JP4406451B2 - 高レベル放射性廃液のガラス溶融方法 - Google Patents
高レベル放射性廃液のガラス溶融方法 Download PDFInfo
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- JP4406451B2 JP4406451B2 JP2007244041A JP2007244041A JP4406451B2 JP 4406451 B2 JP4406451 B2 JP 4406451B2 JP 2007244041 A JP2007244041 A JP 2007244041A JP 2007244041 A JP2007244041 A JP 2007244041A JP 4406451 B2 JP4406451 B2 JP 4406451B2
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- 239000011521 glass Substances 0.000 title claims description 160
- 238000002844 melting Methods 0.000 title claims description 42
- 230000008018 melting Effects 0.000 title claims description 42
- 239000010808 liquid waste Substances 0.000 title claims description 27
- 238000000034 method Methods 0.000 title claims description 26
- 230000002285 radioactive effect Effects 0.000 title claims description 26
- 239000007788 liquid Substances 0.000 claims description 65
- 239000011324 bead Substances 0.000 claims description 62
- 239000002699 waste material Substances 0.000 claims description 58
- 239000002994 raw material Substances 0.000 claims description 37
- 239000000203 mixture Substances 0.000 claims description 30
- 229910018072 Al 2 O 3 Inorganic materials 0.000 claims description 26
- 239000002927 high level radioactive waste Substances 0.000 claims description 7
- 238000006243 chemical reaction Methods 0.000 claims description 6
- 229910004298 SiO 2 Inorganic materials 0.000 claims description 5
- 238000010309 melting process Methods 0.000 claims description 5
- 238000002156 mixing Methods 0.000 claims description 5
- 239000000843 powder Substances 0.000 claims description 4
- 239000007864 aqueous solution Substances 0.000 claims description 3
- 239000003365 glass fiber Substances 0.000 claims description 3
- -1 B 2 O 3 Inorganic materials 0.000 claims description 2
- 238000010348 incorporation Methods 0.000 claims 1
- 239000012071 phase Substances 0.000 description 21
- 238000001556 precipitation Methods 0.000 description 11
- 238000004090 dissolution Methods 0.000 description 9
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 8
- JKWMSGQKBLHBQQ-UHFFFAOYSA-N diboron trioxide Chemical compound O=BOB=O JKWMSGQKBLHBQQ-UHFFFAOYSA-N 0.000 description 8
- 239000006060 molten glass Substances 0.000 description 8
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 7
- 229910052810 boron oxide Inorganic materials 0.000 description 5
- 238000010438 heat treatment Methods 0.000 description 5
- 238000005191 phase separation Methods 0.000 description 5
- 150000003839 salts Chemical class 0.000 description 5
- KKCBUQHMOMHUOY-UHFFFAOYSA-N sodium oxide Chemical compound [O-2].[Na+].[Na+] KKCBUQHMOMHUOY-UHFFFAOYSA-N 0.000 description 5
- 239000000470 constituent Substances 0.000 description 3
- 229910052796 boron Inorganic materials 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- 238000009375 geological disposal Methods 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 230000009257 reactivity Effects 0.000 description 2
- 239000000377 silicon dioxide Substances 0.000 description 2
- 229910001948 sodium oxide Inorganic materials 0.000 description 2
- ZOXJGFHDIHLPTG-UHFFFAOYSA-N Boron Chemical compound [B] ZOXJGFHDIHLPTG-UHFFFAOYSA-N 0.000 description 1
- ZOKXTWBITQBERF-UHFFFAOYSA-N Molybdenum Chemical compound [Mo] ZOKXTWBITQBERF-UHFFFAOYSA-N 0.000 description 1
- MXRIRQGCELJRSN-UHFFFAOYSA-N O.O.O.[Al] Chemical compound O.O.O.[Al] MXRIRQGCELJRSN-UHFFFAOYSA-N 0.000 description 1
- 238000009825 accumulation Methods 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- JLDSOYXADOWAKB-UHFFFAOYSA-N aluminium nitrate Chemical compound [Al+3].[O-][N+]([O-])=O.[O-][N+]([O-])=O.[O-][N+]([O-])=O JLDSOYXADOWAKB-UHFFFAOYSA-N 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- KGBXLFKZBHKPEV-UHFFFAOYSA-N boric acid Chemical compound OB(O)O KGBXLFKZBHKPEV-UHFFFAOYSA-N 0.000 description 1
- 239000005388 borosilicate glass Substances 0.000 description 1
- 238000002485 combustion reaction Methods 0.000 description 1
- 239000000498 cooling water Substances 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000002708 enhancing effect Effects 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 239000000156 glass melt Substances 0.000 description 1
- 239000007791 liquid phase Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 229910052750 molybdenum Inorganic materials 0.000 description 1
- 239000011733 molybdenum Substances 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 238000002203 pretreatment Methods 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- RPACBEVZENYWOL-XFULWGLBSA-M sodium;(2r)-2-[6-(4-chlorophenoxy)hexyl]oxirane-2-carboxylate Chemical compound [Na+].C=1C=C(Cl)C=CC=1OCCCCCC[C@]1(C(=O)[O-])CO1 RPACBEVZENYWOL-XFULWGLBSA-M 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000005303 weighing Methods 0.000 description 1
Images
Classifications
-
- G—PHYSICS
- G21—NUCLEAR PHYSICS; NUCLEAR ENGINEERING
- G21F—PROTECTION AGAINST X-RADIATION, GAMMA RADIATION, CORPUSCULAR RADIATION OR PARTICLE BOMBARDMENT; TREATING RADIOACTIVELY CONTAMINATED MATERIAL; DECONTAMINATION ARRANGEMENTS THEREFOR
- G21F9/00—Treating radioactively contaminated material; Decontamination arrangements therefor
- G21F9/04—Treating liquids
- G21F9/06—Processing
- G21F9/16—Processing by fixation in stable solid media
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
- C03B1/00—Preparing the batches
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B09—DISPOSAL OF SOLID WASTE; RECLAMATION OF CONTAMINATED SOIL
- B09B—DISPOSAL OF SOLID WASTE NOT OTHERWISE PROVIDED FOR
- B09B3/00—Destroying solid waste or transforming solid waste into something useful or harmless
- B09B3/20—Agglomeration, binding or encapsulation of solid waste
- B09B3/25—Agglomeration, binding or encapsulation of solid waste using mineral binders or matrix
- B09B3/29—Agglomeration, binding or encapsulation of solid waste using mineral binders or matrix involving a melting or softening step
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
- C03B3/00—Charging the melting furnaces
