JP5336368B2 - マクロ孔質カチオン交換樹脂を製造する方法 - Google Patents
マクロ孔質カチオン交換樹脂を製造する方法 Download PDFInfo
- Publication number
- JP5336368B2 JP5336368B2 JP2009522920A JP2009522920A JP5336368B2 JP 5336368 B2 JP5336368 B2 JP 5336368B2 JP 2009522920 A JP2009522920 A JP 2009522920A JP 2009522920 A JP2009522920 A JP 2009522920A JP 5336368 B2 JP5336368 B2 JP 5336368B2
- Authority
- JP
- Japan
- Prior art keywords
- cation exchange
- aqueous phase
- exchange resin
- monomer
- porogen
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F2/00—Processes of polymerisation
- C08F2/32—Polymerisation in water-in-oil emulsions
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
- B01D15/08—Selective adsorption, e.g. chromatography
- B01D15/26—Selective adsorption, e.g. chromatography characterised by the separation mechanism
- B01D15/36—Selective adsorption, e.g. chromatography characterised by the separation mechanism involving ionic interaction, e.g. ion-exchange, ion-pair, ion-suppression or ion-exclusion
- B01D15/361—Ion-exchange
- B01D15/362—Cation-exchange
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J39/00—Cation exchange; Use of material as cation exchangers; Treatment of material for improving the cation exchange properties
- B01J39/08—Use of material as cation exchangers; Treatment of material for improving the cation exchange properties
- B01J39/16—Organic material
- B01J39/18—Macromolecular compounds
- B01J39/20—Macromolecular compounds obtained by reactions only involving unsaturated carbon-to-carbon bonds
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J39/00—Cation exchange; Use of material as cation exchangers; Treatment of material for improving the cation exchange properties
- B01J39/26—Cation exchangers for chromatographic processes
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F2/00—Processes of polymerisation
- C08F2/12—Polymerisation in non-solvents
- C08F2/16—Aqueous medium
- C08F2/18—Suspension polymerisation
- C08F2/20—Suspension polymerisation with the aid of macromolecular dispersing agents
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J5/00—Manufacture of articles or shaped materials containing macromolecular substances
- C08J5/20—Manufacture of shaped structures of ion-exchange resins
- C08J5/22—Films, membranes or diaphragms
- C08J5/2206—Films, membranes or diaphragms based on organic and/or inorganic macromolecular compounds
- C08J5/2218—Synthetic macromolecular compounds
- C08J5/2231—Synthetic macromolecular compounds based on macromolecular compounds obtained by reactions involving unsaturated carbon-to-carbon bonds
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J2333/00—Characterised by the use of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and only one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Derivatives of such polymers
- C08J2333/24—Homopolymers or copolymers of amides or imides
- C08J2333/26—Homopolymers or copolymers of acrylamide or methacrylamide
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/249921—Web or sheet containing structurally defined element or component
- Y10T428/249953—Composite having voids in a component [e.g., porous, cellular, etc.]
