012255605 A JP 2012255605A JP 6138463 B2 JP6138463 B2 JP 6138463B2
- Authority
- JP
- Japan
- Prior art keywords
- emulsifier
- gluten
- present
- weight
- composition
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- 239000003995 emulsifying agent Substances 0.000 title claims description 73
- 108010068370 Glutens Proteins 0.000 title claims description 60
- 235000021312 gluten Nutrition 0.000 title claims description 60
- 239000000203 mixture Substances 0.000 title claims description 46
- 238000004519 manufacturing process Methods 0.000 title description 10
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 21
- 238000000034 method Methods 0.000 claims description 18
- 235000010956 sodium stearoyl-2-lactylate Nutrition 0.000 claims description 17
- KNYAZNABVSEZDS-UHFFFAOYSA-M sodium;2-octadecanoyloxypropanoate Chemical compound [Na+].CCCCCCCCCCCCCCCCCC(=O)OC(C)C([O-])=O KNYAZNABVSEZDS-UHFFFAOYSA-M 0.000 claims description 17
- OEUVSBXAMBLPES-UHFFFAOYSA-L calcium stearoyl-2-lactylate Chemical compound [Ca+2].CCCCCCCCCCCCCCCCCC(=O)OC(C)C(=O)OC(C)C([O-])=O.CCCCCCCCCCCCCCCCCC(=O)OC(C)C(=O)OC(C)C([O-])=O OEUVSBXAMBLPES-UHFFFAOYSA-L 0.000 claims 1
- 235000013305 food Nutrition 0.000 description 19
- 239000000047 product Substances 0.000 description 19
- HEDRZPFGACZZDS-UHFFFAOYSA-N Chloroform Chemical compound ClC(Cl)Cl HEDRZPFGACZZDS-UHFFFAOYSA-N 0.000 description 10
- 235000008429 bread Nutrition 0.000 description 10
- 239000000284 extract Substances 0.000 description 10
- 238000003860 storage Methods 0.000 description 9
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 8
- 230000000052 comparative effect Effects 0.000 description 8
- JVTAAEKCZFNVCJ-UHFFFAOYSA-N lactic acid Chemical compound CC(O)C(O)=O JVTAAEKCZFNVCJ-UHFFFAOYSA-N 0.000 description 8
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 6
- 239000007795 chemical reaction product Substances 0.000 description 6
- 238000002156 mixing Methods 0.000 description 6
- 239000003795 chemical substances by application Substances 0.000 description 5
- 235000013312 flour Nutrition 0.000 description 5
- 239000003495 polar organic solvent Substances 0.000 description 5
- GLAVXDCIRMNZLL-UHFFFAOYSA-N C(C(O)C)(=O)O.C(CCCCCCCCCCCCCCCCC)(=O)[Na] Chemical compound C(C(O)C)(=O)O.C(CCCCCCCCCCCCCCCCC)(=O)[Na] GLAVXDCIRMNZLL-UHFFFAOYSA-N 0.000 description 4
- 241000209140 Triticum Species 0.000 description 4
- 235000021307 Triticum Nutrition 0.000 description 4
- 235000013361 beverage Nutrition 0.000 description 4
- 239000011230 binding agent Substances 0.000 description 4
- 150000002148 esters Chemical class 0.000 description 4
- 239000004310 lactic acid Substances 0.000 description 4
- 235000014655 lactic acid Nutrition 0.000 description 4
- 229910052757 nitrogen Inorganic materials 0.000 description 4
- 239000003960 organic solvent Substances 0.000 description 4
- 235000018102 proteins Nutrition 0.000 description 4
- 108090000623 proteins and genes Proteins 0.000 description 4
- 102000004169 proteins and genes Human genes 0.000 description 4
