JP4858165B2

JP4858165B2 - 静電荷像現像用トナー、静電荷像現像剤、トナーカートリッジ、プロセスカートリッジ及び画像形成装置

静電荷像現像用トナー、静電荷像現像剤、トナーカートリッジ、プロセスカートリッジ及び画像形成装置 Download PDF

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Publication number: JP4858165B2
Authority: JP; Japan
Prior art keywords: polyester resin; toner; mass; image; resin
Prior art date: 2006-12-28
Legal status : Active

Application number

JP2006355538A

Other languages

English (en)

Japanese (ja)

Other versions

JP2008165017A (ja

JP2008165017A5 (enrdf_load_stackoverflow

Inventor

慎平高木

則之水谷

真也中嶋

進吉野

聡吉田

Current Assignee

Fujifilm Business Innovation Corp

Original Assignee

Fuji Xerox Co Ltd

Fujifilm Business Innovation Corp

Priority date

2006-12-28

Filing date

2006-12-28

Publication date

2012-01-18

2006-12-28 Application filed by Fuji Xerox Co Ltd, Fujifilm Business Innovation Corp filed Critical Fuji Xerox Co Ltd

2006-12-28 Priority to JP2006355538A priority Critical patent/JP4858165B2/ja

2008-07-17 Publication of JP2008165017A publication Critical patent/JP2008165017A/ja

2010-02-12 Publication of JP2008165017A5 publication Critical patent/JP2008165017A5/ja

