JP5658141B2 - ナノ粒子の製造方法 - Google Patents

ナノ粒子の製造方法 Download PDF

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Publication number
JP5658141B2
JP5658141B2 JP2011508631A JP2011508631A JP5658141B2 JP 5658141 B2 JP5658141 B2 JP 5658141B2 JP 2011508631 A JP2011508631 A JP 2011508631A JP 2011508631 A JP2011508631 A JP 2011508631A JP 5658141 B2 JP5658141 B2 JP 5658141B2
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phosphate
metal
combinations
carbon atoms
organic
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Japanese (ja)
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JP2011519816A (ja
JP2011519816A5 (https=
Inventor
シャルマ，ネーラジ
シー． ブ，チョウア
シー． ブ，チョウア
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3M Innovative Properties Co
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3M Innovative Properties Co
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    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C3/00—Treatment in general of inorganic materials, other than fibrous fillers, to enhance their pigmenting or filling properties
    • C09C3/12—Treatment with organosilicon compounds
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K47/00—Medicinal preparations characterised by the non-active ingredients used, e.g. carriers or inert additives; Targeting or modifying agents chemically bound to the active ingredient
    • A61K47/02—Inorganic compounds
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K9/00—Medicinal preparations characterised by special physical form
    • A61K9/0012—Galenical forms characterised by the site of application
    • A61K9/007—Pulmonary tract; Aromatherapy
    • A61K9/0073—Sprays or powders for inhalation; Aerolised or nebulised preparations generated by other means than thermal energy
    • A61K9/0075—Sprays or powders for inhalation; Aerolised or nebulised preparations generated by other means than thermal energy for inhalation via a dry powder inhaler [DPI], e.g. comprising micronized drug mixed with lactose carrier particles
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P11/00—Drugs for disorders of the respiratory system
    • A61P11/06—Antiasthmatics
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P29/00—Non-central analgesic, antipyretic or antiinflammatory agents, e.g. antirheumatic agents; Non-steroidal antiinflammatory drugs [NSAID]
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
    • C09C1/02—Compounds of alkaline earth metals or magnesium
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C01P2004/64—Nanometer sized, i.e. from 1-100 nanometer
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/80—Particles consisting of a mixture of two or more inorganic phases
    • C01P2004/82—Particles consisting of a mixture of two or more inorganic phases two phases having the same anion, e.g. both oxidic phases
    • C01P2004/84—Particles consisting of a mixture of two or more inorganic phases two phases having the same anion, e.g. both oxidic phases one phase coated with the other
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/22—Rheological behaviour as dispersion, e.g. viscosity, sedimentation stability
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00—Stock material or miscellaneous articles
    • Y10T428/29—Coated or structually defined flake, particle, cell, strand, strand portion, rod, filament, macroscopic fiber or mass thereof
    • Y10T428/2982—Particulate matter [e.g., sphere, flake, etc.]

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  • Health & Medical Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Medicinal Chemistry (AREA)
  • Pharmacology & Pharmacy (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Bioinformatics & Cheminformatics (AREA)
  • Pulmonology (AREA)
  • Epidemiology (AREA)
  • Nanotechnology (AREA)
  • Inorganic Chemistry (AREA)
  • Nuclear Medicine, Radiotherapy & Molecular Imaging (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Composite Materials (AREA)
  • Physics & Mathematics (AREA)
  • Materials Engineering (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Condensed Matter Physics & Semiconductors (AREA)
  • Otolaryngology (AREA)
  • General Physics & Mathematics (AREA)
  • Pain & Pain Management (AREA)
  • Rheumatology (AREA)
  • Pigments, Carbon Blacks, Or Wood Stains (AREA)
  • Oxygen, Ozone, And Oxides In General (AREA)
  • Silicon Compounds (AREA)
  • Medicinal Preparation (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
JP2011508631A 2008-05-08 2009-05-06 ナノ粒子の製造方法 Expired - Fee Related JP5658141B2 (ja)

Applications Claiming Priority (5)

Application Number Priority Date Filing Date Title
US5146808P 2008-05-08 2008-05-08
US5147708P 2008-05-08 2008-05-08
US61/051,468 2008-05-08
US61/051,477 2008-05-08
PCT/US2009/043006 WO2009137595A2 (en) 2008-05-08 2009-05-06 Process for producing nanoparticles

Publications (3)

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JP2011519816A JP2011519816A (ja) 2011-07-14
JP2011519816A5 JP2011519816A5 (https=) 2012-06-07
JP5658141B2 true JP5658141B2 (ja) 2015-01-21

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JP2011508631A Expired - Fee Related JP5658141B2 (ja) 2008-05-08 2009-05-06 ナノ粒子の製造方法
JP2011508629A Pending JP2011520015A (ja) 2008-05-08 2009-05-06 表面修飾ナノ粒子

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JP2011508629A Pending JP2011520015A (ja) 2008-05-08 2009-05-06 表面修飾ナノ粒子

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US (2) US20110039947A1 (https=)
EP (2) EP2297172B1 (https=)
JP (2) JP5658141B2 (https=)
CN (2) CN102089317B (https=)
WO (2) WO2009137595A2 (https=)

Families Citing this family (31)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20110039947A1 (en) * 2008-05-08 2011-02-17 3M Innovative Properties Company Surface-modified nanoparticles
WO2010059812A1 (en) * 2008-11-24 2010-05-27 3M Innovative Properties Company Surface-modified metal phosphate nanoparticles
US20110046238A1 (en) * 2009-08-24 2011-02-24 Keiser Bruce A Calcium based carrier particles
US20110046239A1 (en) * 2009-08-24 2011-02-24 Keiser Bruce A Calcium based carrier particles
WO2011023266A1 (en) * 2009-08-28 2011-03-03 Basf Se Modified nanoparticles
ES2352635B1 (es) * 2010-09-16 2011-12-29 Biotechnology Institute, I Mas D, S.L. Implante con calcio en su superficie, y método de modificación de la superficie de un implante para dotar a dicha superficie de calcio.
US8906415B1 (en) * 2011-10-26 2014-12-09 The University Of Toledo Calcium phosphate nanowhisker particles, method of making and using the same
WO2013067049A1 (en) 2011-10-31 2013-05-10 The University Of Toledo Method for modifying surfaces for better osseointegration
CN102530905B (zh) * 2011-12-22 2014-09-03 浙江天能能源科技有限公司 粒径可控的纳米FePO4的制备方法
CN103374120B (zh) * 2012-04-13 2016-03-09 中国石油天然气股份有限公司 一种发光聚对苯二甲酸乙二醇酯的制备方法
WO2014064710A1 (en) 2012-10-22 2014-05-01 Department Of Biotechnology A process for the prepartion of non-viral vector for delivery of nucleic acids by mucosal route
WO2015066717A1 (en) 2013-11-04 2015-05-07 BioPharmX, Inc. Dosage form comprising an active ingredient and a plurality of solid porous microcarriers
JP6326896B2 (ja) * 2014-03-25 2018-05-23 富士ゼロックス株式会社 ゾルゲルシリカ粒子、静電荷像現像用トナー、静電荷像現像剤、トナーカートリッジ、プロセスカートリッジ、画像形成装置及び画像形成方法
CN104109405B (zh) * 2014-07-28 2016-08-24 深圳市沃特新材料股份有限公司 表面改性的c-Si及其制备方法与应用
CN104649243B (zh) * 2015-02-11 2017-02-01 深圳新宙邦科技股份有限公司 一种磷酸镍中空纳米球及制备方法
US11129363B2 (en) * 2015-05-08 2021-09-28 The Florida International University Board Of Trustees Polymer-based training aids and methods of use
CN105482498A (zh) * 2015-11-30 2016-04-13 东华大学 一种有机磷杂化α-ZrP阻燃材料及其制备方法
CA3019132A1 (en) 2016-04-01 2017-10-05 NOHMs Technologies, Inc. Modified ionic liquids containing phosphorus
CN107055500B (zh) * 2017-03-08 2019-04-30 中国海洋大学 非水体系中制备三水磷酸氢镁
CN110785459B (zh) * 2017-06-23 2022-06-24 3M创新有限公司 具有含有被有机硅烷改性的二氧化硅纳米粒子的底漆层的膜
WO2019018432A1 (en) 2017-07-17 2019-01-24 NOHMs Technologies, Inc. ELECTROLYTES CONTAINING PHOSPHORUS
JP7098555B2 (ja) * 2018-03-02 2022-07-11 株式会社アルバック コアシェル型量子ドット分散液の製造方法及び量子ドット分散液の製造方法
RU2744126C1 (ru) * 2020-05-26 2021-03-02 Федеральное бюджетное учреждение науки "Федеральный научный центр медико-профилактических технологий управления рисками здоровью населения" Федеральной службы по надзору в сфере защиты прав потребителей и благополучия человека (ФБУН "ФНЦ медико-профилактических технологий управления рисками здоровью Способ модификации поверхности неорганических наночастиц - оксидов двухвалентных металлов, используемых для оценки токсического эффекта
IT202000021292A1 (it) * 2020-09-09 2022-03-09 Consiglio Nazionale Ricerche Composizione in forma di polvere a base di microparticelle incorporanti nanoparticelle per la veicolazione di composti terapeutici/diagnostici
CN112176330A (zh) * 2020-10-10 2021-01-05 苏州特密达新材料有限公司 一种用于金属表面钝化的纳米硅烷处理剂
CN113876601B (zh) * 2021-09-30 2023-09-29 宁波爱诗化妆品有限公司 一种化妆品用改性无定形磷酸三钙及其制备方法
CN114451423B (zh) * 2021-12-27 2023-04-14 杭州同晨环保科技有限公司 一种边缘有机修饰的磷酸锆载铜抗菌剂
CN114479780B (zh) * 2022-02-22 2023-05-30 西南石油大学 一种双亲改性纳米颗粒及其乳状液和抗高温高密度可逆油基钻井液
CN116144191B (zh) * 2022-09-09 2024-12-31 中科广化（重庆）新材料研究院有限公司 一种利用植物木质纤维制备的可降解塑料及其制备方法
CN115678314B (zh) * 2022-09-27 2024-03-08 南昌航空大学 一种有机-无机复合磷酸盐的制备方法
CN115717001B (zh) * 2022-11-21 2024-02-06 桂林电子科技大学 一种磷硅酸包覆炭黑及其制备方法和应用

Family Cites Families (23)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP3218401B2 (ja) * 1991-08-02 2001-10-15 日本化学工業株式会社 防錆顔料組成物
JP3653760B2 (ja) * 1994-12-07 2005-06-02 東ソー株式会社 層状リン酸スズ化合物およびその製造方法
WO2000046147A2 (en) 1999-02-03 2000-08-10 Biosante Pharmaceuticals, Inc. Therapeutic calcium phosphate particles and methods of manufacture and use
GB0006050D0 (en) * 2000-03-14 2000-05-03 Johnson Matthey Plc Liquid gold compositions
US6426114B1 (en) * 2000-05-02 2002-07-30 The University Of British Columbia Sol-gel calcium phosphate ceramic coatings and method of making same
US7241399B2 (en) * 2000-09-08 2007-07-10 Centrum Fuer Angewandte Nanotechnologie (Can) Gmbh Synthesis of nanoparticles
WO2002020695A1 (de) * 2000-09-08 2002-03-14 Nanosolutions Gmbh Dotierte nanopartikel
FR2823992B1 (fr) * 2001-04-27 2003-06-20 Rhodia Chimie Sa Dispersions d'hydroxyapatite comprenant un acide amine en tant qu'agent stabilisant, et leur procede de preparation
JP3893966B2 (ja) * 2001-12-18 2007-03-14 Ｊｓｒ株式会社 保護膜の形成方法とそのための組成物
FR2839657B1 (fr) 2002-05-14 2004-08-13 Rhodia Chimie Sa Dispersion colloidale de nanoparticules de phosphate de calcium et d'au moins une proteine, ainsi que les nanoparticules redispersables et les particules calcinees correspondantes, procede de preparation et utilisations
AU2004233873B2 (en) * 2003-04-25 2010-11-18 The Penn State Research Foundation Method and system for systemic delivery of growth arresting, lipid-derived bioactive compounds
US20040242729A1 (en) * 2003-05-30 2004-12-02 3M Innovative Properties Company Stabilized particle dispersions containing surface-modified inorganic nanoparticles
US7459146B2 (en) * 2003-05-30 2008-12-02 3M Innovative Properties Company Stabilized aerosol dispersions
US7169375B2 (en) * 2003-08-29 2007-01-30 General Electric Company Metal oxide nanoparticles, methods of making, and methods of use
CN1942396B (zh) * 2004-03-15 2010-09-01 苏黎世联合高等工业学校 金属盐纳米颗粒，特别是包含钙和磷酸根的纳米颗粒的火焰合成
US7410631B2 (en) * 2005-03-02 2008-08-12 Aps Laboratory Metal phosphate sols, metal nanoparticles, metal-chalcogenide nanoparticles, and nanocomposites made therefrom
JP2006299126A (ja) * 2005-04-21 2006-11-02 Nissan Motor Co Ltd ナノフィラーの表面改質方法、ポリマーナノコンポジット及びポリマーナノコンポジットの製造方法
JP2006315871A (ja) * 2005-05-10 2006-11-24 Pentax Corp リン酸カルシウム系化合物ナノ粒子、その分散液およびそれらの製造方法
CA2617909C (en) * 2005-08-05 2014-02-04 3M Innovative Properties Company Compositions exhibiting improved flowability
US8287914B2 (en) * 2006-01-12 2012-10-16 Rutgers, The State University Of New Jersey Biomimetic hydroxyapatite synthesis
JP2008056513A (ja) * 2006-08-30 2008-03-13 Masahiko Abe リン酸カルシウム粒子の製造方法、略球状リン酸カルシウム粒子、（亜）リン酸エステルの使用、リン酸源
US20080069887A1 (en) * 2006-09-15 2008-03-20 3M Innovative Properties Company Method for nanoparticle surface modification
US20110039947A1 (en) 2008-05-08 2011-02-17 3M Innovative Properties Company Surface-modified nanoparticles

Also Published As

Publication number Publication date
CN102089317B (zh) 2016-10-19
JP2011520015A (ja) 2011-07-14
JP2011519816A (ja) 2011-07-14
CN102089317A (zh) 2011-06-08
WO2009137592A3 (en) 2010-03-25
US20110039947A1 (en) 2011-02-17
WO2009137595A2 (en) 2009-11-12
WO2009137592A2 (en) 2009-11-12
EP2291460A2 (en) 2011-03-09
WO2009137595A3 (en) 2010-03-25
US8404876B2 (en) 2013-03-26
EP2297172B1 (en) 2012-06-27
CN102076784A (zh) 2011-05-25
US20110046404A1 (en) 2011-02-24
EP2297172A2 (en) 2011-03-23

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