- 229920002472 Starch Polymers 0.000 description 3
- 235000021355 Stearic acid Nutrition 0.000 description 3
- WORJEOGGNQDSOE-UHFFFAOYSA-N chloroform;methanol Chemical compound OC.ClC(Cl)Cl WORJEOGGNQDSOE-UHFFFAOYSA-N 0.000 description 3
- 238000001035 drying Methods 0.000 description 3
- 239000012046 mixed solvent Substances 0.000 description 3
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 description 3
- OQCDKBAXFALNLD-UHFFFAOYSA-N octadecanoic acid Natural products CCCCCCCC(C)CCCCCCCCC(O)=O OQCDKBAXFALNLD-UHFFFAOYSA-N 0.000 description 3
- 239000000843 powder Substances 0.000 description 3
- 239000008107 starch Substances 0.000 description 3
- 235000019698 starch Nutrition 0.000 description 3
- 239000008117 stearic acid Substances 0.000 description 3
- -1 sucrose fatty acid esters Chemical class 0.000 description 3
- LDVVTQMJQSCDMK-UHFFFAOYSA-N 1,3-dihydroxypropan-2-yl formate Chemical compound OCC(CO)OC=O LDVVTQMJQSCDMK-UHFFFAOYSA-N 0.000 description 2
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 2
- FDKAAIFOPLCYAM-UHFFFAOYSA-M C(C(O)C)(=O)[O-].C(CCCCCCCCCCCCCCCCC)(=O)[Ca+] Chemical compound C(C(O)C)(=O)[O-].C(CCCCCCCCCCCCCCCCC)(=O)[Ca+] FDKAAIFOPLCYAM-UHFFFAOYSA-M 0.000 description 2
- 238000007696 Kjeldahl method Methods 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 235000009508 confectionery Nutrition 0.000 description 2
- 238000011156 evaluation Methods 0.000 description 2
- 235000010037 flour treatment agent Nutrition 0.000 description 2
- IPCSVZSSVZVIGE-UHFFFAOYSA-N hexadecanoic acid Chemical compound CCCCCCCCCCCCCCCC(O)=O IPCSVZSSVZVIGE-UHFFFAOYSA-N 0.000 description 2
- 230000000887 hydrating effect Effects 0.000 description 2
- 238000010907 mechanical stirring Methods 0.000 description 2
- 238000011002 quantification Methods 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- KDYFGRWQOYBRFD-UHFFFAOYSA-N succinic acid Chemical compound OC(=O)CCC(O)=O KDYFGRWQOYBRFD-UHFFFAOYSA-N 0.000 description 2
- DNISEZBAYYIQFB-PHDIDXHHSA-N (2r,3r)-2,3-diacetyloxybutanedioic acid Chemical compound CC(=O)O[C@@H](C(O)=O)[C@H](C(O)=O)OC(C)=O DNISEZBAYYIQFB-PHDIDXHHSA-N 0.000 description 1
- OZZQHCBFUVFZGT-BKLSDQPFSA-N (2s)-2-(2-hydroxypropanoyloxy)propanoic acid Chemical compound CC(O)C(=O)O[C@@H](C)C(O)=O OZZQHCBFUVFZGT-BKLSDQPFSA-N 0.000 description 1
- CYDQOEWLBCCFJZ-UHFFFAOYSA-N 4-(4-fluorophenyl)oxane-4-carboxylic acid Chemical compound C=1C=C(F)C=CC=1C1(C(=O)O)CCOCC1 CYDQOEWLBCCFJZ-UHFFFAOYSA-N 0.000 description 1
- 240000007594 Oryza sativa Species 0.000 description 1
- 235000007164 Oryza sativa Nutrition 0.000 description 1
- 235000021314 Palmitic acid Nutrition 0.000 description 1
- 239000004698 Polyethylene Substances 0.000 description 1
- 229930006000 Sucrose Natural products 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 230000032683 aging Effects 0.000 description 1
- 229910021529 ammonia Inorganic materials 0.000 description 1
- 239000012874 anionic emulsifier Substances 0.000 description 1