2012-01-18 Application granted granted Critical

2012-01-18 Publication of JP4858165B2 publication Critical patent/JP4858165B2/ja

Status Active legal-status Critical Current

2026-12-28 Anticipated expiration legal-status Critical

Links

238000000034 method Methods 0.000 title claims description 84
230000008569 process Effects 0.000 title claims description 23
229920001225 polyester resin Polymers 0.000 claims description 385
239000004645 polyester resin Substances 0.000 claims description 385
229920005989 resin Polymers 0.000 claims description 179
239000011347 resin Substances 0.000 claims description 179
238000012546 transfer Methods 0.000 claims description 86
KDYFGRWQOYBRFD-UHFFFAOYSA-N Succinic acid Natural products OC(=O)CCC(O)=O KDYFGRWQOYBRFD-UHFFFAOYSA-N 0.000 claims description 60
239000003795 chemical substances by application Substances 0.000 claims description 51
239000003086 colorant Substances 0.000 claims description 50
239000002253 acid Substances 0.000 claims description 48
KKEYFWRCBNTPAC-UHFFFAOYSA-N Terephthalic acid Chemical compound OC(=O)C1=CC=C(C(O)=O)C=C1 KKEYFWRCBNTPAC-UHFFFAOYSA-N 0.000 claims description 40
239000000178 monomer Substances 0.000 claims description 39
239000011230 binding agent Substances 0.000 claims description 31
239000000470 constituent Substances 0.000 claims description 29
LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 24
125000001931 aliphatic group Chemical group 0.000 claims description 24
125000000217 alkyl group Chemical group 0.000 claims description 23
125000003342 alkenyl group Chemical group 0.000 claims description 22
KDYFGRWQOYBRFD-NUQCWPJISA-N butanedioic acid Chemical compound O[14C](=O)CC[14C](O)=O KDYFGRWQOYBRFD-NUQCWPJISA-N 0.000 claims description 21
125000004432 carbon atom Chemical group C* 0.000 claims description 21
OFOBLEOULBTSOW-UHFFFAOYSA-N Malonic acid Chemical compound OC(=O)CC(O)=O OFOBLEOULBTSOW-UHFFFAOYSA-N 0.000 claims description 19
150000008064 anhydrides Chemical class 0.000 claims description 16
OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 15
239000001384 succinic acid Substances 0.000 claims description 15
229910052799 carbon Inorganic materials 0.000 claims description 13
150000008065 acid anhydrides Chemical class 0.000 claims description 10
239000007771 core particle Substances 0.000 claims description 8
125000005907 alkyl ester group Chemical group 0.000 claims description 7
VNGLVZLEUDIDQH-UHFFFAOYSA-N 4-[2-(4-hydroxyphenyl)propan-2-yl]phenol;2-methyloxirane Chemical compound CC1CO1.C=1C=C(O)C=CC=1C(C)(C)C1=CC=C(O)C=C1 VNGLVZLEUDIDQH-UHFFFAOYSA-N 0.000 claims description 3
WPSWDCBWMRJJED-UHFFFAOYSA-N 4-[2-(4-hydroxyphenyl)propan-2-yl]phenol;oxirane Chemical compound C1CO1.C=1C=C(O)C=CC=1C(C)(C)C1=CC=C(O)C=C1 WPSWDCBWMRJJED-UHFFFAOYSA-N 0.000 claims description 3
WEHZNZTWKUYVIY-UHFFFAOYSA-N 3-oxabicyclo[3.2.2]nona-1(7),5,8-triene-2,4-dione Chemical compound O=C1OC(=O)C2=CC=C1C=C2 WEHZNZTWKUYVIY-UHFFFAOYSA-N 0.000 claims description 2
239000002245 particle Substances 0.000 description 251
239000006185 dispersion Substances 0.000 description 231
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 96
HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 63
XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 description 48
238000003756 stirring Methods 0.000 description 46
KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 45
239000012071 phase Substances 0.000 description 42
238000006243 chemical reaction Methods 0.000 description 41
239000000203 mixture Substances 0.000 description 39
IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 36
-1 alkyl succinic acid, Chemical compound 0.000 description 36
238000002844 melting Methods 0.000 description 36
230000008018 melting Effects 0.000 description 36
239000002904 solvent Substances 0.000 description 34
230000009477 glass transition Effects 0.000 description 32
238000004519 manufacturing process Methods 0.000 description 29
239000000654 additive Substances 0.000 description 28
229920006038 crystalline resin Polymers 0.000 description 28
238000009826 distribution Methods 0.000 description 28
239000000243 solution Substances 0.000 description 28
108091008695 photoreceptors Proteins 0.000 description 27
239000003945 anionic surfactant Substances 0.000 description 26
238000005342 ion exchange Methods 0.000 description 25
230000000996 additive effect Effects 0.000 description 24
VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 23
238000005406 washing Methods 0.000 description 23
239000007864 aqueous solution Substances 0.000 description 22
VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 21
GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 description 21
239000000706 filtrate Substances 0.000 description 21
229910017604 nitric acid Inorganic materials 0.000 description 21
238000002360 preparation method Methods 0.000 description 21
LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 20
238000001816 cooling Methods 0.000 description 20
238000001914 filtration Methods 0.000 description 20
238000001291 vacuum drying Methods 0.000 description 20
QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 19
WYURNTSHIVDZCO-UHFFFAOYSA-N Tetrahydrofuran Chemical compound C1CCOC1 WYURNTSHIVDZCO-UHFFFAOYSA-N 0.000 description 19
230000002776 aggregation Effects 0.000 description 19
JGFBRKRYDCGYKD-UHFFFAOYSA-N dibutyl(oxo)tin Chemical compound CCCC[Sn](=O)CCCC JGFBRKRYDCGYKD-UHFFFAOYSA-N 0.000 description 19
238000004945 emulsification Methods 0.000 description 19
229920006127 amorphous resin Polymers 0.000 description 18
238000004140 cleaning Methods 0.000 description 18
230000000052 comparative effect Effects 0.000 description 18
238000005259 measurement Methods 0.000 description 17
229910052751 metal Inorganic materials 0.000 description 16
239000002184 metal Substances 0.000 description 16
229910052757 nitrogen Inorganic materials 0.000 description 16
239000000049 pigment Substances 0.000 description 16
238000003860 storage Methods 0.000 description 16
238000010438 heat treatment Methods 0.000 description 15
VZCYOOQTPOCHFL-OWOJBTEDSA-N Fumaric acid Chemical compound OC(=O)\C=C\C(O)=O VZCYOOQTPOCHFL-OWOJBTEDSA-N 0.000 description 14
238000004220 aggregation Methods 0.000 description 14
NLXLAEXVIDQMFP-UHFFFAOYSA-N Ammonium chloride Substances [NH4+].[Cl-] NLXLAEXVIDQMFP-UHFFFAOYSA-N 0.000 description 13
VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 description 13
235000011114 ammonium hydroxide Nutrition 0.000 description 13
238000006482 condensation reaction Methods 0.000 description 13
239000011162 core material Substances 0.000 description 13
230000018044 dehydration Effects 0.000 description 13
238000006297 dehydration reaction Methods 0.000 description 13
239000000155 melt Substances 0.000 description 13
239000012046 mixed solvent Substances 0.000 description 13
QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 12
239000000839 emulsion Substances 0.000 description 12
238000002156 mixing Methods 0.000 description 12
229920000642 polymer Polymers 0.000 description 12
239000000843 powder Substances 0.000 description 12
239000007787 solid Substances 0.000 description 12
CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 11
230000015572 biosynthetic process Effects 0.000 description 11
239000002270 dispersing agent Substances 0.000 description 11
239000003960 organic solvent Substances 0.000 description 11
150000003839 salts Chemical class 0.000 description 11
ZWEHNKRNPOVVGH-UHFFFAOYSA-N 2-Butanone Chemical compound CCC(C)=O ZWEHNKRNPOVVGH-UHFFFAOYSA-N 0.000 description 10
YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Natural products CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 10
238000005227 gel permeation chromatography Methods 0.000 description 10
GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 9
238000000576 coating method Methods 0.000 description 9
238000000113 differential scanning calorimetry Methods 0.000 description 9
239000007788 liquid Substances 0.000 description 9
239000004094 surface-active agent Substances 0.000 description 9
YLQBMQCUIZJEEH-UHFFFAOYSA-N tetrahydrofuran Natural products C=1C=COC=1 YLQBMQCUIZJEEH-UHFFFAOYSA-N 0.000 description 9
OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 description 9
UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 8
VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 description 8
230000007423 decrease Effects 0.000 description 8
238000001035 drying Methods 0.000 description 8
239000000377 silicon dioxide Substances 0.000 description 8
VZCYOOQTPOCHFL-UHFFFAOYSA-N trans-butenedioic acid Natural products OC(=O)C=CC(O)=O VZCYOOQTPOCHFL-UHFFFAOYSA-N 0.000 description 8
239000001993 wax Substances 0.000 description 8
DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 description 7
239000006229 carbon black Substances 0.000 description 7
150000001732 carboxylic acid derivatives Chemical class 0.000 description 7
239000003054 catalyst Substances 0.000 description 7
239000011248 coating agent Substances 0.000 description 7
239000011247 coating layer Substances 0.000 description 7
239000001530 fumaric acid Substances 0.000 description 7
239000010954 inorganic particle Substances 0.000 description 7
239000010410 layer Substances 0.000 description 7
239000000463 material Substances 0.000 description 7
ARCGXLSVLAOJQL-UHFFFAOYSA-N trimellitic acid Chemical compound OC(=O)C1=CC=C(C(O)=O)C(C(O)=O)=C1 ARCGXLSVLAOJQL-UHFFFAOYSA-N 0.000 description 7
150000007513 acids Chemical class 0.000 description 6
150000001298 alcohols Chemical class 0.000 description 6
230000000903 blocking effect Effects 0.000 description 6
230000003247 decreasing effect Effects 0.000 description 6
238000011161 development Methods 0.000 description 6
230000000694 effects Effects 0.000 description 6
230000004927 fusion Effects 0.000 description 6
230000005291 magnetic effect Effects 0.000 description 6
239000011164 primary particle Substances 0.000 description 6
239000003381 stabilizer Substances 0.000 description 6
239000000126 substance Substances 0.000 description 6
XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 5
XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 description 5
238000005054 agglomeration Methods 0.000 description 5
PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 5
239000008119 colloidal silica Substances 0.000 description 5
235000014113 dietary fatty acids Nutrition 0.000 description 5
RTZKZFJDLAIYFH-UHFFFAOYSA-N ether Substances CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 5
239000000194 fatty acid Substances 0.000 description 5
229930195729 fatty acid Natural products 0.000 description 5
239000002563 ionic surfactant Substances 0.000 description 5
230000003472 neutralizing effect Effects 0.000 description 5
QJGQUHMNIGDVPM-UHFFFAOYSA-N nitrogen group Chemical group [N] QJGQUHMNIGDVPM-UHFFFAOYSA-N 0.000 description 5
230000003746 surface roughness Effects 0.000 description 5
238000003786 synthesis reaction Methods 0.000 description 5
PGMMMHFNKZSYEP-UHFFFAOYSA-N 1,20-Eicosanediol Chemical compound OCCCCCCCCCCCCCCCCCCCCO PGMMMHFNKZSYEP-UHFFFAOYSA-N 0.000 description 4
QDCPNGVVOWVKJG-VAWYXSNFSA-N 2-[(e)-dodec-1-enyl]butanedioic acid Chemical compound CCCCCCCCCC\C=C\C(C(O)=O)CC(O)=O QDCPNGVVOWVKJG-VAWYXSNFSA-N 0.000 description 4
PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 4
OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical group OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 4
PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 4
PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 description 4
WNLRTRBMVRJNCN-UHFFFAOYSA-N adipic acid Chemical compound OC(=O)CCCCC(O)=O WNLRTRBMVRJNCN-UHFFFAOYSA-N 0.000 description 4
239000012736 aqueous medium Substances 0.000 description 4
239000012298 atmosphere Substances 0.000 description 4
AYJRCSIUFZENHW-UHFFFAOYSA-L barium carbonate Chemical compound [Ba+2].[O-]C([O-])=O AYJRCSIUFZENHW-UHFFFAOYSA-L 0.000 description 4
WPYMKLBDIGXBTP-UHFFFAOYSA-N benzoic acid Chemical compound OC(=O)C1=CC=CC=C1 WPYMKLBDIGXBTP-UHFFFAOYSA-N 0.000 description 4
IISBACLAFKSPIT-UHFFFAOYSA-N bisphenol A Chemical class C=1C=C(O)C=CC=1C(C)(C)C1=CC=C(O)C=C1 IISBACLAFKSPIT-UHFFFAOYSA-N 0.000 description 4
WERYXYBDKMZEQL-UHFFFAOYSA-N butane-1,4-diol Chemical compound OCCCCO WERYXYBDKMZEQL-UHFFFAOYSA-N 0.000 description 4
229910000019 calcium carbonate Inorganic materials 0.000 description 4
239000001506 calcium phosphate Substances 0.000 description 4
OSGAYBCDTDRGGQ-UHFFFAOYSA-L calcium sulfate Chemical compound [Ca+2].[O-]S([O-])(=O)=O OSGAYBCDTDRGGQ-UHFFFAOYSA-L 0.000 description 4
230000008859 change Effects 0.000 description 4
238000010586 diagram Methods 0.000 description 4
WOZVHXUHUFLZGK-UHFFFAOYSA-N dimethyl terephthalate Chemical compound COC(=O)C1=CC=C(C(=O)OC)C=C1 WOZVHXUHUFLZGK-UHFFFAOYSA-N 0.000 description 4
229910001873 dinitrogen Inorganic materials 0.000 description 4
150000002009 diols Chemical class 0.000 description 4
TVIDDXQYHWJXFK-UHFFFAOYSA-N dodecanedioic acid Chemical compound OC(=O)CCCCCCCCCCC(O)=O TVIDDXQYHWJXFK-UHFFFAOYSA-N 0.000 description 4
230000008030 elimination Effects 0.000 description 4
238000003379 elimination reaction Methods 0.000 description 4
238000011156 evaluation Methods 0.000 description 4
150000004665 fatty acids Chemical class 0.000 description 4
XXMIOPMDWAUFGU-UHFFFAOYSA-N hexane-1,6-diol Chemical compound OCCCCCCO XXMIOPMDWAUFGU-UHFFFAOYSA-N 0.000 description 4
125000002887 hydroxy group Chemical group [H]O* 0.000 description 4
239000011572 manganese Substances 0.000 description 4
238000000691 measurement method Methods 0.000 description 4
238000010907 mechanical stirring Methods 0.000 description 4
239000002609 medium Substances 0.000 description 4
LUUFSCNUZAYHAT-UHFFFAOYSA-N octadecane-1,18-diol Chemical compound OCCCCCCCCCCCCCCCCCCO LUUFSCNUZAYHAT-UHFFFAOYSA-N 0.000 description 4
239000011146 organic particle Substances 0.000 description 4
238000006068 polycondensation reaction Methods 0.000 description 4
CXMXRPHRNRROMY-UHFFFAOYSA-N sebacic acid Chemical compound OC(=O)CCCCCCCCC(O)=O CXMXRPHRNRROMY-UHFFFAOYSA-N 0.000 description 4
230000003068 static effect Effects 0.000 description 4
TYFQFVWCELRYAO-UHFFFAOYSA-N suberic acid Chemical compound OC(=O)CCCCCCC(O)=O TYFQFVWCELRYAO-UHFFFAOYSA-N 0.000 description 4
239000000758 substrate Substances 0.000 description 4
QORWJWZARLRLPR-UHFFFAOYSA-H tricalcium bis(phosphate) Chemical compound [Ca+2].[Ca+2].[Ca+2].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O QORWJWZARLRLPR-UHFFFAOYSA-H 0.000 description 4
229910000391 tricalcium phosphate Inorganic materials 0.000 description 4
229940078499 tricalcium phosphate Drugs 0.000 description 4
235000019731 tricalcium phosphate Nutrition 0.000 description 4
JIAARYAFYJHUJI-UHFFFAOYSA-L zinc dichloride Chemical compound [Cl-].[Cl-].[Zn+2] JIAARYAFYJHUJI-UHFFFAOYSA-L 0.000 description 4
WVDDGKGOMKODPV-UHFFFAOYSA-N Benzyl alcohol Chemical compound OCC1=CC=CC=C1 WVDDGKGOMKODPV-UHFFFAOYSA-N 0.000 description 3
OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 3
YMWUJEATGCHHMB-UHFFFAOYSA-N Dichloromethane Chemical compound ClCCl YMWUJEATGCHHMB-UHFFFAOYSA-N 0.000 description 3
BDAGIHXWWSANSR-UHFFFAOYSA-N Formic acid Chemical class OC=O BDAGIHXWWSANSR-UHFFFAOYSA-N 0.000 description 3
LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 description 3
MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 description 3
229920003171 Poly (ethylene oxide) Polymers 0.000 description 3
ZMANZCXQSJIPKH-UHFFFAOYSA-N Triethylamine Chemical compound CCN(CC)CC ZMANZCXQSJIPKH-UHFFFAOYSA-N 0.000 description 3
235000010724 Wisteria floribunda Nutrition 0.000 description 3
230000004931 aggregating effect Effects 0.000 description 3
229910021529 ammonia Inorganic materials 0.000 description 3
BTANRVKWQNVYAZ-UHFFFAOYSA-N butan-2-ol Chemical compound CCC(C)O BTANRVKWQNVYAZ-UHFFFAOYSA-N 0.000 description 3
239000011575 calcium Substances 0.000 description 3
229910052791 calcium Inorganic materials 0.000 description 3
150000001735 carboxylic acids Chemical class 0.000 description 3
239000010941 cobalt Substances 0.000 description 3
229910017052 cobalt Inorganic materials 0.000 description 3
GUTLYIVDDKVIGB-UHFFFAOYSA-N cobalt atom Chemical compound [Co] GUTLYIVDDKVIGB-UHFFFAOYSA-N 0.000 description 3
XCJYREBRNVKWGJ-UHFFFAOYSA-N copper(II) phthalocyanine Chemical compound [Cu+2].C12=CC=CC=C2C(N=C2[N-]C(C3=CC=CC=C32)=N2)=NC1=NC([C]1C=CC=CC1=1)=NC=1N=C1[C]3C=CC=CC3=C2[N-]1 XCJYREBRNVKWGJ-UHFFFAOYSA-N 0.000 description 3
239000007822 coupling agent Substances 0.000 description 3
230000007547 defect Effects 0.000 description 3
MTHSVFCYNBDYFN-UHFFFAOYSA-N diethylene glycol Chemical compound OCCOCCO MTHSVFCYNBDYFN-UHFFFAOYSA-N 0.000 description 3
150000002148 esters Chemical class 0.000 description 3
150000002170 ethers Chemical class 0.000 description 3
235000011187 glycerol Nutrition 0.000 description 3
230000002209 hydrophobic effect Effects 0.000 description 3
229920000728 polyester Polymers 0.000 description 3
238000006116 polymerization reaction Methods 0.000 description 3
BDERNNFJNOPAEC-UHFFFAOYSA-N propan-1-ol Chemical compound CCCO BDERNNFJNOPAEC-UHFFFAOYSA-N 0.000 description 3
235000013772 propylene glycol Nutrition 0.000 description 3
238000005507 spraying Methods 0.000 description 3
150000005846 sugar alcohols Polymers 0.000 description 3
125000000542 sulfonic acid group Chemical group 0.000 description 3
239000000725 suspension Substances 0.000 description 3
239000011787 zinc oxide Substances 0.000 description 3
235000014692 zinc oxide Nutrition 0.000 description 3
229910000859 α-Fe Inorganic materials 0.000 description 3
PUPZLCDOIYMWBV-UHFFFAOYSA-N (+/-)-1,3-Butanediol Chemical compound CC(O)CCO PUPZLCDOIYMWBV-UHFFFAOYSA-N 0.000 description 2
DSEKYWAQQVUQTP-XEWMWGOFSA-N (2r,4r,4as,6as,6as,6br,8ar,12ar,14as,14bs)-2-hydroxy-4,4a,6a,6b,8a,11,11,14a-octamethyl-2,4,5,6,6a,7,8,9,10,12,12a,13,14,14b-tetradecahydro-1h-picen-3-one Chemical compound C([C@H]1[C@]2(C)CC[C@@]34C)C(C)(C)CC[C@]1(C)CC[C@]2(C)[C@H]4CC[C@@]1(C)[C@H]3C[C@@H](O)C(=O)[C@@H]1C DSEKYWAQQVUQTP-XEWMWGOFSA-N 0.000 description 2
ALVZNPYWJMLXKV-UHFFFAOYSA-N 1,9-Nonanediol Chemical compound OCCCCCCCCCO ALVZNPYWJMLXKV-UHFFFAOYSA-N 0.000 description 2
OSNILPMOSNGHLC-UHFFFAOYSA-N 1-[4-methoxy-3-(piperidin-1-ylmethyl)phenyl]ethanone Chemical compound COC1=CC=C(C(C)=O)C=C1CN1CCCCC1 OSNILPMOSNGHLC-UHFFFAOYSA-N 0.000 description 2
RTBFRGCFXZNCOE-UHFFFAOYSA-N 1-methylsulfonylpiperidin-4-one Chemical compound CS(=O)(=O)N1CCC(=O)CC1 RTBFRGCFXZNCOE-UHFFFAOYSA-N 0.000 description 2
WOPLHDNLGYOSPG-UHFFFAOYSA-N 2-butylbutanedioic acid Chemical compound CCCCC(C(O)=O)CC(O)=O WOPLHDNLGYOSPG-UHFFFAOYSA-N 0.000 description 2
QDCPNGVVOWVKJG-UHFFFAOYSA-N 2-dodec-1-enylbutanedioic acid Chemical compound CCCCCCCCCCC=CC(C(O)=O)CC(O)=O QDCPNGVVOWVKJG-UHFFFAOYSA-N 0.000 description 2
229910002012 Aerosil® Inorganic materials 0.000 description 2
PAYRUJLWNCNPSJ-UHFFFAOYSA-N Aniline Chemical compound NC1=CC=CC=C1 PAYRUJLWNCNPSJ-UHFFFAOYSA-N 0.000 description 2
239000005711 Benzoic acid Substances 0.000 description 2
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