JP5745541B2 - ポリジオルガノシロキサンポリオキサミドコポリマーの製造方法 - Google Patents
ポリジオルガノシロキサンポリオキサミドコポリマーの製造方法 Download PDFInfo
- Publication number
- JP5745541B2 JP5745541B2 JP2012547155A JP2012547155A JP5745541B2 JP 5745541 B2 JP5745541 B2 JP 5745541B2 JP 2012547155 A JP2012547155 A JP 2012547155A JP 2012547155 A JP2012547155 A JP 2012547155A JP 5745541 B2 JP5745541 B2 JP 5745541B2
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- group
- formula
- aryl
- alkyl
- aralkyl
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 0 CC(C)(C(C(O*)=O)=O)N(*)*N(*)C(C(C(C)(*)O*)=O)=O Chemical compound CC(C)(C(C(O*)=O)=O)N(*)*N(*)C(C(C(C)(*)O*)=O)=O 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
- C08G77/42—Block-or graft-polymers containing polysiloxane sequences
- C08G77/452—Block-or graft-polymers containing polysiloxane sequences containing nitrogen-containing sequences
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
- C08G77/42—Block-or graft-polymers containing polysiloxane sequences
- C08G77/452—Block-or graft-polymers containing polysiloxane sequences containing nitrogen-containing sequences
- C08G77/455—Block-or graft-polymers containing polysiloxane sequences containing nitrogen-containing sequences containing polyamide, polyesteramide or polyimide sequences
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C233/00—Carboxylic acid amides
- C07C233/01—Carboxylic acid amides having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms
- C07C233/56—Carboxylic acid amides having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms having carbon atoms of carboxamide groups bound to carbon atoms of carboxyl groups, e.g. oxamides
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C69/00—Esters of carboxylic acids; Esters of carbonic or haloformic acids
- C07C69/34—Esters of acyclic saturated polycarboxylic acids having an esterified carboxyl group bound to an acyclic carbon atom
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G69/00—Macromolecular compounds obtained by reactions forming a carboxylic amide link in the main chain of the macromolecule
- C08G69/02—Polyamides derived from amino-carboxylic acids or from polyamines and polycarboxylic acids
- C08G69/26—Polyamides derived from amino-carboxylic acids or from polyamines and polycarboxylic acids derived from polyamines and polycarboxylic acids
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
- C08G77/04—Polysiloxanes
- C08G77/38—Polysiloxanes modified by chemical after-treatment
- C08G77/382—Polysiloxanes modified by chemical after-treatment containing atoms other than carbon, hydrogen, oxygen or silicon
- C08G77/388—Polysiloxanes modified by chemical after-treatment containing atoms other than carbon, hydrogen, oxygen or silicon containing nitrogen
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- General Chemical & Material Sciences (AREA)
- Macromolecular Compounds Obtained By Forming Nitrogen-Containing Linkages In General (AREA)
- Polyamides (AREA)
- Silicon Polymers (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US29100809P | 2009-12-30 | 2009-12-30 | |
| US61/291,008 | 2009-12-30 | ||
| PCT/US2010/061817 WO2011082069A1 (en) | 2009-12-30 | 2010-12-22 | Methods of making polydiorganosiloxane polyoxamide copolymers |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2013516518A JP2013516518A (ja) | 2013-05-13 |
| JP2013516518A5 JP2013516518A5 (enExample) | 2014-02-06 |
| JP5745541B2 true JP5745541B2 (ja) | 2015-07-08 |
Family
ID=43530724
