JP5424897B2 - パラタングステン酸アンモニウム水和物を製造する方法及びパラタングステン酸アンモニウム十水和物 - Google Patents
パラタングステン酸アンモニウム水和物を製造する方法及びパラタングステン酸アンモニウム十水和物 Download PDFInfo
- Publication number
- JP5424897B2 JP5424897B2 JP2009547657A JP2009547657A JP5424897B2 JP 5424897 B2 JP5424897 B2 JP 5424897B2 JP 2009547657 A JP2009547657 A JP 2009547657A JP 2009547657 A JP2009547657 A JP 2009547657A JP 5424897 B2 JP5424897 B2 JP 5424897B2
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- Prior art keywords
- mixer
- phase
- ammonia
- organic phase
- ammonium paratungstate
- Prior art date
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G41/00—Compounds of tungsten
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G41/00—Compounds of tungsten
- C01G41/003—Preparation involving a liquid-liquid extraction, an adsorption or an ion-exchange
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2002/00—Crystal-structural characteristics
- C01P2002/01—Crystal-structural characteristics depicted by a TEM-image
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2002/00—Crystal-structural characteristics
- C01P2002/60—Compounds characterised by their crystallite size
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2002/00—Crystal-structural characteristics
- C01P2002/70—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
- C01P2002/72—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by d-values or two theta-values, e.g. as X-ray diagram
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/01—Particle morphology depicted by an image
- C01P2004/03—Particle morphology depicted by an image obtained by SEM
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/54—Particles characterised by their aspect ratio, i.e. the ratio of sizes in the longest to the shortest dimension
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/10—Solid density
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/11—Powder tap density
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/80—Compositional purity
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/29—Coated or structually defined flake, particle, cell, strand, strand portion, rod, filament, macroscopic fiber or mass thereof
- Y10T428/2982—Particulate matter [e.g., sphere, flake, etc.]
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Inorganic Compounds Of Heavy Metals (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE102007005286A DE102007005286B4 (de) | 2007-02-02 | 2007-02-02 | Verfahren zur Herstellung von Ammoniumparawolframathydraten und Ammoniumparawolframatdekahydrat |
| DE102007005286.5 | 2007-02-02 | ||
| PCT/EP2008/050995 WO2008092837A1 (de) | 2007-02-02 | 2008-01-29 | Verfahren zur herstellung von ammoniumparawolframathydraten und ammoniumparawolframatdekahydrat |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2010517902A JP2010517902A (ja) | 2010-05-27 |
| JP2010517902A5 JP2010517902A5 (enExample) | 2013-09-05 |
| JP5424897B2 true JP5424897B2 (ja) | 2014-02-26 |
Family
ID=39400947
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2009547657A Active JP5424897B2 (ja) | 2007-02-02 | 2008-01-29 | パラタングステン酸アンモニウム水和物を製造する方法及びパラタングステン酸アンモニウム十水和物 |
Country Status (8)
| Country | Link |
|---|---|
| US (2) | US8216533B2 (enExample) |
| EP (1) | EP2118017B1 (enExample) |
| JP (1) | JP5424897B2 (enExample) |
| CN (1) | CN101600654B (enExample) |
| DE (2) | DE102007005286B4 (enExample) |
| ES (1) | ES2608681T3 (enExample) |
| PT (1) | PT2118017T (enExample) |
| WO (1) | WO2008092837A1 (enExample) |
Families Citing this family (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE102007005285B4 (de) * | 2007-02-02 | 2009-06-25 | H.C. Starck Gmbh | Verfahren zur Herstellung von Ammoniumheptamolybdat |
| DE102007005287B4 (de) * | 2007-02-02 | 2009-10-01 | H.C. Starck Gmbh | Verfahren zur Herstellung von Ammoniumparawolframattetrahydrat und hochreines Ammoniumparawolframattetrahydrat |
| JP4797099B2 (ja) * | 2009-10-01 | 2011-10-19 | Jx日鉱日石金属株式会社 | 高純度タングステン粉末の製造方法 |
| CN203085734U (zh) | 2010-05-19 | 2013-07-24 | 法国圣戈班玻璃厂 | 混合天线构造 |
| DE212012000003U1 (de) | 2011-02-16 | 2012-09-06 | Saint-Gobain Glass France | Transparente Scheibe mit elektrischer Heizschicht |
| US9751498B2 (en) | 2011-03-22 | 2017-09-05 | Saint-Gobain Glass France | Method and arrangement for de-icing a transparent window using an electric heating device |
| CN110790312B (zh) * | 2019-11-13 | 2022-05-17 | 厦门钨业股份有限公司 | 利用含钨废料制备仲钨酸铵的方法 |
| CN111689520B (zh) * | 2020-06-17 | 2023-04-18 | 赣州有色冶金研究所有限公司 | 一种二段真空制备十水合仲钨酸铵的方法 |
