JP5980206B2 - 低い２−（ジメチルアミノメチル）−グルタロニトリル（ｄｇｎ）含量を有する３−ジメチルアミノプリオニトリル（ｄｍａｐｎ）および低い２−（ジメチルアミノメチル）−グルタロニトリル（ｄｇｎ）含量を有する３−ジメチルアミノプロピオニトリル（ｄｍａｐｎ）から３−ジメチルアミノプロピルアミン（ｄｍａｐａ）を製造する方法 - Google Patents

低い２−（ジメチルアミノメチル）−グルタロニトリル（ｄｇｎ）含量を有する３−ジメチルアミノプリオニトリル（ｄｍａｐｎ）および低い２−（ジメチルアミノメチル）−グルタロニトリル（ｄｇｎ）含量を有する３−ジメチルアミノプロピオニトリル（ｄｍａｐｎ）から３−ジメチルアミノプロピルアミン（ｄｍａｐａ）を製造する方法 Download PDF

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JP5980206B2
JP5980206B2 JP2013521074A JP2013521074A JP5980206B2 JP 5980206 B2 JP5980206 B2 JP 5980206B2 JP 2013521074 A JP2013521074 A JP 2013521074A JP 2013521074 A JP2013521074 A JP 2013521074A JP 5980206 B2 JP5980206 B2 JP 5980206B2
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dmapn
column
dgn
temperature
catalyst
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JP2013521074A
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Japanese (ja)
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JP2013535455A5 (https=
JP2013535455A (ja
Inventor
メーガーライン ヴォルフガング
メーガーライン ヴォルフガング
エーバーハート ヤン
エーバーハート ヤン
ヨハン−ペーター　メルダー
メルダー ヨハン−ペーター
ケーラー ウルリッヒ
ケーラー ウルリッヒ
ハーン ティロ
ハーン ティロ
クライチュマン ミルコ
クライチュマン ミルコ
ヘアブレヒト ドミニク
ヘアブレヒト ドミニク
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BASF SE
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BASF SE
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Publication of JP2013535455A5 publication Critical patent/JP2013535455A5/ja
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
    • C07C209/44—Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of carboxylic acids or esters thereof in presence of ammonia or amines, or by reduction of nitriles, carboxylic acid amides, imines or imino-ethers
    • C07C209/48—Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of carboxylic acids or esters thereof in presence of ammonia or amines, or by reduction of nitriles, carboxylic acid amides, imines or imino-ethers by reduction of nitriles
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
    • C07C209/82—Purification; Separation; Stabilisation; Use of additives
    • C07C209/84—Purification
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C253/00—Preparation of carboxylic acid nitriles
    • C07C253/30—Preparation of carboxylic acid nitriles by reactions not involving the formation of cyano groups
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/582—Recycling of unreacted starting or intermediate materials

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
JP2013521074A 2010-07-29 2011-07-21 低い２−（ジメチルアミノメチル）−グルタロニトリル（ｄｇｎ）含量を有する３−ジメチルアミノプリオニトリル（ｄｍａｐｎ）および低い２−（ジメチルアミノメチル）−グルタロニトリル（ｄｇｎ）含量を有する３−ジメチルアミノプロピオニトリル（ｄｍａｐｎ）から３−ジメチルアミノプロピルアミン（ｄｍａｐａ）を製造する方法 Expired - Fee Related JP5980206B2 (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP10171187.7 2010-07-29
EP10171187 2010-07-29
PCT/EP2011/062496 WO2012013563A1 (de) 2010-07-29 2011-07-21 Dmapn mit niedrigem dgn-gehalt und ein verfahren zur herstellung von dmapa aus dmapn mit niedrigem dgn-gehalt

Publications (3)

Publication Number Publication Date
JP2013535455A JP2013535455A (ja) 2013-09-12
JP2013535455A5 JP2013535455A5 (https=) 2015-07-30
JP5980206B2 true JP5980206B2 (ja) 2016-08-31