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2012547155A Active JP5745541B2 (ja) | 2009-12-30 | 2010-12-22 | ポリジオルガノシロキサンポリオキサミドコポリマーの製造方法 |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US8765881B2 (enExample) |
| EP (1) | EP2519563B1 (enExample) |
| JP (1) | JP5745541B2 (enExample) |
| KR (1) | KR101820979B1 (enExample) |
| CN (1) | CN102712758B (enExample) |
| TW (1) | TWI512018B (enExample) |
| WO (1) | WO2011082069A1 (enExample) |
Families Citing this family (51)
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| US8907046B2 (en) | 2009-12-30 | 2014-12-09 | 3M Innovative Properties Company | Copolymers with perfluoropolyether segment and multiple aminooxalylamino groups |
| WO2011082067A2 (en) | 2009-12-30 | 2011-07-07 | 3M Innovative Properties Company | Perfluoropolyether-containing compounds with oxalylamino groups |
| US8614281B2 (en) * | 2009-12-30 | 2013-12-24 | 3M Innovative Properties Company | Moisture-curable siloxanes and siloxane polymers |
| WO2011082063A1 (en) * | 2009-12-30 | 2011-07-07 | 3M Innovative Properties Company | Copolymers with perfluorpolyether segment and polydiorganosiloxane segment |
| JP5635622B2 (ja) * | 2009-12-30 | 2014-12-03 | スリーエム イノベイティブ プロパティズ カンパニー | 水分硬化性シロキサン含有及びフルオロカーボン含有化合物、並びに該化合物から形成されるポリマー |
| JP5782718B2 (ja) * | 2011-01-18 | 2015-09-24 | 三菱化学株式会社 | 非水電解液、およびそれを用いた非水電解液電池 |
| CA2916251C (en) | 2013-06-24 | 2021-05-25 | 3M Innovative Properties Company | Article comprising pressure-sensitive adhesive stripes |
| EP3013913B1 (en) | 2013-06-24 | 2019-09-25 | 3M Innovative Properties Company | Pressure-sensitive adhesive layers with surface-enriched stripes and methods of making |
| WO2015095173A1 (en) | 2013-12-16 | 2015-06-25 | 3M Innovative Properties Company | Blended release materials |
| JP2017511755A (ja) | 2014-01-22 | 2017-04-27 | スリーエム イノベイティブ プロパティズ カンパニー | ガラス用微小光学要素 |
| JP6464567B2 (ja) * | 2014-04-22 | 2019-02-06 | 宇部興産株式会社 | ポリアミド樹脂及びそれを用いて製造される成形品 |
| US9970614B2 (en) | 2014-10-20 | 2018-05-15 | 3M Innovative Properties Company | Insulated glazing units and microoptical layer comprising microstructured diffuser and methods |
| US10723894B2 (en) | 2014-12-23 | 2020-07-28 | 3M Innovative Properties Company | Tie layers prepared from particle-containing waterborne suspensions |
| US11286404B2 (en) | 2014-12-23 | 2022-03-29 | 3M Innovative Properties Company | Dual-sided multi-layer adhesive |
| CN107683313B (zh) | 2015-06-03 | 2021-02-05 | 3M创新有限公司 | 用于柔性显示器的组件层 |
| WO2016196541A1 (en) | 2015-06-03 | 2016-12-08 | 3M Innovative Properties Company | Acrylic-based flexible assembly layer |
| US20180126706A1 (en) | 2015-06-03 | 2018-05-10 | 3M Innovative Properties Company | Silicone-based assembly layers for flexible display applications |
| US10618247B2 (en) | 2015-06-19 | 2020-04-14 | 3M Innovative Properties Company | Segmented and non-segmented transfer tapes, articles therefrom and method of making and use thereof |
| US11086056B2 (en) | 2015-06-19 | 2021-08-10 | 3M Innovative Properties Company | Micro-optical assemblies including transparent substrates having graphic layer and method of making thereof |
| CN107820461B (zh) | 2015-06-19 | 2019-12-17 | 3M创新有限公司 | 分段式转印带及其制备和使用方法 |
| JP2018521357A (ja) | 2015-06-30 | 2018-08-02 | スリーエム イノベイティブ プロパティズ カンパニー | 微細構造化異方性拡散体を含む断熱ガラスユニット及び微小光学層並びに方法 |
| CN108603090A (zh) * | 2016-02-01 | 2018-09-28 | 3M创新有限公司 | 粘合剂组合物 |
| TWI722105B (zh) | 2016-02-01 | 2021-03-21 | 美商3M新設資產公司 | 可適形、拉伸可離型黏著物品 |
| CN108603079B (zh) | 2016-02-01 | 2021-11-26 | 3M创新有限公司 | 可适形的、可剥离的粘合剂制品 |
| WO2018005040A1 (en) | 2016-06-27 | 2018-01-04 | 3M Innovative Properties Company | Fluorochemical piperazine carboxamides |
