JP4970699B2 - 脂肪族C1〜C4カルボン酸のt−ブチルエステルの製造方法 - Google Patents
脂肪族C1〜C4カルボン酸のt−ブチルエステルの製造方法 Download PDFInfo
- Publication number
- JP4970699B2 JP4970699B2 JP2002516242A JP2002516242A JP4970699B2 JP 4970699 B2 JP4970699 B2 JP 4970699B2 JP 2002516242 A JP2002516242 A JP 2002516242A JP 2002516242 A JP2002516242 A JP 2002516242A JP 4970699 B2 JP4970699 B2 JP 4970699B2
- Authority
- JP
- Japan
- Prior art keywords
- reactor
- section
- isobutene
- carboxylic acid
- nozzle
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C67/00—Preparation of carboxylic acid esters
- C07C67/04—Preparation of carboxylic acid esters by reacting carboxylic acids or symmetrical anhydrides onto unsaturated carbon-to-carbon bonds
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/582—Recycling of unreacted starting or intermediate materials
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE10036959.6 | 2000-07-28 | ||
| DE10036959A DE10036959A1 (de) | 2000-07-28 | 2000-07-28 | Verfahren zur Herstellung von tert.-Butylestern aliphatischer C1-C4-Carbonsäuren |
| PCT/EP2001/008710 WO2002010109A1 (de) | 2000-07-28 | 2001-07-27 | Verfahren zur herstellung von tert.-butylestern aliphatischer c1-c4-carbonsäuren |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2004505101A JP2004505101A (ja) | 2004-02-19 |
| JP2004505101A5 JP2004505101A5 (https=) | 2008-09-04 |
| JP4970699B2 true JP4970699B2 (ja) | 2012-07-11 |
Family
ID=7650633
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2002516242A Expired - Lifetime JP4970699B2 (ja) | 2000-07-28 | 2001-07-27 | 脂肪族C1〜C4カルボン酸のt−ブチルエステルの製造方法 |
Country Status (5)
| Country | Link |
|---|---|
| US (2) | US6756506B2 (https=) |
| EP (1) | EP1305275B1 (https=) |
| JP (1) | JP4970699B2 (https=) |
| DE (2) | DE10036959A1 (https=) |
| WO (1) | WO2002010109A1 (https=) |
Families Citing this family (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP2017255A1 (de) * | 2007-07-19 | 2009-01-21 | Basf Se | Verfahren zur Herstellung von teritären Alkylestern der (Meth)Acrylsäure mit mindestens 4 Kohlenstoffatomen im Alkylrest |
| EP2017293A1 (de) * | 2007-07-19 | 2009-01-21 | Basf Se | Gemische, enthaltend Inhibitoren der radikalischen Polymerisation und ionische Flüssigkeiten, und ihre Verwendung zur Stabilisierung von radikalisch polymerisierbaren Monomeren |
| CN104028177A (zh) * | 2013-03-06 | 2014-09-10 | 中石化上海工程有限公司 | 强化水力学反应设备混合效果的方法 |
| DE102015205752A1 (de) | 2015-03-31 | 2016-10-20 | Basf Se | Herstellung von tert-Butylestern aliphatischer Carbonsäuren |
| KR102568040B1 (ko) | 2015-06-17 | 2023-08-22 | 바스프 에스이 | 라디칼 중합의 즉시 중단을 위한 조성물 |
| EA035883B1 (ru) * | 2015-12-15 | 2020-08-27 | Басф Се | Получение трет-бутиловых эфиров этилен-ненасыщенных карбоновых кислот |
| CN109134176A (zh) * | 2018-10-24 | 2019-01-04 | 岳阳富和科技有限公司 | 一种利用混合c4醋酸酯化后分解生产高纯异丁烯的制造方法 |
| CN112920049B (zh) * | 2019-12-05 | 2022-07-15 | 湖南中创化工股份有限公司 | 一种制备乙酸叔丁酯的方法和装置 |
| CN112062678A (zh) * | 2020-09-24 | 2020-12-11 | 岳阳富和科技有限公司 | 一种丙烯酸叔丁酯生产过程中防止聚合的方法 |
| CN114507131B (zh) * | 2022-01-24 | 2024-08-06 | 华谊合丰特种化学淄博有限公司 | 一种(甲基)丙烯酸叔丁酯的合成方法 |
| CN120129670A (zh) | 2022-10-28 | 2025-06-10 | 巴斯夫欧洲公司 | 用于由可再生来源的乙醇制造感兴趣的丙烯衍生的化学品、特别是丙烯酸酯的方法 |
| EP4634150A1 (de) | 2022-12-15 | 2025-10-22 | Basf Se | Verfahren zur kontinuierlichen herstellung von tert.-butyl(meth)acrylat |