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Engineering & Computer Science (AREA)
- Manufacturing & Machinery (AREA)
- Analytical Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Materials Engineering (AREA)
- Treatment Of Liquids With Adsorbents In General (AREA)
- Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
- Filtering Materials (AREA)
- Manufacture Of Porous Articles, And Recovery And Treatment Of Waste Products (AREA)
- Peptides Or Proteins (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US11/460,826 US7674836B2 (en) | 2006-07-28 | 2006-07-28 | Method of making macroporous cation exchange resins |
| US11/460,826 | 2006-07-28 | ||
| PCT/US2007/073571 WO2008014137A1 (en) | 2006-07-28 | 2007-07-16 | Method of making macroporous cation exchange resins |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2009544835A JP2009544835A (ja) | 2009-12-17 |
| JP2009544835A5 JP2009544835A5 (https=) | 2010-09-02 |
| JP5336368B2 true JP5336368B2 (ja) | 2013-11-06 |
Family
ID=38686867
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2009522920A Expired - Fee Related JP5336368B2 (ja) | 2006-07-28 | 2007-07-16 | マクロ孔質カチオン交換樹脂を製造する方法 |
Country Status (4)
| Country | Link |
|---|---|
| US (2) | US7674836B2 (https=) |
| EP (1) | EP2046877B1 (https=) |
| JP (1) | JP5336368B2 (https=) |
| WO (1) | WO2008014137A1 (https=) |
Families Citing this family (23)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| AU2005295757A1 (en) * | 2004-10-15 | 2006-04-27 | 3M Innovative Properties Company | Pleated multi-layer filter media and cartridge |
| US7674835B2 (en) * | 2005-12-21 | 2010-03-09 | 3M Innovative Properties Company | Method of making macroporous anion exchange resins |
| US7683100B2 (en) * | 2005-12-21 | 2010-03-23 | 3M Innovative Properties Company | Method of making macroporous cation exchange resins |
| US7674836B2 (en) * | 2006-07-28 | 2010-03-09 | 3M Innovative Properties Company | Method of making macroporous cation exchange resins |
| WO2009061759A1 (en) | 2007-11-09 | 2009-05-14 | 3M Innovative Properties Company | Porous polymeric resins |
| CN102959018B (zh) | 2010-06-25 | 2015-11-25 | 3M创新有限公司 | 半互穿聚合物网络 |
| CN104093754B (zh) | 2011-11-21 | 2017-06-23 | 3M创新有限公司 | 用于储存并递送活性剂的聚合物粒子 |
| SG10201701224UA (en) * | 2012-03-12 | 2017-04-27 | Merck Patent Gmbh | Removal of protein aggregates from biopharmaceutical preparations in a flowthrough mode |
| KR20150023331A (ko) * | 2012-05-31 | 2015-03-05 | 에이전시 포 사이언스, 테크놀로지 앤드 리서치 | 음으로 대전된 입자들로의 폴리뉴클레오티드들의 크로마토그래피 정제 |
| JP6576335B2 (ja) * | 2013-10-03 | 2019-09-18 | スリーエム イノベイティブ プロパティズ カンパニー | 結合能力が向上したリガンド官能化基材 |
| CN109689189B (zh) | 2016-09-09 | 2022-02-01 | 3M创新有限公司 | 官能化共聚物及其使用 |
| US20190194250A1 (en) * | 2016-09-09 | 2019-06-27 | 3M Innovative Properties Company | Processes for separating aggregated proteins from monomeric proteins in a biological solution |
| US10927228B2 (en) | 2017-11-16 | 2021-02-23 | 3M Innovative Properties Company | Polymer matrix composites comprising intumescent particles and methods of making the same |
| CN111357061B (zh) | 2017-11-16 | 2022-04-12 | 3M创新有限公司 | 包含介电粒子的聚合物基质复合材料及其制备方法 |
| US10836873B2 (en) | 2017-11-16 | 2020-11-17 | 3M Innovative Properties Company | Polymer matrix composites comprising thermally insulating particles and methods of making the same |
| US10913834B2 (en) | 2017-11-16 | 2021-02-09 | 3M Innovative Properties Company | Polymer matrix composites comprising indicator particles and methods of making the same |
| TW201925296A (zh) | 2017-11-16 | 2019-07-01 | 美商3M新設資產公司 | 製造聚合物基質複合物之方法 |
| JP7308828B2 (ja) | 2017-11-16 | 2023-07-14 | スリーエム イノベイティブ プロパティズ カンパニー | 機能性粒子を含むポリマーマトリックス複合体及びその製造方法 |
| CN108043463B (zh) * | 2017-11-27 | 2020-10-16 | 天津工业大学 | 一种用于二氧化碳资源化的高性能催化剂及其制备方法 |
| US20210001278A1 (en) * | 2017-12-04 | 2021-01-07 | King Abdullah University Of Science And Technology | Methods of making porous membranes |
| US20230203221A1 (en) | 2020-04-14 | 2023-06-29 | 3M Innovative Properties Company | Monomers, polymers, and articles for biomaterial capture |
| CN112588272B (zh) * | 2020-11-23 | 2023-01-24 | 扬州工业职业技术学院 | 一种黄酮类物质吸附剂及其制备方法 |
| CN115487875A (zh) * | 2022-10-17 | 2022-12-20 | 蚌埠市天星树脂有限责任公司 | 一种改性酸性阳离子交换树脂及其用途 |
Family Cites Families (54)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2527300A (en) * | 1948-03-18 | 1950-10-24 | American Cyanamid Co | Copolymers of unsaturated sulfonic acids and polyunsaturated compounds |
| US3058594A (en) * | 1960-06-06 | 1962-10-16 | Purolator Products Inc | Pleated paper filter |
| CS171962B1 (https=) * | 1974-02-01 | 1976-11-29 | ||
| CS177507B1 (https=) * | 1974-02-12 | 1977-07-29 | ||
| US3929741A (en) * | 1974-07-16 | 1975-12-30 | Datascope Corp | Hydrophilic acrylamido polymers |
| US4071508A (en) * | 1975-02-11 | 1978-01-31 | Plastomedical Sciences, Inc. | Anionic hydrogels based on hydroxyalkyl acrylates and methacrylates |
| US4134815A (en) * | 1976-05-31 | 1979-01-16 | Ici Australia Limited | Amphoteric composite resins and method of preparing same by polymerization of a two-phase dispersion of monomers |
| US4153661A (en) * | 1977-08-25 | 1979-05-08 | Minnesota Mining And Manufacturing Company | Method of making polytetrafluoroethylene composite sheet |
| JPS54100489A (en) * | 1978-01-26 | 1979-08-08 | Asahi Chem Ind Co Ltd | New basic crosslinked copolymer and its preparation |
| US4157418A (en) * | 1978-02-08 | 1979-06-05 | Minnesota Mining And Manufacturing Company | Acrylic functional aminocarboxylic acids and derivatives as components of pressure sensitive adhesives |
| FR2482112B1 (fr) | 1980-05-09 | 1985-06-07 | Pharmindustrie | Nouveaux copolymeres hydrophiles a base de n-(tris (hydroxymethyl) methyl) acrylamide, procedes pour leur preparation, gels aqueux desdits copolymeres et leur utilisation comme echangeurs d'ions |
| JPS57158209A (en) * | 1981-03-25 | 1982-09-30 | Kao Corp | Production of bead-form highly water-absorbing polymer |
| US4565663A (en) * | 1981-06-26 | 1986-01-21 | Minnesota Mining And Manufacturing Company | Method for making water-swellable composite sheet |
| US4436874A (en) * | 1981-11-19 | 1984-03-13 | Societe D'expansion Scientifique "Expansia" | Acrylic copolymers and their use in solid phase peptide synthesis |
| US4552939A (en) * | 1983-12-19 | 1985-11-12 | Exxon Research And Engineering Co. | Preparation of sulfonated copolymers by suspension copolymerization |
| US4833198A (en) * | 1985-07-22 | 1989-05-23 | The Dow Chemical Company | Suspending agent for the suspension polymerization of water-soluble monomers |
| US5336742A (en) * | 1987-03-13 | 1994-08-09 | Minnesota Mining And Manufacturing Company | Polymeric supports |
| US4842739A (en) * | 1987-08-20 | 1989-06-27 | Minnesota Mining And Manufacturing Company | High surface area filter cartridge |
| US4810381A (en) * | 1987-12-28 | 1989-03-07 | Minnesota Mining And Manufacturing Company | Composite chromatographic article |
| US4971736A (en) * | 1987-12-28 | 1990-11-20 | Minnesota Mining And Manufacturing Company | Method of preparing composite chromatographic article |
| US6323249B1 (en) * | 1988-09-26 | 2001-11-27 | Purolite International, Ltd. | Macroporous resins having large pores but with high crush strength |
| US4957943A (en) * | 1988-10-14 | 1990-09-18 | Minnesota Mining And Manufacturing Company | Particle-filled microporous materials |
| US5264125A (en) * | 1989-09-08 | 1993-11-23 | Ionics' Incorporated | Process for manufacturing continuous supported ion selective membranes using non-polymerizable high boiling point solvents |
| US5171808A (en) * | 1990-06-11 | 1992-12-15 | American Cyanamid Company | Cross-linked anionic and amphoteric polymeric microparticles |
| US5037858A (en) * | 1990-06-21 | 1991-08-06 | Ionics, Incorporated | Anion selective polymers prepared from concentrated solutions of N,N'-methylenebisacrylamide |
| US5104729A (en) * | 1990-08-20 | 1992-04-14 | Monsanto Company | Process for surface modifying a support membrane and product produced |
| US5993935A (en) * | 1991-10-11 | 1999-11-30 | 3M Innovative Properties Company | Covalently reactive particles incorporated in a continous porous matrix |
| JP3301628B2 (ja) | 1992-03-06 | 2002-07-15 | 日立化成工業株式会社 | りん酸基を有する陽イオン交換樹脂及びその製造法 |
| US5906734A (en) * | 1992-06-19 | 1999-05-25 | Biosepra Inc. | Passivated porous polymer supports and methods for the preparation and use of same |
| DE69329676T2 (de) * | 1992-06-19 | 2001-03-15 | Life Technologies, Inc. | Passivierte und stabilisierte träger und methoden zu deren herstellung und verwendung |
| JPH06228215A (ja) | 1993-02-03 | 1994-08-16 | Dainippon Ink & Chem Inc | 感温性多孔質重合体の製造方法 |
| JPH06228216A (ja) | 1993-02-03 | 1994-08-16 | Dainippon Ink & Chem Inc | pH応答性多孔質重合体の製造方法 |
| US5468847A (en) * | 1994-03-10 | 1995-11-21 | Minnesota Mining And Manufacturing Company | Method of isolating and purifying a biomacromolecule |
| US5561097A (en) * | 1994-04-28 | 1996-10-01 | Minnesota Mining And Manufacturing Company | Method of controlling density of ligand coupled onto supports and products produced therefrom |
| AUPM587094A0 (en) * | 1994-05-25 | 1994-06-16 | Poseidon Scientific Instruments Pty Ltd | Microwave loop oscillators |
| FR2722097B1 (fr) * | 1994-07-11 | 1997-05-16 | Oreal | Composition cosmetique et/ou dermatologique gelifiee, riche en solvant et contenant des particules creuses, ses application |
| US5906747A (en) * | 1995-11-13 | 1999-05-25 | Biosepra Inc. | Separation of molecules from dilute solutions using composite chromatography media having high dynamic sorptive capacity at high flow rates |
| US6059975A (en) * | 1997-09-02 | 2000-05-09 | Lockheed Martin Energy Research Corporation | Bifunctional anion-exchange resins with improved selectivity and exchange kinetics |
| DE19907023A1 (de) | 1999-02-19 | 2000-08-24 | Bayer Ag | Verfahren zur Isolierung von Nucleinsäuren |
| US6423666B1 (en) | 1999-10-05 | 2002-07-23 | Bio-Rad Laboratories, Inc. | Large-pore chromatographic beads prepared by suspension polymerization |
| DE19959264A1 (de) * | 1999-12-03 | 2001-07-12 | Elipsa Gmbh | Templat-geprägte Kompositmaterialien mit hoher Bindungsspezifität und Selektivität, Verfahren zu ihrer Herstellung und ihre Verwendung |
| DE10009982A1 (de) * | 2000-03-03 | 2001-09-06 | Qiagen Gmbh | Polymere Anionenaustauscher und deren Verwendung in chromatographischen Verfahren |
| WO2002000337A1 (en) | 2000-06-27 | 2002-01-03 | Bia Separations D.O.O. | A chromatography material and a process of manufacturing that material |
| DE10033583A1 (de) * | 2000-07-11 | 2002-01-24 | Bayer Ag | Superparamagnetische Perlpolymerisate |
| BR0113999A (pt) * | 2000-09-21 | 2003-08-12 | Rohm & Haas | Processo para preparar uma dispersão polimérica aquosa nanocompósita de argila, dispersão nanocompósita aquosa, espessador, dispersante, aglutinante, composição de tinta flexográfica, verniz de sobre impressão, modificador de pó de cimento seco, semente polimérica nanocompósita de argila, composição polimérica nanocompósita de argila, e, método para preparar uma pluralidade de partìculas poliméricas nanocompósitas de argila ocas |
| US6783838B2 (en) | 2001-04-30 | 2004-08-31 | 3M Innovative Properties Company | Coated film laminate having an ionic surface |
| FR2824734B1 (fr) * | 2001-05-16 | 2003-06-27 | Oreal | Composition pulverulente pour la decoloration des fibres keratiniques humaines |
| US6756462B2 (en) * | 2001-07-03 | 2004-06-29 | Rohm And Haas Company | Method for preparation of anion exchange resins |
| FI20011575A0 (fi) * | 2001-07-26 | 2001-07-26 | Fortum Oyj | Polttoainekomponentit ja niiden selektiiviset valmistusmenetelmät |
| US7098253B2 (en) * | 2004-05-20 | 2006-08-29 | 3M Innovative Properties Company | Macroporous ion exchange resins |
| JP5032324B2 (ja) * | 2004-10-01 | 2012-09-26 | スリーエム イノベイティブ プロパティズ カンパニー | 複合濾過物品 |
| US7674835B2 (en) * | 2005-12-21 | 2010-03-09 | 3M Innovative Properties Company | Method of making macroporous anion exchange resins |
| US7683100B2 (en) * | 2005-12-21 | 2010-03-23 | 3M Innovative Properties Company | Method of making macroporous cation exchange resins |
| US7674836B2 (en) * | 2006-07-28 | 2010-03-09 | 3M Innovative Properties Company | Method of making macroporous cation exchange resins |
-
2006
- 2006-07-28 US US11/460,826 patent/US7674836B2/en active Active
-
2007
- 2007-07-16 JP JP2009522920A patent/JP5336368B2/ja not_active Expired - Fee Related
- 2007-07-16 WO PCT/US2007/073571 patent/WO2008014137A1/en not_active Ceased
- 2007-07-16 EP EP07812958.2A patent/EP2046877B1/en not_active Not-in-force
-
2010
- 2010-01-20 US US12/690,334 patent/US8349906B2/en not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| EP2046877A1 (en) | 2009-04-15 |
| WO2008014137A1 (en) | 2008-01-31 |
| JP2009544835A (ja) | 2009-12-17 |
| US8349906B2 (en) | 2013-01-08 |
| US7674836B2 (en) | 2010-03-09 |
| EP2046877B1 (en) | 2016-02-17 |
| US20100116739A1 (en) | 2010-05-13 |
| US20080027153A1 (en) | 2008-01-31 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| JP5336368B2 (ja) | マクロ孔質カチオン交換樹脂を製造する方法 | |
| JP5144535B2 (ja) | マクロ孔質カチオン交換樹脂の製造方法 | |
| CN101341195B (zh) | 制备大孔阴离子交换树脂的方法 | |
| JP5814360B2 (ja) | 半相互貫入ポリマー網状組織 | |
| JP5426564B2 (ja) | 多孔質高分子樹脂 | |
| JP4988574B2 (ja) | マクロ孔質イオン交換樹脂 |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| A521 | Request for written amendment filed |
Free format text: JAPANESE INTERMEDIATE CODE: A523 Effective date: 20100716 |
|
| A621 | Written request for application examination |
Free format text: JAPANESE INTERMEDIATE CODE: A621 Effective date: 20100716 |
|
| A977 | Report on retrieval |
Free format text: JAPANESE INTERMEDIATE CODE: A971007 Effective date: 20120711 |
|
| A131 | Notification of reasons for refusal |
Free format text: JAPANESE INTERMEDIATE CODE: A131 Effective date: 20120717 |
|
| TRDD | Decision of grant or rejection written | ||
| A01 | Written decision to grant a patent or to grant a registration (utility model) |
Free format text: JAPANESE INTERMEDIATE CODE: A01 Effective date: 20130702 |
|
| A61 | First payment of annual fees (during grant procedure) |
Free format text: JAPANESE INTERMEDIATE CODE: A61 Effective date: 20130801 |
|
| R150 | Certificate of patent or registration of utility model |
Free format text: JAPANESE INTERMEDIATE CODE: R150 |
|
| LAPS | Cancellation because of no payment of annual fees |