| JP2019529596A (ja) | 2016-07-28 | 2019-10-17 | スリーエム イノベイティブ プロパティズ カンパニー | セグメント化シリコーンポリアミドブロックコポリマー及びそれを含む物品 |
| EP3491047B1 (en) | 2016-07-28 | 2021-09-15 | 3M Innovative Properties Company | Segmented silicone polyamide block copolymers and articles containing the same |
| TW201918700A (zh) | 2017-05-05 | 2019-05-16 | 美商3M新設資產公司 | 散射測量系統及其使用方法 |
| US9960389B1 (en) | 2017-05-05 | 2018-05-01 | 3M Innovative Properties Company | Polymeric films and display devices containing such films |
| CN111032333B (zh) | 2017-08-25 | 2022-10-04 | 3M创新有限公司 | 允许无损移除的粘合剂制品 |
| WO2019082023A1 (en) | 2017-10-26 | 2019-05-02 | 3M Innovative Properties Company | COMPOSITION CONTAINING SILICONE ADHESIVE AND CELLULOSE NANOCRYSTALS, METHODS AND ARTICLES |
| WO2019125931A1 (en) | 2017-12-20 | 2019-06-27 | 3M Innovative Properties Company | Composite particles, compositions and foam compositions containing composite particles, articles, and methods of making and using same |
| WO2019224769A1 (en) | 2018-05-25 | 2019-11-28 | 3M Innovative Properties Company | Phase separated articles |
| CN112041375B (zh) * | 2018-07-30 | 2022-03-29 | 瓦克化学股份公司 | 用于制备草酰胺官能的硅氧烷的方法 |
| KR102292493B1 (ko) * | 2018-08-10 | 2021-08-23 | 와커 헤미 아게 | 옥사미도에스테르-관능화 오르가노폴리실록산의 수성 에멀젼 |
| US20210317279A1 (en) | 2018-09-13 | 2021-10-14 | 3M Innovative Properties Company | Foam compositions and methods of making same |
| EP3986958A1 (en) | 2019-06-18 | 2022-04-27 | 3M Innovative Properties Company | Compositions and foam compositions containing composite particles, articles, composite particles, and methods |
| EP4013910B1 (en) | 2019-08-15 | 2023-04-05 | 3M Innovative Properties Company | Core-sheath filament with a silicone-containing block copolymer core |
| CN110483320A (zh) * | 2019-09-10 | 2019-11-22 | 山西省化工研究所（有限公司） | 一种利用醇类溶剂合成双-氧代乙酸酯类化合物的方法 |
| WO2021099997A1 (en) | 2019-11-20 | 2021-05-27 | 3M Innovative Properties Company | Medical tapes with high optical clarity when over-taped |
| AU2020406363B2 (en) * | 2019-12-19 | 2023-05-11 | 3M Innovative Properties Company | Silicone polyoxamide copolymers with amine-based end groups |
| CN116096788A (zh) * | 2020-09-08 | 2023-05-09 | 瓦克化学股份公司 | 有机硅共聚物，其制备方法及其在纤维基材处理中的用途 |
| US20230323124A1 (en) | 2020-09-30 | 2023-10-12 | 3M Innovative Properties Company | Compositions and Foam Compositions Including Silicone Components, Foam Gaskets, Articles, and Methods |
| US20230363858A1 (en) | 2020-10-13 | 2023-11-16 | 3M Innovative Properties Company | Methods of controlling haze in orthodontic appliances including semi-crystalline polymers |
| JP7386379B2 (ja) | 2020-10-28 | 2023-11-24 | スリーエム イノベイティブ プロパティズ カンパニー | 硬化接着剤組成物及び製造方法 |
| US20230355352A1 (en) | 2020-11-20 | 2023-11-09 | 3M Innovative Properties Company | Articles, methods and compositions comprising polymerizable dicarbonyl polymers |
| CN116802524A (zh) | 2020-12-07 | 2023-09-22 | 3M创新有限公司 | 光学膜、光学构造体和显示系统 |
| WO2022219424A1 (en) | 2021-04-13 | 2022-10-20 | 3M Innovative Properties Company | Chain–extended silicones, method of making, curable composition including the same, and thermal gap filler |
| KR20230173123A (ko) * | 2021-04-23 | 2023-12-26 | 쓰리엠 이노베이티브 프로퍼티즈 컴파니 | 벽지에 적용하기 위한 라미네이트 및 이를 사용한 물품 |
| CN117750951A (zh) | 2021-07-29 | 2024-03-22 | 3M创新有限公司 | 包含水杨酸的成膜组合物和使用方法 |
| WO2025099507A1 (en) | 2023-11-10 | 2025-05-15 | Solventum Intellectual Properties Company | Method of using a negative pressure wound therapy dressing |
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| US2343808A (en) | 1939-05-17 | 1944-03-07 | Schlack Paul | Nitrogenous condensation products |
