JP5886193B2 - LiFePO4−炭素合成物を製造するための方法 - Google Patents
LiFePO4−炭素合成物を製造するための方法 Download PDFInfo
- Publication number
- JP5886193B2 JP5886193B2 JP2012516703A JP2012516703A JP5886193B2 JP 5886193 B2 JP5886193 B2 JP 5886193B2 JP 2012516703 A JP2012516703 A JP 2012516703A JP 2012516703 A JP2012516703 A JP 2012516703A JP 5886193 B2 JP5886193 B2 JP 5886193B2
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- JP
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- Prior art keywords
- compound
- reducing agent
- particles
- general formula
- carbon
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B25/00—Phosphorus; Compounds thereof
- C01B25/16—Oxyacids of phosphorus; Salts thereof
- C01B25/26—Phosphates
- C01B25/45—Phosphates containing plural metal, or metal and ammonium
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B25/00—Phosphorus; Compounds thereof
- C01B25/16—Oxyacids of phosphorus; Salts thereof
- C01B25/26—Phosphates
- C01B25/455—Phosphates containing halogen
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01B—CABLES; CONDUCTORS; INSULATORS; SELECTION OF MATERIALS FOR THEIR CONDUCTIVE, INSULATING OR DIELECTRIC PROPERTIES
- H01B1/00—Conductors or conductive bodies characterised by the conductive materials; Selection of materials as conductors
- H01B1/20—Conductive material dispersed in non-conductive organic material
- H01B1/24—Conductive material dispersed in non-conductive organic material the conductive material comprising carbon-silicon compounds, carbon or silicon
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/13—Electrodes for accumulators with non-aqueous electrolyte, e.g. for lithium-accumulators; Processes of manufacture thereof
- H01M4/131—Electrodes based on mixed oxides or hydroxides, or on mixtures of oxides or hydroxides, e.g. LiCoOx
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/13—Electrodes for accumulators with non-aqueous electrolyte, e.g. for lithium-accumulators; Processes of manufacture thereof
- H01M4/131—Electrodes based on mixed oxides or hydroxides, or on mixtures of oxides or hydroxides, e.g. LiCoOx
- H01M4/1315—Electrodes based on mixed oxides or hydroxides, or on mixtures of oxides or hydroxides, e.g. LiCoOx containing halogen atoms, e.g. LiCoOxFy
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/13—Electrodes for accumulators with non-aqueous electrolyte, e.g. for lithium-accumulators; Processes of manufacture thereof
- H01M4/133—Electrodes based on carbonaceous material, e.g. graphite-intercalation compounds or CFx
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/36—Selection of substances as active materials, active masses, active liquids
- H01M4/48—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
- H01M4/485—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of mixed oxides or hydroxides for inserting or intercalating light metals, e.g. LiTi2O4 or LiTi2OxFy
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/36—Selection of substances as active materials, active masses, active liquids
- H01M4/48—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
- H01M4/50—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of manganese
- H01M4/505—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of manganese of mixed oxides or hydroxides containing manganese for inserting or intercalating light metals, e.g. LiMn2O4 or LiMn2OxFy
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/36—Selection of substances as active materials, active masses, active liquids