- 125000000129 anionic group Chemical group 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- OGBUMNBNEWYMNJ-UHFFFAOYSA-N batilol Chemical class CCCCCCCCCCCCCCCCCCOCC(O)CO OGBUMNBNEWYMNJ-UHFFFAOYSA-N 0.000 description 1
- 235000012970 cakes Nutrition 0.000 description 1
- 238000004364 calculation method Methods 0.000 description 1
- 235000013339 cereals Nutrition 0.000 description 1
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 1
- 238000007596 consolidation process Methods 0.000 description 1
- 235000014510 cooky Nutrition 0.000 description 1
- 235000014113 dietary fatty acids Nutrition 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 239000000839 emulsion Substances 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000003925 fat Substances 0.000 description 1
- 229930195729 fatty acid Natural products 0.000 description 1
- 239000000194 fatty acid Substances 0.000 description 1
- 235000021588 free fatty acids Nutrition 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 238000000265 homogenisation Methods 0.000 description 1
- 230000036571 hydration Effects 0.000 description 1
- 238000006703 hydration reaction Methods 0.000 description 1
- 238000009413 insulation Methods 0.000 description 1
- 238000004898 kneading Methods 0.000 description 1
- JJTUDXZGHPGLLC-UHFFFAOYSA-N lactide Chemical compound CC1OC(=O)C(C)OC1=O JJTUDXZGHPGLLC-UHFFFAOYSA-N 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- WQEPLUUGTLDZJY-UHFFFAOYSA-N n-Pentadecanoic acid Natural products CCCCCCCCCCCCCCC(O)=O WQEPLUUGTLDZJY-UHFFFAOYSA-N 0.000 description 1
- 230000003472 neutralizing effect Effects 0.000 description 1
- 239000012454 non-polar solvent Substances 0.000 description 1
- 235000012149 noodles Nutrition 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 229920000573 polyethylene Polymers 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 235000009566 rice Nutrition 0.000 description 1
- 239000001540 sodium lactate Substances 0.000 description 1
- 229940005581 sodium lactate Drugs 0.000 description 1
- 235000011088 sodium lactate Nutrition 0.000 description 1
- 159000000000 sodium salts Chemical class 0.000 description 1
- 238000007711 solidification Methods 0.000 description 1
- 230000008023 solidification Effects 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 238000001694 spray drying Methods 0.000 description 1
- 239000003381 stabilizer Substances 0.000 description 1
- 125000003696 stearoyl group Chemical group O=C([*])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
- 239000001384 succinic acid Substances 0.000 description 1
- 239000005720 sucrose Substances 0.000 description 1
Landscapes
- Bakery Products And Manufacturing Methods Therefor (AREA)
- General Preparation And Processing Of Foods (AREA)
- Noodles (AREA)
Description
(1)乳化剤と生グルテンおよび/または活性グルテンとを混合し、得られる混合物の水分含量を60〜80重量%として、乳化剤と生グルテンおよび/または活性グルテンとを反応させることを含んでなる、乳化剤組成物の製造方法。
(2)組成物が食品の品質改良剤である、上記(1)に記載の方法。
(3)上記(1)に記載の方法により得られる組成物を含んでなる、食品の品質改良剤。
(4)乳化剤と生グルテンおよび/または活性グルテンとを混合し、得られる混合物の水分含量を60〜80重量%として、乳化剤と生グルテンおよび/または活性グルテンとを反応させることを含んでなる、乳化剤の固結防止方法。