| US3250807A (en) | 1963-08-23 | 1966-05-10 | Du Pont | Dicarboxylic acids of fluorocarbon ethers and fluorides, esters, amides and salts thereof |
| NL148300B (nl) | 1964-01-02 | 1976-01-15 | Edison Soc | Werkwijze ter bereiding van polyoxyperfluormethylenen. |
| NL6709067A (enExample) | 1964-04-09 | 1968-01-08 | ||
| US3442942A (en) | 1964-04-09 | 1969-05-06 | Montedison Spa | Fluorinated oxygen containing acyl fluorides |
| US3399137A (en) * | 1965-09-08 | 1968-08-27 | American Cyanamid Co | Generation of light by the reaction of anhydrides of oxalic acid with a peroxide in tpresence of a fluorescer |
| DE1745169B2 (de) | 1967-02-09 | 1977-04-21 | Montecatini Edison S.P.A., Mailand (Italien) | Fluorierte lineare polyaether und verfahren zu ihrer herstellung |
| GB1225622A (enExample) * | 1967-05-10 | 1971-03-17 | ||
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| US4085137A (en) | 1969-03-10 | 1978-04-18 | Minnesota Mining And Manufacturing Company | Poly(perfluoroalkylene oxide) derivatives |
| US3728311A (en) | 1971-12-16 | 1973-04-17 | Du Pont | Polyureas,polyurethanes and polyamides based on a tetra-oxo diamine component |
| US3890269A (en) | 1972-08-11 | 1975-06-17 | Stauffer Chemical Co | Process for preparing aminofunctional polysiloxane polymers |
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| US4178432A (en) * | 1977-08-15 | 1979-12-11 | The Upjohn Company | Copolyoxalamide from branched chain diamine |
| US4684728A (en) | 1979-01-12 | 1987-08-04 | Bayer Aktiengesellschaft | Solubilizing biologically active compounds with reactive hydrogen atoms |
| US4661577A (en) | 1985-10-01 | 1987-04-28 | General Electric Company | Aminofunctional polysiloxanes |
| US5214119A (en) | 1986-06-20 | 1993-05-25 | Minnesota Mining And Manufacturing Company | Block copolymer, method of making the same, dimaine precursors of the same, method of making such diamines and end products comprising the block copolymer |
| US5512650A (en) | 1986-06-20 | 1996-04-30 | Minnesota Mining And Manufacturing Company | Block copolymer, method of making the same, diamine precursors of the same, method of making such diamines and end products comprising the block copolymer |
| US5026890A (en) | 1988-05-20 | 1991-06-25 | General Electric Company | Method and intermediates for preparation of bis(aminoalkyl)polydiorganosiloxanes |
| US5093432A (en) | 1988-09-28 | 1992-03-03 | Exfluor Research Corporation | Liquid phase fluorination |
| JP2743432B2 (ja) * | 1989-02-03 | 1998-04-22 | 日本油脂株式会社 | 抗血栓性材料 |
| US5266650A (en) | 1990-10-11 | 1993-11-30 | Minnesota Mining And Manufacturing Company | Curing fluorocarbon elastomers |
| JP2684130B2 (ja) | 1991-08-15 | 1997-12-03 | 信越化学工業株式会社 | アミノ基含有ポリシロキサンの製造方法 |
| US5488142A (en) | 1993-10-04 | 1996-01-30 | Minnesota Mining And Manufacturing Company | Fluorination in tubular reactor system |
| US5663127A (en) | 1994-07-29 | 1997-09-02 | Minnesota Mining And Manufacturing Company | Perfluoropolyether lubricating compositions |
| ES2199288T3 (es) | 1995-04-25 | 2004-02-16 | Minnesota Mining And Manufacturing Company | Copolimeros segmentados de polidiorganosiloxano-oligourea y procedimiento para preparar los mismos. |
| US6355759B1 (en) | 1996-04-25 | 2002-03-12 | 3M Innovative Properties Company | Polydiorganosiloxane polyurea segmented copolymers and a process for making same |
| US6313335B1 (en) | 1997-11-25 | 2001-11-06 | 3M Innovative Properties | Room temperature curable silane terminated and stable waterborne polyurethane dispersions which contain fluorine and/or silicone and low surface energy coatings prepared therefrom |