Family

ID=43127415

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Application Number Title Priority Date Filing Date
JP2013521074A Expired - Fee Related JP5980206B2 (ja) 2010-07-29 2011-07-21 低い２−（ジメチルアミノメチル）−グルタロニトリル（ｄｇｎ）含量を有する３−ジメチルアミノプリオニトリル（ｄｍａｐｎ）および低い２−（ジメチルアミノメチル）−グルタロニトリル（ｄｇｎ）含量を有する３−ジメチルアミノプロピオニトリル（ｄｍａｐｎ）から３−ジメチルアミノプロピルアミン（ｄｍａｐａ）を製造する方法

Country Status (6)

Country Link
EP (1) EP2412698B1 (https=)
JP (1) JP5980206B2 (https=)
CN (1) CN103124716B (https=)
BR (1) BR112013002105B1 (https=)
ES (1) ES2394680T3 (https=)
WO (1) WO2012013563A1 (https=)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US8981093B2 (en) 2012-06-06 2015-03-17 Basf Se Process for preparing piperazine
CN103012199B (zh) * 2012-09-19 2014-11-26 济南大学 快速高选择性硫化氢比色探针的制备方法
CN109970574B (zh) * 2019-04-11 2022-04-15 中北大学 一种n,n-二异丙基-1,3-丙二胺的制备方法

Family Cites Families (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DD58306A (https=)
DE2709966C2 (de) * 1977-03-08 1979-04-12 Ruhrchemie Ag, 4200 Oberhausen Verfahren zur Herstellung von ß- Dimethylaminopropionitril
DD222011A1 (de) 1983-11-15 1985-05-08 Schwarzheide Synthesewerk Veb Verfahren und vorrichtung zur kontinuierlichen herstellung von 3(n,n-dimethylamino)propionitril
DE4325847A1 (de) * 1993-07-31 1995-02-02 Basf Ag Kobaltkatalysatoren
DE59608407D1 (de) 1995-05-09 2002-01-24 Basf Ag Kobaltkatalysatoren
DE10100314A1 (de) * 2001-01-05 2002-07-11 Basf Ag Verfahren zur Herstellung von sekundären Aminen aus Nitrilen
DE10152135A1 (de) 2001-10-23 2003-04-30 Basf Ag Cobalt-Trägerkatalysatoren für Nitrilhydrierungen
RU2326108C2 (ru) * 2002-12-23 2008-06-10 Солютиа Инк. Способ производства 3-диметиламинопропиламина (дмапа) при низком давлении
US6660887B1 (en) * 2002-12-23 2003-12-09 Solutia Inc. Low pressure process for manufacture of 3-dimethylaminopropylamine (DMAPA)
DE102005004853A1 (de) * 2005-02-01 2006-08-03 Basf Ag Verfahren zur Herstellung von Bis-[(3-Dimethylamino)propyl]amin (BisDMAPA)
DE102005052457A1 (de) 2005-11-03 2007-05-10 Basf Ag Verfahren zur Synthese von DMAPA
RU2434676C9 (ru) * 2006-03-10 2012-12-27 Басф Се Катализатор на основе смешанных оксидов для гидрирования органических соединений, способ его получения и способ гидрирования
JP5227309B2 (ja) * 2006-05-09 2013-07-03 ビーエーエスエフ ソシエタス・ヨーロピア アミノアルキルニトリルおよびそのようなニトリルからのジアミンの製造法
FR2971248B1 (fr) * 2011-02-04 2013-08-16 Rhodia Operations Preparation de diamine via la preparation d'aminonitrile

Also Published As

Publication number Publication date
ES2394680T3 (es) 2013-02-04
CN103124716B (zh) 2014-11-05
JP2013535455A (ja) 2013-09-12
CN103124716A (zh) 2013-05-29
EP2412698A1 (de) 2012-02-01
EP2412698B1 (de) 2012-11-21
WO2012013563A1 (de) 2012-02-02
BR112013002105B1 (pt) 2019-04-30
BR112013002105A2 (pt) 2016-05-24

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