乳化剤とグルテンとの反応生成物を含むことが推定される組成物(以下、「結合物含有組成物」という)20gに、200mLのクロロホルムを加え、機械的攪拌により常温で20分間抽出し、得られた抽出物をろ紙(アドバンテック社製、No.50)を用いて減圧ろ過する。その後、残渣に再度クロロホルム200mLを加え、同様の操作を繰り返す。2回の抽出液を合わせ、減圧濃縮し、次いで、重量変化が見られなくなるまで60〜70℃で乾燥する。次に、抽出物中のタンパク質含量を算出する。抽出物中のタンパク質量は、例えば、ミクロケルダール法により全窒素を測定し、全窒素量に係数5.7を乗じて求めることができる。遊離乳化剤量は、全抽出物量からタンパク質量を差し引いた値として求めることができる。
クロロホルムの代わりにクロロホルム−メタノール混合溶媒(容量比で2:1)を用いる以外は、(a)と同様の操作を行い、極性有機溶媒中の乳化剤(全乳化剤)の量を算出する。すなわち、乳化剤とグルテンとの結合物を含むことが推定される組成物20gに、200mLのクロロホルム−メタノール混合溶媒(容量比で2:1)を加え、機械的攪拌により常温で20分間抽出し、得られた抽出物をろ紙(アドバンテック社製、No.50)を用いて減圧ろ過する。その後、残渣に再度クロロホルム200mLを加え、同様の操作を繰り返す。2回の抽出液を合わせ、減圧濃縮し、次いで、重量変化が見られなくなるまで60〜70℃で乾燥する。次に、抽出物中のタンパク質含量を算出する。抽出物中のタンパク質量は、例えば、ミクロケルダール法により全窒素を測定し、全窒素量に係数5.7を乗じて求めることができる。遊離乳化剤と結合物の量の和は、全抽出物量からタンパク質量を差し引いた値として求めることができる。
結合物の量は、(b)で求められた遊離乳化剤と結合物の量の和から、(a)で求められた遊離乳化剤量を差し引くことにより求めることができる。
ステアロイル乳酸ナトリウム70gを水300gと混合し、ステアロイル乳酸ナトリウム水溶液を得た。小麦粉と水を混合し、澱粉をのぞいて得た生グルテン(水分含量67重量%)1910gと上記水溶液とを60℃に加熱し、ミキサーボウルを用いて均一になるまで20分間混合して、ステアロイル乳酸ナトリウムと生グルテンとの反応生成物2279g(水分含量69重量%)を得た。その後、反応生成物を、水分含量7%になるまで気流乾燥して、760gの組成物(乾燥物)を得た。
本実施例では、実施例1で得られた実験例1の乾燥物を用いて製パンした場合のパンの品質を確認した。
Claims (1)
- 乳化剤と生グルテンおよび/または活性グルテンとを混合し、得られる混合物の水分含量を60〜80重量%として、乳化剤と生グルテンおよび/または活性グルテンとを反応させることを含んでなり、該乳化剤がステアロイル乳酸ナトリウムまたはステアロイル乳酸カルシウムである、乳化剤の固結防止方法。
Priority Applications (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP2012255605A JP6138463B2 (ja) | 2012-11-21 | 2012-11-21 | 乳化剤とグルテンを反応させてなる組成物の製造方法 |
CN201310446352.5A CN103828881B (zh) | 2012-11-21 | 2013-09-26 | 使乳化剂与面筋反应而成的组合物的制造方法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP2012255605A JP6138463B2 (ja) | 2012-11-21 | 2012-11-21 | 乳化剤とグルテンを反応させてなる組成物の製造方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
JP2014100113A JP2014100113A (ja) | 2014-06-05 |
JP6138463B2 true JP6138463B2 (ja) | 2017-05-31 |
Family
ID=50793033
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP2012255605A Active JP6138463B2 (ja) | 2012-11-21 | 2012-11-21 | 乳化剤とグルテンを反応させてなる組成物の製造方法 |
Country Status (2)
Country | Link |
---|---|
JP (1) | JP6138463B2 (ja) |
CN (1) | CN103828881B (ja) |
Family Cites Families (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3880824A (en) * | 1972-07-18 | 1975-04-29 | Far Mar Co | Gluten lipid complexes and process for preparing same |
US3870799A (en) * | 1974-02-28 | 1975-03-11 | Patterson Co C | Dough conditioning composition and method |
US4035519A (en) * | 1975-05-22 | 1977-07-12 | General Mills Chemicals, Inc. | Process for preparation of emulsified wheat gluten |
US4200569A (en) * | 1978-04-17 | 1980-04-29 | John Labatt Limited | Wheat-based lipoprotein complexes and methods of making and using same |
JPS56158044A (en) * | 1980-05-12 | 1981-12-05 | Riken Vitamin Oil Co Ltd | Production of quality improving agent of novel starch containing food |
JPS61162127A (ja) * | 1985-01-12 | 1986-07-22 | 協和醗酵工業株式会社 | 生地改良剤 |
JP5242219B2 (ja) * | 2008-03-31 | 2013-07-24 | 花王株式会社 | 乳化油脂組成物 |
JP5859282B2 (ja) * | 2010-11-26 | 2016-02-10 | 株式会社Adeka | 製パン練り込み用油中水型乳化油脂組成物 |
-
2012
- 2012-11-21 JP JP2012255605A patent/JP6138463B2/ja active Active
-
2013