- H01M4/48—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
- H01M4/52—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of nickel, cobalt or iron
- H01M4/525—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of nickel, cobalt or iron of mixed oxides or hydroxides containing iron, cobalt or nickel for inserting or intercalating light metals, e.g. LiNiO2, LiCoO2 or LiCoOxFy
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/36—Selection of substances as active materials, active masses, active liquids
- H01M4/58—Selection of substances as active materials, active masses, active liquids of inorganic compounds other than oxides or hydroxides, e.g. sulfides, selenides, tellurides, halogenides or LiCoFy; of polyanionic structures, e.g. phosphates, silicates or borates
- H01M4/5825—Oxygenated metallic salts or polyanionic structures, e.g. borates, phosphates, silicates, olivines
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/36—Selection of substances as active materials, active masses, active liquids
- H01M4/58—Selection of substances as active materials, active masses, active liquids of inorganic compounds other than oxides or hydroxides, e.g. sulfides, selenides, tellurides, halogenides or LiCoFy; of polyanionic structures, e.g. phosphates, silicates or borates
- H01M4/583—Carbonaceous material, e.g. graphite-intercalation compounds or CFx
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M10/00—Secondary cells; Manufacture thereof
- H01M10/05—Accumulators with non-aqueous electrolyte
- H01M10/052—Li-accumulators
- H01M10/0525—Rocking-chair batteries, i.e. batteries with lithium insertion or intercalation in both electrodes; Lithium-ion batteries
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
- Y02E60/10—Energy storage using batteries
Landscapes
- Chemical & Material Sciences (AREA)
- General Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Electrochemistry (AREA)
- Inorganic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Organic Chemistry (AREA)
- Materials Engineering (AREA)
- Physics & Mathematics (AREA)
- Dispersion Chemistry (AREA)
- Spectroscopy & Molecular Physics (AREA)
- Crystallography & Structural Chemistry (AREA)
- Manufacturing & Machinery (AREA)
- Battery Electrode And Active Subsutance (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US21980209P | 2009-06-24 | 2009-06-24 | |
| US61/219,802 | 2009-06-24 | ||
| PCT/EP2010/058868 WO2010149681A1 (en) | 2009-06-24 | 2010-06-23 | Process for the preparation of lifepo4-carbon composites |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2012530672A JP2012530672A (ja) | 2012-12-06 |
| JP2012530672A5 JP2012530672A5 (https=) | 2013-07-25 |
| JP5886193B2 true JP5886193B2 (ja) | 2016-03-16 |
Family
ID=42584231
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2012516703A Active JP5886193B2 (ja) | 2009-06-24 | 2010-06-23 | LiFePO4−炭素合成物を製造するための方法 |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US9209461B2 (https=) |
| EP (1) | EP2445834B1 (https=) |
| JP (1) | JP5886193B2 (https=) |
| KR (1) | KR101718972B1 (https=) |
| CN (1) | CN102803133B (https=) |
| CA (1) | CA2764410A1 (https=) |
| TW (1) | TW201111276A (https=) |
| WO (1) | WO2010149681A1 (https=) |
Families Citing this family (16)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20120292367A1 (en) | 2006-01-31 | 2012-11-22 | Ethicon Endo-Surgery, Inc. | Robotically-controlled end effector |
| CN102556996A (zh) * | 2010-12-30 | 2012-07-11 | 中国电子科技集团公司第十八研究所 | 一种高振实密度磷酸铁锂的制备方法 |
| US20140004473A1 (en) * | 2011-03-16 | 2014-01-02 | Hanwha Chemical Corporation | Method for calcining electrode materials using a rotary kiln |
| JP2012204322A (ja) * | 2011-03-28 | 2012-10-22 | Gs Yuasa Corp | 非水電解質二次電池用活物質の製造方法 |
| FR2997076B1 (fr) * | 2012-10-19 | 2014-12-26 | Commissariat Energie Atomique | Materiau composite comprenant des nano-objets notamment des nano-objets de carbone, son procede de preparation, et encre et electrode comprenant ce materiau. |
| WO2014180333A1 (zh) * | 2013-05-08 | 2014-11-13 | 台湾立凯电能科技股份有限公司 | 电池复合材料及其前驱物的制备方法 |
| EP2835349A1 (en) * | 2013-08-09 | 2015-02-11 | Basf Se | Process for the preparation of an electrode material and its use in lithium-ion batteries |
| KR101608632B1 (ko) * | 2013-08-20 | 2016-04-05 | 주식회사 엘지화학 | 리튬 복합 전이금속 산화물 제조용 전구체, 그 제조방법 및 이를 이용한 리튬 복합 전이금속 산화물 |
| PL233550B1 (pl) * | 2014-03-12 | 2019-10-31 | Akademia Gorniczo Hutnicza Im Stanislawa Staszica W Krakowie | Sposób otrzymywania krystalicznego nanometrycznego fosforanu litowo-żelazowego |
| JP6326366B2 (ja) * | 2014-12-25 | 2018-05-16 | 信越化学工業株式会社 | リチウムリン系複合酸化物炭素複合体及びその製造方法並びに、電気化学デバイス及びリチウムイオン二次電池 |
| KR102161590B1 (ko) * | 2016-03-29 | 2020-10-05 | 주식회사 엘지화학 | 이차전지용 양극의 제조방법, 및 이를 이용하여 제조된 양극 및 이차전지 |
| FR3077012B1 (fr) * | 2018-01-25 | 2020-01-03 | Brgm | Procede d'obtention de (nano)particules minerales enrobees de carbone |
| JP6964055B2 (ja) * | 2018-08-23 | 2021-11-10 | 住友大阪セメント株式会社 | リチウムイオン二次電池用正極材料の製造方法 |
| WO2020264464A1 (en) | 2019-06-28 | 2020-12-30 | eJoule, Inc. | Assisted gas flow inside a reaction chamber of a processing system |
| US11376559B2 (en) | 2019-06-28 | 2022-07-05 | eJoule, Inc. | Processing system and method for producing a particulate material |
| US11121354B2 (en) | 2019-06-28 | 2021-09-14 | eJoule, Inc. | System with power jet modules and method thereof |
Family Cites Families (30)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6514640B1 (en) | 1996-04-23 | 2003-02-04 | Board Of Regents, The University Of Texas System | Cathode materials for secondary (rechargeable) lithium batteries |
| CA2270771A1 (fr) | 1999-04-30 | 2000-10-30 | Hydro-Quebec | Nouveaux materiaux d'electrode presentant une conductivite de surface elevee |
| US6528033B1 (en) | 2000-01-18 | 2003-03-04 | Valence Technology, Inc. | Method of making lithium-containing materials |
| US6777132B2 (en) * | 2000-04-27 | 2004-08-17 | Valence Technology, Inc. | Alkali/transition metal halo—and hydroxy-phosphates and related electrode active materials |
| CA2320661A1 (fr) * | 2000-09-26 | 2002-03-26 | Hydro-Quebec | Nouveau procede de synthese de materiaux limpo4 a structure olivine |
| JP2003203628A (ja) * | 2001-12-28 | 2003-07-18 | Sanyo Electric Co Ltd | 非水電解質電池及びその製造方法 |
| US6913855B2 (en) | 2002-07-22 | 2005-07-05 | Valence Technology, Inc. | Method of synthesizing electrochemically active materials from a slurry of precursors |
| FR2852148B1 (fr) | 2003-03-07 | 2014-04-11 | Batscap Sa | Materiau pour electrode composite, procede pour sa preparation |
| CN1233054C (zh) | 2003-12-17 | 2005-12-21 | 北京科技大学 | 一种采用微波法制备LiFePO4材料的方法 |
| JP2006155941A (ja) | 2004-11-25 | 2006-06-15 | Kyushu Univ | 電極活物質の製造方法 |
| DE102005012640B4 (de) * | 2005-03-18 | 2015-02-05 | Süd-Chemie Ip Gmbh & Co. Kg | Kreisprozess zur nasschemischen Herstellung von Lithiummetallphosphaten |