Family Cites Families (16)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3172905A (en) | 1965-03-09 | Catalytic preparation of esters from tertiary olefins and carboxylic acids | ||
| BE590370A (https=) | 1959-04-29 | 1900-01-01 | ||
| DE1128428B (de) | 1959-08-08 | 1962-04-26 | Hoechst Ag | Verfahren zur Herstellung von Carbonsaeure-tertiaer-alkylestern und zur Abtrennung und bzw. oder Gewinnung von tertiaeren Olefinen aus diese enthaltenden Kohlenwasserstoffgemischen |
| DE1135897B (de) | 1959-12-28 | 1962-09-06 | Basf Ag | Verfahren zur Herstellung von Tertiaer-butylestern der Acrylsaeure oder von in ª‡-Stellung durch Chlor oder Alkylreste substituierter Acrylsaeure |
| US3087962A (en) | 1960-01-21 | 1963-04-30 | Rohm & Haas | Process of making esters of acrylic and methacrylic acids |
| US3082246A (en) | 1960-02-17 | 1963-03-19 | Texaco Inc | Preparation of tertiary esters |
| US3031495A (en) | 1960-05-13 | 1962-04-24 | Sinclair Refining Co | Preparation of tertiary alkyl formate and acetate |
| DE1249857B (de) | 1961-03-29 | 1967-09-14 | Badische Anilin &. Soda-Fabnk Aktiengesellschaft, Ludwigshaf en/Rhem | Verfahren zur kontinuierlichen gewinnung von carbonsäureestern tertiärer alkohole. |
| US3088969A (en) | 1961-04-21 | 1963-05-07 | Standard Oil Co | Manufacture of t-butyl esters of unsaturated acids |
| DE3105399A1 (de) | 1981-02-14 | 1982-10-21 | EC Erdölchemie GmbH, 5000 Köln | Verfahren zur herstellung von carbonsaeureestern |
| JPS6263544A (ja) * | 1985-08-23 | 1987-03-20 | Nippon Shokubai Kagaku Kogyo Co Ltd | アクリル酸またはメタクリル酸のタ−シヤリ−ブチルエステルの製造方法 |
| JPH07116103B2 (ja) | 1986-11-27 | 1995-12-13 | 三菱レイヨン株式会社 | メタクリル酸t−ブチルの製造法 |
| US5762888A (en) * | 1994-11-25 | 1998-06-09 | Uop | Process and apparatus for discharging particles and fluid from a flow channel |
| DE19638567A1 (de) * | 1996-09-20 | 1998-03-26 | Bayer Ag | Mischer-Reaktor und Verfahren zur Durchführung von Reaktionen, insbesondere die Phosgenierung von primären Aminen |
| GB9815135D0 (en) * | 1998-07-14 | 1998-09-09 | Bp Chem Int Ltd | Ester synthesis |
| US6410804B1 (en) * | 1999-12-21 | 2002-06-25 | Exxon Mobil Oil Corporation | Production of phenol using reactive distillation |
-
2000
- 2000-07-28 DE DE10036959A patent/DE10036959A1/de not_active Withdrawn
-
2001
- 2001-07-27 EP EP01958028A patent/EP1305275B1/de not_active Expired - Lifetime
- 2001-07-27 WO PCT/EP2001/008710 patent/WO2002010109A1/de not_active Ceased
- 2001-07-27 JP JP2002516242A patent/JP4970699B2/ja not_active Expired - Lifetime
- 2001-07-27 DE DE50104555T patent/DE50104555D1/de not_active Expired - Lifetime
- 2001-07-27 US US10/334,000 patent/US6756506B2/en not_active Expired - Lifetime
-
2004
- 2004-02-03 US US10/769,911 patent/US20040158094A1/en not_active Abandoned
Also Published As
| Publication number | Publication date |
|---|---|
| DE50104555D1 (de) | 2004-12-23 |
| US20030181754A1 (en) | 2003-09-25 |
| DE10036959A1 (de) | 2002-02-07 |
| US20040158094A1 (en) | 2004-08-12 |
| WO2002010109A1 (de) | 2002-02-07 |
| EP1305275B1 (de) | 2004-11-17 |
| JP2004505101A (ja) | 2004-02-19 |
| EP1305275A1 (de) | 2003-05-02 |
| US6756506B2 (en) | 2004-06-29 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| TWI441808B (zh) | 製造丙烯酸的方法 | |
| US6433222B1 (en) | Method for producing acrylic acid | |
| JP4970699B2 (ja) | 脂肪族C1〜C4カルボン酸のt−ブチルエステルの製造方法 | |
| KR101372204B1 (ko) | 불포화 카르복실산 무수물의 연속적 제조 방법 | |
| CN100516006C (zh) | 易聚合的物质的制造方法 | |
| KR20090108099A (ko) | 아크릴산의 제조 방법 | |
| CN1275972A (zh) | 丙烯酸和甲基丙烯酸的制备方法 | |
| JPH101454A (ja) | (メタ)アクリル酸のアルキルエステルの連続的製造方法 | |
| JP4410935B2 (ja) | アクリル酸およびアクリル酸エステルを製造する方法 | |
| CN1343195A (zh) | 生产丙烯酸的方法 | |
| JP5021116B2 (ja) | アクリル酸およびアクリル酸エステルの製造方法 | |
| JPH09110789A (ja) | (メタ)アクリル酸のアルキルエステルを連続的に製造するための方法及び装置 | |
| JP2002509902A (ja) | アクリル酸及びアクリル酸エステルの製造法 | |
| KR20090092283A (ko) | 불포화 카르복실산 무수물의 개선된 제조 방법 | |
| CN115515923A (zh) | 丙烯酸制备中形成的包含于液体f中的迈克尔加合物的分解方法 | |
| JP2019501907A (ja) | エチレン性不飽和カルボン酸のtert−ブチルエステルの製造 | |
| US4824998A (en) | Process for producing tau-butyl methacrylate | |
| CN106795086A (zh) | 回收丙烯酸的方法和系统 | |
| US10053442B2 (en) | Preparation of dialkyl esters of 2,5-furandicarboxylic acid | |
| JP2013147501A (ja) | アルキル基中に少なくとも4個の炭素原子を有する(メタ)アクリル酸の3級アルキルエステルの製造法 | |
| JP6762957B2 (ja) | 脂肪族カルボン酸のtert−ブチルエステルの製造 | |
| CN87105726A (zh) | 不饱和羧酸酯的生产方法 | |
| JP4970700B2 (ja) | (メタ)アクリル酸のt−C4〜C8−アルキルエステルの製造方法 | |
| JP7664945B2 (ja) | メタクリル酸へのタンデムc-4酸化のための改良された安全な方法 | |
| US20230250045A1 (en) | Method for producing easily polymerizable compound |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| A521 | Request for written amendment filed |
Free format text: JAPANESE INTERMEDIATE CODE: A523 Effective date: 20080716 |
|
| A621 | Written request for application examination |
Free format text: JAPANESE INTERMEDIATE CODE: A621 Effective date: 20080716 |
|
| RD04 | Notification of resignation of power of attorney |
Free format text: JAPANESE INTERMEDIATE CODE: A7424 Effective date: 20101227 |
|
| RD04 | Notification of resignation of power of attorney |
Free format text: JAPANESE INTERMEDIATE CODE: A7424 Effective date: 20101228 |
|
| A977 | Report on retrieval |
Free format text: JAPANESE INTERMEDIATE CODE: A971007 Effective date: 20110512 |
|
| A131 | Notification of reasons for refusal |
Free format text: JAPANESE INTERMEDIATE CODE: A131 Effective date: 20110525 |
|
| A521 | Request for written amendment filed |
Free format text: JAPANESE INTERMEDIATE CODE: A523 Effective date: 20110823 |
|
| TRDD | Decision of grant or rejection written | ||
| A01 | Written decision to grant a patent or to grant a registration (utility model) |
Free format text: JAPANESE INTERMEDIATE CODE: A01 Effective date: 20120307 |
|
| A01 | Written decision to grant a patent or to grant a registration (utility model) |
Free format text: JAPANESE INTERMEDIATE CODE: A01 |
|
| A61 | First payment of annual fees (during grant procedure) |
Free format text: JAPANESE INTERMEDIATE CODE: A61 Effective date: 20120405 |
|
| FPAY | Renewal fee payment (event date is renewal date of database) |
Free format text: PAYMENT UNTIL: 20150413 Year of fee payment: 3 |
|
| R150 | Certificate of patent or registration of utility model |
Free format text: JAPANESE INTERMEDIATE CODE: R150 |
|
| R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
| R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
| R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
| R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
| R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |