JP6006222B2 - 環状ポリアミン及び環状／非環状ポリアミン混合物を製造するための窒素含有化合物のアミノ基転移 - Google Patents
環状ポリアミン及び環状／非環状ポリアミン混合物を製造するための窒素含有化合物のアミノ基転移 Download PDFInfo
- Publication number
- JP6006222B2 JP6006222B2 JP2013538757A JP2013538757A JP6006222B2 JP 6006222 B2 JP6006222 B2 JP 6006222B2 JP 2013538757 A JP2013538757 A JP 2013538757A JP 2013538757 A JP2013538757 A JP 2013538757A JP 6006222 B2 JP6006222 B2 JP 6006222B2
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- Japan
- Prior art keywords
- spacing
- nitrogen
- mixture
- reaction
- cyclic
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D295/00—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms
- C07D295/02—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms containing only hydrogen and carbon atoms in addition to the ring hetero elements
- C07D295/023—Preparation; Separation; Stabilisation; Use of additives
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D243/00—Heterocyclic compounds containing seven-membered rings having two nitrogen atoms as the only ring hetero atoms
- C07D243/06—Heterocyclic compounds containing seven-membered rings having two nitrogen atoms as the only ring hetero atoms having the nitrogen atoms in positions 1 and 4
- C07D243/08—Heterocyclic compounds containing seven-membered rings having two nitrogen atoms as the only ring hetero atoms having the nitrogen atoms in positions 1 and 4 not condensed with other rings
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D295/00—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms
- C07D295/04—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms
- C07D295/12—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms substituted by singly or doubly bound nitrogen atoms
- C07D295/125—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms substituted by singly or doubly bound nitrogen atoms with the ring nitrogen atoms and the substituent nitrogen atoms attached to the same carbon chain, which is not interrupted by carbocyclic rings
- C07D295/13—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms substituted by singly or doubly bound nitrogen atoms with the ring nitrogen atoms and the substituent nitrogen atoms attached to the same carbon chain, which is not interrupted by carbocyclic rings to an acyclic saturated chain
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US41202610P | 2010-11-10 | 2010-11-10 | |
| US61/412,026 | 2010-11-10 | ||
| PCT/US2011/057045 WO2012064483A1 (en) | 2010-11-10 | 2011-10-20 | Transamination of nitrogen-containing compounds to make cyclic and cyclic/acyclic polyamine mixtures |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2014501715A JP2014501715A (ja) | 2014-01-23 |
| JP2014501715A5 JP2014501715A5 (cg-RX-API-DMAC7.html) | 2014-12-11 |
| JP6006222B2 true JP6006222B2 (ja) | 2016-10-12 |
Family
ID=45044698
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2013538757A Expired - Fee Related JP6006222B2 (ja) | 2010-11-10 | 2011-10-20 | 環状ポリアミン及び環状／非環状ポリアミン混合物を製造するための窒素含有化合物のアミノ基転移 |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US8993759B2 (cg-RX-API-DMAC7.html) |
| EP (1) | EP2638020B1 (cg-RX-API-DMAC7.html) |
| JP (1) | JP6006222B2 (cg-RX-API-DMAC7.html) |
| CN (1) | CN103261174B (cg-RX-API-DMAC7.html) |
| BR (1) | BR112013011672A2 (cg-RX-API-DMAC7.html) |
| WO (1) | WO2012064483A1 (cg-RX-API-DMAC7.html) |
Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP3725767B1 (en) | 2013-10-17 | 2022-03-30 | Swimc Llc | Di(amido(alkyl)phenol) compounds and polymers formed therefrom |
| JP2017500386A (ja) * | 2013-12-02 | 2017-01-05 | ダウ グローバル テクノロジーズ エルエルシー | 高分子量の分岐鎖非環式ポリアルキレンアミン及びその混合物の調製 |
| BR112016026342B1 (pt) | 2014-05-19 | 2022-03-03 | Swimc Llc | Artigo |
| WO2016204981A1 (en) | 2015-06-19 | 2016-12-22 | Dow Global Technologies Llc | Autocatalytic polyol useful for polyurethane foam manufacture |
| JP6970129B2 (ja) | 2016-06-13 | 2021-11-24 | ダウ グローバル テクノロジーズ エルエルシー | 自己触媒性ポリオール |
| MX2022014897A (es) | 2020-06-17 | 2023-01-04 | Basf Se | Copolimeros anfifilicos alcoxilados de polietileno/propilenimina para formulaciones de detergentes multibeneficio. |
Family Cites Families (39)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2267686A (en) * | 1938-08-08 | 1941-12-23 | Monsanto Chemicals | Manufacture of piperazine |
| US2454404A (en) * | 1942-10-03 | 1948-11-23 | American Cyanamid Co | Preparation of piperazine |
| US2809195A (en) * | 1955-08-30 | 1957-10-08 | Du Pont | Synthesis of piperazine and substituted piperazines |
| US2901482A (en) * | 1956-07-23 | 1959-08-25 | Dow Chemical Co | Manufacturing process for piperazine |
| US3120524A (en) * | 1958-12-15 | 1964-02-04 | Jefferson Chem Co Inc | Method for preparing n-alkyl substituted piperazines |
| US3285920A (en) * | 1964-01-16 | 1966-11-15 | Jefferson Chem Co Inc | Combination process for producing piperazine and triethylenediamine |
| DE2439275B2 (de) | 1974-08-16 | 1978-09-21 | Basf Ag, 6700 Ludwigshafen | Verfahren zur Herstellung von Diäthylentriamin und Triäthylentetramin aus Äthylendiamin |
| GB1551127A (en) | 1975-09-13 | 1979-08-22 | Basf Ag | Manufacture of polypropylenepolyamines |
| US4552961A (en) | 1982-04-30 | 1985-11-12 | Union Carbide Corporation | Preparation of polyalkylene polyamines using phosphorus amide catalyst |
| US4568746A (en) | 1982-12-29 | 1986-02-04 | Union Carbide Corporation | Catalytic preparation of diethylenetriamine |
| US4584405A (en) | 1983-04-18 | 1986-04-22 | Texaco Inc. | Activated carbon catalysts and preparation of linear polyethylene polyamines therewith |
| US4602091A (en) | 1984-01-25 | 1986-07-22 | Texaco Inc. | Production of ethylenediamine and N-aminoethylpiperazine from piperazine |
| US4806517A (en) | 1986-01-21 | 1989-02-21 | Texaco Inc. | Method for making pelleted phosphated catalysts derived from group IVB transition metal oxides and catalysts thus prepared |
| JPH0830040B2 (ja) | 1986-08-13 | 1996-03-27 | 東ソー株式会社 | アルキレンアミン類の製造法 |
| US4922024A (en) | 1988-04-14 | 1990-05-01 | The Dow Chemical Company | Amination process employing group vib metal catalysts |
| US4983735A (en) | 1988-07-20 | 1991-01-08 | The Dow Chemical Company | Preparation of alcohol-extended and amine-extended piperazines |
| US5030740A (en) | 1988-10-14 | 1991-07-09 | The Dow Chemical Company | Process for preparing linearly-extended polyalkylenepolyamines |
| US4927931A (en) | 1988-11-01 | 1990-05-22 | The Dow Chemical Company | Preparation of alkyl-extended, alcohol-extended or amine-extended piperazines |
| US5073635A (en) | 1990-06-22 | 1991-12-17 | The Dow Chemical Company | Process of preparing linearly-extended polyalkylenepolyamines employing metal silicate catalysts |
| CA2051476A1 (en) | 1990-09-17 | 1992-03-18 | Yasushi Hara | Process for producing an ethylenamine |
| US5256786A (en) | 1992-03-02 | 1993-10-26 | The Dow Chemical Company | Catalytic reforming of cyclic alkyleneamines |
| US5222599A (en) | 1992-05-15 | 1993-06-29 | Boyce Donald R | Needle/syringe and blood containment device |
| DE4325848A1 (de) | 1993-07-31 | 1995-02-02 | Basf Ag | Verfahren zur Herstellung von N-(2-Hydroxyethyl)-piperazin |
| DK1114076T3 (da) | 1998-09-14 | 2003-07-07 | Vantico Ag | Acceleratorer til hærdbare systemer |
| DE19842905A1 (de) * | 1998-09-18 | 2000-03-23 | Basf Ag | Verfahren zur gleichzeitigen Herstellung eines cyclischen Lactams und eines cyclischen Amins |
| DE19842900A1 (de) * | 1998-09-18 | 2000-03-23 | Basf Ag | Verfahren zur gemeinsamen Herstellung eines cyclischen Lactams und eines cyclischen Amins |
| US6534441B1 (en) | 1999-03-06 | 2003-03-18 | Union Carbide Chemicals & Plastics Technology Corporation | Nickel-rhenium catalyst for use in reductive amination processes |
| RU2186761C1 (ru) | 2001-02-27 | 2002-08-10 | Закрытое акционерное общество "Каустик" | Способ получения диэтилентриамина |
| SE524126C2 (sv) | 2001-07-24 | 2004-06-29 | Akzo Nobel Nv | Förfarande för framställning av dietylentriamin och högre polyetylenpolyaminer genom transaminering av etylendiamin |
| RU2226188C1 (ru) | 2002-10-25 | 2004-03-27 | Закрытое акционерное общество "Каустик" | Способ получения ди- и полиаминов |
| EP1977816B1 (en) | 2003-09-26 | 2011-08-31 | 3M Innovative Properties Company | Nanoscale gold catalysts, activating agents, support media, and related methodologies useful for making such catalyst systems especially when the gold is deposited onto the support media using physical vapor deposition |
| JP2006306790A (ja) | 2005-04-28 | 2006-11-09 | Koei Chem Co Ltd | ホモピペラジンの製造方法 |
| JP5612583B2 (ja) | 2008-10-06 | 2014-10-22 | ダウ グローバル テクノロジーズ エルエルシー | エチレンオキサイド及びアンモニアからのエタノールアミン及びエチレンアミンの製造方法並びに関連方法 |
| ES2561362T3 (es) | 2008-10-06 | 2016-02-25 | Union Carbide Chemicals & Plastics Technology Llc | Método de fabricación de etilenaminas |
| JP5774992B2 (ja) | 2008-10-06 | 2015-09-09 | ユニオン カーバイド ケミカルズ アンド プラスティックス テクノロジー エルエルシー | 環状、ｎ−アミノ官能性トリアミンの生成方法 |
| EP2352585B1 (en) | 2008-10-06 | 2020-06-17 | Union Carbide Corporation | Low metal loaded, alumina supported, catalyst compositions and amination process |
| US8383860B2 (en) | 2008-10-06 | 2013-02-26 | Union Carbide Chemicals & Plastics Technology Llc | Process to selectively manufacture diethylenetriamine (DETA) or other desirable ethyleneamines via continuous transamination of ethylenediamine (EDA), and other ethyleneamines over a heterogeneous catalyst system |
| US8187997B2 (en) | 2008-10-06 | 2012-05-29 | Union Carbide Chemicals & Technology LLC | Low metal loaded, catalyst compositions including acidic mixed metal oxide as support |
| EP2638003B1 (en) | 2010-11-10 | 2019-11-20 | Dow Global Technologies LLC | Transamination of nitrogen-containing compounds to high molecular weight polyalkyleneamines |
-
2011
- 2011-10-20 EP EP11788253.0A patent/EP2638020B1/en active Active
- 2011-10-20 WO PCT/US2011/057045 patent/WO2012064483A1/en not_active Ceased
- 2011-10-20 JP JP2013538757A patent/JP6006222B2/ja not_active Expired - Fee Related
- 2011-10-20 CN CN201180059241.8A patent/CN103261174B/zh active Active
- 2011-10-20 BR BR112013011672A patent/BR112013011672A2/pt not_active IP Right Cessation
- 2011-10-20 US US13/884,430 patent/US8993759B2/en active Active
Also Published As
| Publication number | Publication date |
|---|---|
| EP2638020A1 (en) | 2013-09-18 |
| CN103261174A (zh) | 2013-08-21 |
| WO2012064483A1 (en) | 2012-05-18 |
| CN103261174B (zh) | 2016-04-20 |
| US20130231476A1 (en) | 2013-09-05 |
| JP2014501715A (ja) | 2014-01-23 |
| US8993759B2 (en) | 2015-03-31 |
| BR112013011672A2 (pt) | 2016-07-12 |
| EP2638020B1 (en) | 2016-09-07 |
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