- 2013-09-26 CN CN201310446352.5A patent/CN103828881B/zh active Active
Also Published As
Publication number | Publication date |
---|---|
CN103828881B (zh) | 2019-06-11 |
CN103828881A (zh) | 2014-06-04 |
JP2014100113A (ja) | 2014-06-05 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
CN102845540B (zh) | 一种高脂粉末油脂及其制备方法 | |
CN108208066A (zh) | 复配乳化剂及其制备方法 | |
CN105555149B (zh) | 面条用松散改良剂的制造方法 | |
RU2583071C2 (ru) | Способ получения сухой смеси для блинчиков | |
JPH0527368B2 (ja) | ||
CN105076946A (zh) | 一种方便粉条的制作工艺 | |
JPWO2016132752A1 (ja) | 麺用品質改良剤 | |
JP7102100B2 (ja) | 粉末状小麦タンパク質及びその製造方法 | |
CA2363266A1 (en) | New flavoured improver for baking applications | |
CN104363771A (zh) | 硬脂酰乳酸钠制剂 | |
JP6138463B2 (ja) | 乳化剤とグルテンを反応させてなる組成物の製造方法 | |
AU2017220217B2 (en) | Method for manufacturing modified gluten | |
US20080233240A1 (en) | Bread Improver Comprising Emulsifier and Stabiliser | |
KR101578781B1 (ko) | 감자 전분을 함유하는 만두피 반죽용 프리믹스 조성물 | |
CN109380640A (zh) | 一种曲奇包馅用果味酱 | |
CN108013089A (zh) | 粉状糕点起泡剂及其制备方法 | |
CN109953252B (zh) | 淀粉脂质复合物及制备方法 | |
JPS61285944A (ja) | パン類改良剤 | |
TW201633929A (zh) | 穀類加工食品用鬆散改良劑及穀類加工食品 | |
JPS6214253B2 (ja) | ||
US20160262431A1 (en) | Binder composition comprising gas | |
JP6298282B2 (ja) | 中華麺用穀粉組成物およびその製造方法 | |
JP2004329154A (ja) | ケーキ生地用の粉末状乳化起泡剤、ケーキ用ミックス粉、及びこれを用いたケーキ | |
JP7102174B2 (ja) | ベーカリー製品用ミックス粉 | |
JP6130215B2 (ja) | 春巻皮の製造方法 |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
A621 | Written request for application examination |
Free format text: JAPANESE INTERMEDIATE CODE: A621 Effective date: 20151020 |
|
A977 | Report on retrieval |
Free format text: JAPANESE INTERMEDIATE CODE: A971007 Effective date: 20160809 |
|
A131 | Notification of reasons for refusal |
Free format text: JAPANESE INTERMEDIATE CODE: A131 Effective date: 20160909 |
|
RD03 | Notification of appointment of power of attorney |
Free format text: JAPANESE INTERMEDIATE CODE: A7423 Effective date: 20161018 |
|
A521 | Request for written amendment filed |
Free format text: JAPANESE INTERMEDIATE CODE: A523 Effective date: 20161019 |
|
A02 | Decision of refusal |
Free format text: JAPANESE INTERMEDIATE CODE: A02 Effective date: 20170106 |
|
A521 | Request for written amendment filed |
Free format text: JAPANESE INTERMEDIATE CODE: A523 Effective date: 20170307 |
|
A911 | Transfer to examiner for re-examination before appeal (zenchi) |
Free format text: JAPANESE INTERMEDIATE CODE: A911 Effective date: 20170315 |
|
TRDD | Decision of grant or rejection written | ||
A01 | Written decision to grant a patent or to grant a registration (utility model) |
Free format text: JAPANESE INTERMEDIATE CODE: A01 Effective date: 20170404 |
|
A61 | First payment of annual fees (during grant procedure) |
Free format text: JAPANESE INTERMEDIATE CODE: A61 Effective date: 20170426 |
|
R150 | Certificate of patent or registration of utility model |
Ref document number: 6138463 Country of ref document: JP Free format text: JAPANESE INTERMEDIATE CODE: R150 |
|
R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |