JP5479502B2 - 電気透析法による沈降シリカを含有する高純度懸濁液の製造 - Google Patents

電気透析法による沈降シリカを含有する高純度懸濁液の製造 Download PDF

Info

Publication number
JP5479502B2
JP5479502B2 JP2011553454A JP2011553454A JP5479502B2 JP 5479502 B2 JP5479502 B2 JP 5479502B2 JP 2011553454 A JP2011553454 A JP 2011553454A JP 2011553454 A JP2011553454 A JP 2011553454A JP 5479502 B2 JP5479502 B2 JP 5479502B2
Authority
JP
Japan
Prior art keywords
suspension
precipitated silica
electrodialysis
anolyte
catholyte
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
JP2011553454A
Other languages
English (en)
Japanese (ja)
Other versions
JP2012520168A5 (enExample
JP2012520168A (ja
Inventor
シュテナー パトリク
チュンケ フローリアン
ベーニッシュ ユルゲン
ルーフ マルクス
ダンネール マンフレート
ズーア ズィルケ
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Evonik Operations GmbH
Original Assignee
Evonik Degussa GmbH
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Evonik Degussa GmbH filed Critical Evonik Degussa GmbH
Publication of JP2012520168A publication Critical patent/JP2012520168A/ja
Publication of JP2012520168A5 publication Critical patent/JP2012520168A5/ja
Application granted granted Critical
Publication of JP5479502B2 publication Critical patent/JP5479502B2/ja
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00—Silicon; Compounds thereof
    • C01B33/113—Silicon oxides; Hydrates thereof
    • C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
    • C01B33/14—Colloidal silica, e.g. dispersions, gels, sols
    • C01B33/141—Preparation of hydrosols or aqueous dispersions
    • C01B33/1415—Preparation of hydrosols or aqueous dispersions by suspending finely divided silica in water
    • C01B33/1417—Preparation of hydrosols or aqueous dispersions by suspending finely divided silica in water an aqueous dispersion being obtained
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D61/00—Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
    • B01D61/42—Electrodialysis; Electro-osmosis ; Electro-ultrafiltration; Membrane capacitive deionization
    • B01D61/44—Ion-selective electrodialysis
    • B01D61/46—Apparatus therefor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D61/00—Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
    • B01D61/42—Electrodialysis; Electro-osmosis ; Electro-ultrafiltration; Membrane capacitive deionization
    • B01D61/44—Ion-selective electrodialysis
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00—Silicon; Compounds thereof
    • C01B33/113—Silicon oxides; Hydrates thereof
    • C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
    • C01B33/18—Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof
    • C01B33/187—Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof by acidic treatment of silicates
    • C01B33/193—Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof by acidic treatment of silicates of aqueous solutions of silicates
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
    • C09C1/28—Compounds of silicon
    • C09C1/30—Silicic acid
    • D—TEXTILES; PAPER
    • D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H19/00—Coated paper; Coating material
    • D21H19/36—Coatings with pigments
    • D21H19/38—Coatings with pigments characterised by the pigments
    • D21H19/40—Coatings with pigments characterised by the pigments siliceous, e.g. clays
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2311/00—Details relating to membrane separation process operations and control
    • B01D2311/04—Specific process operations in the feed stream; Feed pretreatment
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2311/00—Details relating to membrane separation process operations and control
    • B01D2311/14—Pressure control
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2313/00—Details relating to membrane modules or apparatus
    • B01D2313/34—Energy carriers
    • B01D2313/345—Electrodes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B41—PRINTING; LINING MACHINES; TYPEWRITERS; STAMPS
    • B41M—PRINTING, DUPLICATING, MARKING, OR COPYING PROCESSES; COLOUR PRINTING
    • B41M5/00—Duplicating or marking methods; Sheet materials for use therein
    • B41M5/50—Recording sheets characterised by the coating used to improve ink, dye or pigment receptivity, e.g. for ink-jet or thermal dye transfer recording
    • B41M5/52—Macromolecular coatings
    • B41M5/5218—Macromolecular coatings characterised by inorganic additives, e.g. pigments, clays
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C01P2004/61—Micrometer sized, i.e. from 1-100 micrometer
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C01P2004/62—Submicrometer sized, i.e. from 0.1-1 micrometer
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/80—Compositional purity

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Dispersion Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Water Supply & Treatment (AREA)
  • Inorganic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Urology & Nephrology (AREA)
  • Health & Medical Sciences (AREA)
  • Silicon Compounds (AREA)
  • Separation Using Semi-Permeable Membranes (AREA)
  • Electrolytic Production Of Non-Metals, Compounds, Apparatuses Therefor (AREA)
  • Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
JP2011553454A 2009-03-12 2010-03-11 電気透析法による沈降シリカを含有する高純度懸濁液の製造 Expired - Fee Related JP5479502B2 (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
DE102009001512.4 2009-03-12
DE200910001512 DE102009001512A1 (de) 2009-03-12 2009-03-12 Herstellung von hochreinen Suspensionen enthaltend gefällte Kieselsäuren durch Elektrodialyse
PCT/EP2010/053098 WO2010103068A1 (en) 2009-03-12 2010-03-11 Production of high-purity suspensions containing precipitated silicas by electrodialysis

Publications (3)

Publication Number Publication Date
JP2012520168A JP2012520168A (ja) 2012-09-06
JP2012520168A5 JP2012520168A5 (enExample) 2013-03-28
JP5479502B2 true JP5479502B2 (ja) 2014-04-23

Family

ID=42174082

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2011553454A Expired - Fee Related JP5479502B2 (ja) 2009-03-12 2010-03-11 電気透析法による沈降シリカを含有する高純度懸濁液の製造

Country Status (13)

Country Link
US (1) US20110302849A1 (enExample)
EP (1) EP2405993A1 (enExample)
JP (1) JP5479502B2 (enExample)
KR (1) KR20110137304A (enExample)
CN (1) CN102348493A (enExample)
BR (1) BRPI1008938A2 (enExample)
CA (1) CA2755058A1 (enExample)
DE (1) DE102009001512A1 (enExample)
MX (1) MX2011009262A (enExample)
RU (1) RU2538594C2 (enExample)
TW (1) TWI465397B (enExample)
WO (1) WO2010103068A1 (enExample)
ZA (1) ZA201106627B (enExample)

Families Citing this family (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2014087748A (ja) * 2012-10-30 2014-05-15 Mitsui Eng & Shipbuild Co Ltd 液間イオン移送方法及び液間イオン移送装置
CN103112926A (zh) * 2012-11-30 2013-05-22 姜英杰 一种节能节水离子交换器在苦咸水淡化中的应用
CN106865555B (zh) * 2017-03-20 2018-09-18 淮南联合大学 一种利用双极膜电渗析制备药用辅料二氧化硅的方法
EP3932862A1 (de) 2020-07-01 2022-01-05 Evonik Operations GmbH Funktionalisiertes graphen, verfahren zur herstellung eines funktionalisierten graphens und dessen verwendung
EP3954743A1 (de) 2020-08-12 2022-02-16 Evonik Operations GmbH Verwendung von siliziumdioxid zur verbesserung der leitfähigkeit von beschichtungen
CN112642295B (zh) * 2020-12-23 2022-05-27 中国科学院青海盐湖研究所 一种电渗析提纯系统及固相体系的提纯方法
CN114659932A (zh) * 2021-12-10 2022-06-24 安徽力普拉斯电源技术有限公司 胶体电池电解质密度的检测方法及其误差校正方法
CA3246944A1 (en) 2022-04-08 2023-10-12 Knauf Gips Kg DESALINATION OF HIGH ABSORPTION POROUS CHLORIDE BEADS
US12390791B2 (en) 2022-04-08 2025-08-19 Knauf Gips Kg Desalination of high chloride salt absorbed porous beads
CN118059681B (zh) * 2024-04-11 2024-11-01 浙江尚辰化工有限公司 一种多组分增光剂除杂工艺方法

Family Cites Families (35)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2854316A (en) * 1955-02-03 1958-09-30 Columbia Southern Chem Corp Process for purifying silica
GB815154A (en) * 1956-02-20 1959-06-17 Permutit Co Ltd Improvements relating to electrodialysis processes
GB1115532A (en) * 1964-10-19 1968-05-29 Foremost Dairies Inc Improvements in or relating to electrodialysis process and apparatus
US3523880A (en) * 1967-12-27 1970-08-11 Ionics Electrolytic cell for removal and recovery of so2 from waste gases
US3661762A (en) * 1967-12-27 1972-05-09 Ionics Electrolytic cell for removal and recovery of so2 from waste gases
US4094771A (en) 1976-01-13 1978-06-13 Deutsche Gold- Und Silber-Scheideanstalt Vormals Roessler Process for preparation of a sprayable precipitated silicic acid suspension
US4508607A (en) * 1982-10-18 1985-04-02 W. R. Grace & Co. Particulate dialytic silica
DE3568946D1 (en) * 1984-07-09 1989-04-27 Millipore Corp Improved electrodeionization apparatus and method
SU1333716A1 (ru) * 1986-04-21 1987-08-30 Предприятие П/Я А-1001 Электролизер дл разделени ионов
US4740281A (en) * 1986-10-14 1988-04-26 Allied Corporation Recovery of acids from materials comprising acid and salt
FR2646665B1 (fr) * 1989-05-03 1991-11-29 Rhone Poulenc Chimie Silice pour compositions dentifrices compatible notamment avec les cations metalliques
US5135626A (en) * 1988-12-01 1992-08-04 Allied-Signal Inc. Method for purification of bases from materials comprising base and salt
US4976838A (en) * 1988-12-01 1990-12-11 Allied-Signal Inc. Method for purification of bases from materials comprising base and salt
US5200046A (en) * 1990-12-12 1993-04-06 Allied-Signal Inc. Apparatus and method for electrodialytic treatment of salts to produce acid and/or base of improved purity
US6375735B1 (en) * 1996-05-06 2002-04-23 Agritec, Inc. Precipitated silicas, silica gels with and free of deposited carbon from caustic biomass ash solutions and processes
JP3485291B2 (ja) * 1996-06-25 2004-01-13 株式会社荏原製作所 固形微細粒子懸濁液の濃縮方法及び装置
AUPO264096A0 (en) * 1996-09-30 1996-10-24 Mclaughlin Geosurveys Pty Ltd. Value improvement of clays
US5972191A (en) * 1997-01-17 1999-10-26 Archer Daniels Midland Company Electrodialysis apparatus
JP3104128B2 (ja) * 1997-08-08 2000-10-30 強化土エンジニヤリング株式会社 地盤注入用材、その製造装置および注入方法
DE19807700A1 (de) 1998-02-24 1999-08-26 Degussa Fällungskieselsäuregranulate
JP3963583B2 (ja) * 1998-07-31 2007-08-22 東曹産業株式会社 珪酸ゾルの製造方法および地盤注入薬の製造方法
JP2001072409A (ja) 1999-09-01 2001-03-21 Kyokado Eng Co Ltd 高純度シリカの製造方法および利用方法
US6274020B1 (en) * 2000-04-28 2001-08-14 Ernst Schmidt Electrodialysis membrane and gasket stack system
AU2002211736A1 (en) * 2000-10-13 2002-04-22 University Of Cincinnati Methods for synthesizing precipitated silica and use thereof
FR2818630B1 (fr) 2000-12-26 2003-10-03 Rhodia Chimie Sa Procede pour la preparation de sols de silice
JP4290348B2 (ja) * 2001-03-21 2009-07-01 東曹産業株式会社 珪酸アルカリ水溶液の製造方法
JP4014896B2 (ja) * 2001-05-25 2007-11-28 株式会社トクヤマ 水処理用凝集剤の製造方法
CN1131350C (zh) * 2001-08-30 2003-12-17 上海交通大学 草浆黑液的碱回收新工艺
JP2003181459A (ja) * 2001-12-18 2003-07-02 Asahi Glass Co Ltd 脱イオン水の製造方法
DE10256267A1 (de) * 2002-12-03 2004-06-24 Degussa Ag Dispersion, Streichfarbe und Aufnahmemedium
US6946119B2 (en) * 2003-02-14 2005-09-20 J.M. Huber Corporation Precipitated silica product with low surface area, dentifrices containing same, and processes
EP1559744A1 (en) * 2004-01-30 2005-08-03 Rhodia Chimie Use of a pretreated precipitated silica as a reinforcing filler for silicone elastomer and curable compositions thus obtained
JP2008178847A (ja) * 2007-01-26 2008-08-07 Sumitomo Chemical Co Ltd 電気透析装置
WO2008130580A1 (en) * 2007-04-19 2008-10-30 Trovion Pte Ltd. Methods and apparatus for electrodeionization
CN101224889A (zh) * 2008-02-01 2008-07-23 湖南金马硅业有限公司 应用膜分离技术对超细二氧化硅洗涤提纯的新工艺

Also Published As

Publication number Publication date
RU2011141185A (ru) 2013-04-20
WO2010103068A1 (en) 2010-09-16
ZA201106627B (en) 2012-05-30
TW201100328A (en) 2011-01-01
RU2538594C2 (ru) 2015-01-10
CN102348493A (zh) 2012-02-08
TWI465397B (zh) 2014-12-21
CA2755058A1 (en) 2010-09-16
EP2405993A1 (en) 2012-01-18
DE102009001512A1 (de) 2010-09-16
JP2012520168A (ja) 2012-09-06
KR20110137304A (ko) 2011-12-22
US20110302849A1 (en) 2011-12-15
MX2011009262A (es) 2011-09-26
BRPI1008938A2 (pt) 2016-03-15

Similar Documents

Publication Publication Date Title
JP5479502B2 (ja) 電気透析法による沈降シリカを含有する高純度懸濁液の製造
CN107428544B (zh) 二氧化硅系复合微粒分散液、其制造方法以及包含二氧化硅系复合微粒分散液的研磨用浆料
JP5383373B2 (ja) 沈降珪酸、その製造法および該化合物の使用
EP3447790B1 (en) Silica-based composite fine particle dispersion and method for manufacturing same
JP3411585B2 (ja) 沈降シリカを基材とする担体に液体を吸収させてなる組成物
TWI537211B (zh) 純化強酸或強酸性介質以移除二及更高價之金屬離子的方法
CN106334524B (zh) 核-壳结构层状双金属氢氧化物复合粒子制备方法及应用
JP5844480B2 (ja) 沈澱シリカ製造方法
JP6008642B2 (ja) 平板状結晶性アルミナ複合酸化物微粒子集合体、平板状結晶性アルミナ複合酸化物微粒子集合体からなる結晶性アルミナ複合酸化物粒子ならびに該平板状結晶性アルミナ複合酸化物微粒子集合体および該結晶性アルミナ複合酸化物粒子の製造方法
JP2009517324A (ja) ナノ気孔シリカの製造装置及びその製造方法
CN106672986A (zh) 沉淀二氧化硅制备方法
JP4646205B2 (ja) 消泡剤組成物のための親水性の沈降ケイ酸
RU2720206C1 (ru) Сферические частицы на основе кремнезема и способы их получения
JP2005231990A (ja) 消泡剤組成物用の疎水性の沈降ケイ酸
CN104326477B (zh) 一种电容器用超高纯硅溶胶的制备方法
JP2012520168A5 (enExample)
EP3530622A1 (en) Halloysite powder and method for producing halloysite powder
KR950006634B1 (ko) 실리카, 그의 제조방법 및 특히 종이용 충진제로서의 용도
JP4502133B2 (ja) 酸性水性アルミナゾルの製造方法
CN104870085B (zh) 二氧化硅‑氧化铝组合物的制备
JP7441163B2 (ja) シリカ微粒子分散液およびその製造方法
KR102850317B1 (ko) 구상 실리카 입자의 제조 방법
CN101269976A (zh) LaPO4包覆α－Al2O3粉体的水热制备方法
KR101227198B1 (ko) 실리카의 화학-보조 분쇄
JP4632022B2 (ja) アルミナ粉末及びアルミナゾルの製造方法γ

Legal Events

Date Code Title Description
A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20130207

A621 Written request for application examination

Free format text: JAPANESE INTERMEDIATE CODE: A621

Effective date: 20130207

A977 Report on retrieval

Free format text: JAPANESE INTERMEDIATE CODE: A971007

Effective date: 20130911

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20130924

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20131216

TRDD Decision of grant or rejection written
A01 Written decision to grant a patent or to grant a registration (utility model)

Free format text: JAPANESE INTERMEDIATE CODE: A01

Effective date: 20140114

A61 First payment of annual fees (during grant procedure)

Free format text: JAPANESE INTERMEDIATE CODE: A61

Effective date: 20140212

R150 Certificate of patent or registration of utility model

Ref document number: 5479502

Country of ref document: JP

Free format text: JAPANESE INTERMEDIATE CODE: R150

LAPS Cancellation because of no payment of annual fees