| JP3729687B2 (ja) | 1999-08-04 | 2005-12-21 | 株式会社巴川製紙所 | 反射防止材料 |
| ITMI20021734A1 (it) | 2002-08-01 | 2004-02-02 | Ausimont S P A Ora Solvay Solexis Spa | Processo per la preparazione di perfluoropolieteri con terminali aldeidici, alcolici, amminici mediante riduzione catalitica. |
| TWI293715B (en) | 2002-10-10 | 2008-02-21 | Sipix Imaging Inc | A method for inducing or enhancing the threshold of an electrophoretic display, an electrophoretic fluid and an electrophoretic display |
| US6923921B2 (en) | 2002-12-30 | 2005-08-02 | 3M Innovative Properties Company | Fluorinated polyether compositions |
| US20040266985A1 (en) | 2003-06-26 | 2004-12-30 | Jon Lee Howell | Nitrogenated perfluoropolyether composition |
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| US20070149745A1 (en) | 2005-12-23 | 2007-06-28 | 3M Innovative Properties Company | Polydiorganosiloxane-containing materials with oxalylamino groups |
| US7371464B2 (en) | 2005-12-23 | 2008-05-13 | 3M Innovative Properties Company | Adhesive compositions |
| CN101346649B (zh) | 2005-12-23 | 2010-09-01 | 3M创新有限公司 | 包含热塑性有机硅嵌段共聚物的膜 |
| KR20090003165A (ko) | 2006-01-13 | 2009-01-09 | 이 아이 듀폰 디 네모아 앤드 캄파니 | 퍼플루오로폴리에테르를 함유하는 냉매 첨가제 조성물 |
| EP2057248A2 (en) | 2006-09-01 | 2009-05-13 | E.I. Du Pont De Nemours And Company | Phenol stabilizers for fluoroolefins |
| WO2008072754A1 (ja) * | 2006-12-11 | 2008-06-19 | Ube Industries, Ltd. | ポリアミド樹脂 |
| US7745653B2 (en) | 2007-03-08 | 2010-06-29 | 3M Innovative Properties Company | Fluorochemical compounds having pendent silyl groups |
| US7335786B1 (en) | 2007-03-29 | 2008-02-26 | 3M Innovative Properties Company | Michael-adduct fluorochemical silanes |
| US8063166B2 (en) | 2007-06-22 | 2011-11-22 | 3M Innovative Properties Company | Polydiorganosiloxane polyamide copolymers having organic soft segments |
| US7705101B2 (en) | 2007-06-22 | 2010-04-27 | 3M Innovative Properties Company | Branched polydiorganosiloxane polyamide copolymers |
| WO2011082067A2 (en) | 2009-12-30 | 2011-07-07 | 3M Innovative Properties Company | Perfluoropolyether-containing compounds with oxalylamino groups |
| WO2011082063A1 (en) | 2009-12-30 | 2011-07-07 | 3M Innovative Properties Company | Copolymers with perfluorpolyether segment and polydiorganosiloxane segment |
| US8907046B2 (en) | 2009-12-30 | 2014-12-09 | 3M Innovative Properties Company | Copolymers with perfluoropolyether segment and multiple aminooxalylamino groups |
-
2010
- 2010-12-22 WO PCT/US2010/061817 patent/WO2011082069A1/en not_active Ceased
- 2010-12-22 CN CN201080060307.0A patent/CN102712758B/zh not_active Expired - Fee Related
- 2010-12-22 KR KR1020127019744A patent/KR101820979B1/ko active Active
- 2010-12-22 EP EP10801775.7A patent/EP2519563B1/en active Active
- 2010-12-22 JP JP2012547155A patent/JP5745541B2/ja active Active
- 2010-12-22 US US13/514,497 patent/US8765881B2/en active Active
- 2010-12-29 TW TW099146702A patent/TWI512018B/zh not_active IP Right Cessation
Also Published As
| Publication number | Publication date |
|---|---|
| TW201139522A (en) | 2011-11-16 |
| EP2519563B1 (en) | 2013-11-06 |
| TWI512018B (zh) | 2015-12-11 |
| US20120271025A1 (en) | 2012-10-25 |
| KR20120106997A (ko) | 2012-09-27 |
| CN102712758B (zh) | 2014-05-07 |
| KR101820979B1 (ko) | 2018-01-22 |
| CN102712758A (zh) | 2012-10-03 |
| WO2011082069A1 (en) | 2011-07-07 |
| EP2519563A1 (en) | 2012-11-07 |
| US8765881B2 (en) | 2014-07-01 |
| JP2013516518A (ja) | 2013-05-13 |
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