| DE102005015613A1 (de) | 2005-04-05 | 2006-10-12 | Süd-Chemie AG | Kristallines Ionenleitendes Nanomaterial und Verfahren zu seiner Herstellung |
| JP4804045B2 (ja) * | 2005-06-15 | 2011-10-26 | Agcセイミケミカル株式会社 | リチウム鉄複合酸化物の製造方法 |
| US7964118B2 (en) * | 2005-09-21 | 2011-06-21 | Kanto Denka Kogyo Co., Ltd. | Positive electrode active material and method of producing the same and nonaqueous electrolyte battery having positive electrode containing positive electrode active material |
| CN101200289A (zh) | 2006-12-15 | 2008-06-18 | 中国电子科技集团公司第十八研究所 | 一种磷酸铁锂材料及其制备方法 |
| JP5385616B2 (ja) * | 2007-01-29 | 2014-01-08 | 関東電化工業株式会社 | オリビン構造を有する化合物及びその製造方法、並びにオリビン構造を有する化合物を使用する正極活物質及び非水電解質電池 |
| CN100540465C (zh) | 2007-07-23 | 2009-09-16 | 河北工业大学 | 锂离子电池正极材料磷酸铁锂的水热合成制备方法 |
| DE102008002989A1 (de) | 2007-08-16 | 2009-02-19 | Basf Se | Elektrisch leitfähiges, magnetisches Kompositmaterial, Verfahren zu seiner Herstellung und seine Verwendung |
| CN100511778C (zh) | 2007-08-24 | 2009-07-08 | 郑州德朗能电池有限公司 | 高性能锂离子电池正极材料LiFePO4/C的制备方法 |
| CN100502103C (zh) * | 2007-09-13 | 2009-06-17 | 广西师范大学 | 一种核壳型纳米级碳包覆磷酸铁锂复合正极材料及其制备方法 |
| EP2212247B1 (en) * | 2007-10-01 | 2013-07-17 | Basf Se | Process for the preparation of crystalline lithium-, vanadium- and phosphate-comprising materials |
| EP2207751B1 (en) | 2007-10-01 | 2013-07-03 | Basf Se | Process for the preparation of porous lithium-, vanadium and phosphate-comprising materials |
| DE102007058674A1 (de) * | 2007-12-06 | 2009-07-02 | Süd-Chemie AG | Nanopartikuläre Zusammensetzung und Verfahren zu deren Herstellung |
| TW201010944A (en) | 2008-04-17 | 2010-03-16 | Basf Se | Process for the preparation of crystalline lithium-, iron-and phosphate-comprising materials |
| TW200951066A (en) | 2008-04-17 | 2009-12-16 | Basf Se | Process for the preparation of crystalline lithium-, iron-and phosphate-comprising materials |
| TW201002623A (en) | 2008-05-30 | 2010-01-16 | Basf Se | Process for preparing lithium vanadium oxides and their use as cathode material |
| CN101339995A (zh) * | 2008-08-12 | 2009-01-07 | 中国兵器工业第二一三研究所 | 锂离子动力电池用磷酸铁锂正极材料的制备方法 |
| TWI440597B (zh) | 2008-08-26 | 2014-06-11 | Basf Se | 於水熱條件下合成LiFePO4 |
| KR20110139281A (ko) | 2009-03-17 | 2011-12-28 | 바스프 에스이 | 열수 조건 하의 리튬-철-포스페이트의 합성 방법 |
| US20110249603A1 (en) | 2009-06-16 | 2011-10-13 | Qualcomm Incorporated | Apparatus and method for multiple wireless service coexistence |
-
2010
- 2010-06-23 JP JP2012516703A patent/JP5886193B2/ja active Active
- 2010-06-23 KR KR1020127001823A patent/KR101718972B1/ko active Active
- 2010-06-23 EP EP10724538.3A patent/EP2445834B1/en active Active
- 2010-06-23 WO PCT/EP2010/058868 patent/WO2010149681A1/en not_active Ceased
- 2010-06-23 US US13/379,048 patent/US9209461B2/en active Active
- 2010-06-23 CA CA2764410A patent/CA2764410A1/en not_active Abandoned
- 2010-06-23 CN CN201080028061.9A patent/CN102803133B/zh active Active
- 2010-06-24 TW TW099120631A patent/TW201111276A/zh unknown
Also Published As
| Publication number | Publication date |
|---|---|
| CA2764410A1 (en) | 2010-12-29 |
| EP2445834B1 (en) | 2020-04-01 |
| KR20120089799A (ko) | 2012-08-13 |
| CN102803133A (zh) | 2012-11-28 |
| CN102803133B (zh) | 2016-01-06 |
| US9209461B2 (en) | 2015-12-08 |
| US20120097901A1 (en) | 2012-04-26 |
| KR101718972B1 (ko) | 2017-03-23 |
| TW201111276A (en) | 2011-04-01 |
| JP2012530672A (ja) | 2012-12-06 |
| WO2010149681A1 (en) | 2010-12-29 |
| EP2445834A1 (en) | 2012-05-02 |
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