| CN113816429B (zh) * | 2021-11-12 | 2023-04-18 | 江西钨业股份有限公司 | 仲钨酸铵的颗粒粗化方法 |
| CN117401715A (zh) * | 2023-11-01 | 2024-01-16 | 中南大学 | 一种从粗钨酸钠溶液制备偏钨酸铵与仲钨酸铵的方法 |
| WO2025168426A1 (en) | 2024-02-09 | 2025-08-14 | Saint-Gobain Sekurit France | Windshield with heating layer and optimized arrangement of an integrated temperature sensor |
Family Cites Families (21)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE150962C (enExample) | ||||
| US3052516A (en) * | 1959-02-10 | 1962-09-04 | Gen Mills Inc | Process for recovering tungsten values from solution |
| DE1150962B (de) | 1959-02-10 | 1963-07-04 | Gen Mills Inc | Verfahren zur Abtrennung von Wolframverbindungen aus waessrigen, wolframhaltigen Loesungen |
| US3158438A (en) * | 1962-09-19 | 1964-11-24 | Union Carbide Corp | Solvent extraction process for recovering tungsten values from contaminated aqueous solutions |
| DE1244141B (de) | 1962-10-26 | 1967-07-13 | Blair Burwell | Verfahren zur Herstellung von hochreinem Ammoniumparawolframat |
| US4092400A (en) | 1977-04-11 | 1978-05-30 | Engelhard Minerals & Chemicals Corp. | Process for recovering high purity tungsten compositions from wolframite ores |
| US4175109A (en) * | 1978-08-03 | 1979-11-20 | Gte Sylvania Incorporated | Process for extracting tungsten from alkali metal tungstate solutions |
| US4279869A (en) * | 1979-12-13 | 1981-07-21 | Kerr-Mcgee Corporation | Process for recovering concentrated, purified tungsten values from brine |
| US4450144A (en) * | 1981-01-19 | 1984-05-22 | Amax Inc. | Ammonium hydroxide stripping of tungsten from organic solvents |
| US4346061A (en) * | 1981-03-31 | 1982-08-24 | Union Carbide Corporation | Purification of ammonium tungstate solutions |
| US4508701A (en) * | 1983-03-31 | 1985-04-02 | Union Carbide Corporation | Extraction of tungsten from spent or scrap catalyst materials |
| US4448755A (en) * | 1983-12-01 | 1984-05-15 | Gte Products Corporation | Method for removal of tin from ammonium tungstates |
| US4613182A (en) * | 1984-08-27 | 1986-09-23 | Stone Jack C | Side panel assembly |
| US4624844A (en) * | 1985-02-04 | 1986-11-25 | Gte Products Corporation | Process for producing ammonium paratungstate |
| US4612183A (en) * | 1985-02-25 | 1986-09-16 | Gte Products Corporation | Method of producing crystalline ammonium metatungstate |
| US4623534A (en) * | 1985-03-21 | 1986-11-18 | Gte Products Corporation | Method for producing ammonium paratungstate |
| US4882131A (en) * | 1987-04-30 | 1989-11-21 | Gte Products Corporation | Process for recovering tungsten from organic solutions |
| US4963336A (en) * | 1989-09-25 | 1990-10-16 | Amax Inc. | Purification of APT |
| US5417945A (en) * | 1990-08-22 | 1995-05-23 | Gte Products Corporation | Process for recovering tungsten as an ammoniacal tungstate compound in which ammoniacal tungstate liquors are reclaimed |
| DE102007005287B4 (de) | 2007-02-02 | 2009-10-01 | H.C. Starck Gmbh | Verfahren zur Herstellung von Ammoniumparawolframattetrahydrat und hochreines Ammoniumparawolframattetrahydrat |
| DE102007005285B4 (de) | 2007-02-02 | 2009-06-25 | H.C. Starck Gmbh | Verfahren zur Herstellung von Ammoniumheptamolybdat |
-
2007
- 2007-02-02 DE DE102007005286A patent/DE102007005286B4/de active Active
- 2007-02-02 DE DE102007063691A patent/DE102007063691B4/de not_active Expired - Fee Related
-
2008
- 2008-01-29 CN CN2008800039606A patent/CN101600654B/zh active Active
- 2008-01-29 EP EP08708312.7A patent/EP2118017B1/de active Active
- 2008-01-29 US US12/524,957 patent/US8216533B2/en active Active
- 2008-01-29 JP JP2009547657A patent/JP5424897B2/ja active Active
- 2008-01-29 WO PCT/EP2008/050995 patent/WO2008092837A1/de not_active Ceased
- 2008-01-29 PT PT87083127T patent/PT2118017T/pt unknown
- 2008-01-29 ES ES08708312.7T patent/ES2608681T3/es active Active
-
2012
- 2012-05-29 US US13/482,075 patent/US8440161B2/en active Active
Also Published As
| Publication number | Publication date |
|---|---|
| DE102007005286B4 (de) | 2009-08-27 |
| WO2008092837A1 (de) | 2008-08-07 |
| US20100098619A1 (en) | 2010-04-22 |
| JP2010517902A (ja) | 2010-05-27 |
| US20130029153A1 (en) | 2013-01-31 |
| PT2118017T (pt) | 2016-12-14 |
| DE102007063691B4 (de) | 2011-01-13 |
| US8440161B2 (en) | 2013-05-14 |
| DE102007005286A8 (de) | 2008-12-24 |
| EP2118017A1 (de) | 2009-11-18 |
| CN101600654B (zh) | 2013-05-29 |
| CN101600654A (zh) | 2009-12-09 |
| US8216533B2 (en) | 2012-07-10 |
| EP2118017B1 (de) | 2016-10-12 |
| DE102007005286A1 (de) | 2008-08-07 |
| ES2608681T3 (es) | 2017-04-12 |
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