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C1/00—Ingredients generally applicable to manufacture of glasses, glazes, or vitreous enamels
- C03C1/002—Use of waste materials, e.g. slags
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P40/00—Technologies relating to the processing of minerals
- Y02P40/50—Glass production, e.g. reusing waste heat during processing or shaping
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P40/00—Technologies relating to the processing of minerals
- Y02P40/50—Glass production, e.g. reusing waste heat during processing or shaping
- Y02P40/57—Improving the yield, e-g- reduction of reject rates
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S588/00—Hazardous or toxic waste destruction or containment
- Y10S588/901—Compositions
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Chemical & Material Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Environmental & Geological Engineering (AREA)
- Physics & Mathematics (AREA)
- General Engineering & Computer Science (AREA)
- High Energy & Nuclear Physics (AREA)
- Glass Compositions (AREA)
Description
請求項6の発明は、ガラス原料が、粒径2〜3mmのガラスビーズからなる請求項1〜5のいずれかに記載の高レベル放射性廃液のガラス溶融方法である。
シリカ(SiO2) 48.5 重量%
酸化ホウ素(B2O3) 14.8 重量%
アルミナ(Al2O3) 5.2 重量%
酸化ナトリウム(Na2O) 10 重量%
その他(廃液等) 21.5 重量%
とする必要がある。
シリカ(SiO2) 57.6 重量%
酸化ホウ素(B2O3) 17.6 重量%
アルミナ(Al2O3) 6.2 重量%
酸化ナトリウム(Na2O) 7.5 重量%
その他(廃液等) 11.1 重量%
のガラスビーズが使用される。
シリカ(SiO2) 62.7 重量%
酸化ホウ素(B2O3) 16.8 重量%
アルミナ(Al2O3) 0 重量%
酸化ナトリウム(Na2O) 8.2 重量%
その他 12.3 重量%
従来例においては、廃液15.8重量%に対してガラスビーズを84.2重量%加えて溶融処理し、実施例1においては、酸化ホウ素を重量比で約12重量%(1.7重量部)を廃液側に、またアルミナの全量(5.2重量部)を廃液側に混入して溶融処理した。
同様に表1に示すガラスビーズ組成に関して、標準燃焼廃液をガラスビーズに混ぜて実験用小型メルターに入れてガラス固化させた試験を行い、実際の運転プロセスを模擬した方法でも効果があるかどうか確認した。
12 主電極
19 キャニスタ
20 溶融ガラス
22 ガラスビーズ
26 高レベル放射性廃液
Claims (7)
- Mo成分を含む高レベル放射性廃液と、SiO 2 、B 2 O 3 、Al 2 O 3 、Na 2 Oを含むガラス原料とをガラス溶融炉内に投入して高レベル放射性廃液をガラスにて溶融固化する高レベル放射性廃液のガラス溶融方法において、前記ガラス原料組成中のB2O3及び/又はAl2O3の含有量を少なくして前記Mo成分との溶融初期反応が良好となる低粘性のガラス原料として前記ガラス溶融炉に投入し、他方、投入前の廃液にガラス原料組成中の含有量を少なくした量のB2O3及び/又はAl2O3を混入して廃液とすると共にこれを前記ガラス溶融炉に投入してガラス溶融させることを特徴とする高レベル放射性廃液のガラス溶融方法。
- B2O3及び/又はAl2O3を、そのまま粉体として投入前の廃液に予め混入する請求項1記載の高レベル放射性廃液のガラス溶融方法。
- B2O3を、H3BO4、として、Al2O3を、Al(OH)3、又はAl(NO3)3の水溶液として投入前の廃液に予め混入する請求項1記載の高レベル放射性廃液のガラス溶融方法。
- ガラス溶融炉に投入するガラス原料組成中のB 2 O 3 を10〜15%少なくし、その少なくした10〜15%に相当するB 2 O 3 を投入前の廃液に混入する請求項1〜3のいずれかに記載の高レベル放射性廃液のガラス溶融方法。
- ガラス溶融炉に投入するガラス原料組成中のAl 2 O 3 の含有量を0とし、そのガラス原料中のAl 2 O 3 組成に相当するAl 2 O 3 の全量を廃液に予め混入する請求項1〜4のいずれかに記載の高レベル放射性廃液のガラス溶融方法。
- ガラス原料が、粒径2〜3mmのガラスビーズからなる請求項1〜5のいずれかに記載の高レベル放射性廃液のガラス溶融方法。
- ガラス原料が、長さが10〜20μmの繊維状ガラスを円筒形に成形したガラスカートリッジからなる請求項1〜5のいずれかに記載の高レベル放射性廃液のガラス溶融方法。
Priority Applications (8)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP2007244041A JP4406451B2 (ja) | 2007-09-20 | 2007-09-20 | 高レベル放射性廃液のガラス溶融方法 |
CA2699304A CA2699304C (en) | 2007-09-20 | 2008-09-15 | Mitigation of secondary phase formation during waste vitrification |
PCT/US2008/076381 WO2009039059A1 (en) | 2007-09-20 | 2008-09-15 | Mitigation of secondary phase formation during waste vitrification |
US12/677,490 US8530718B2 (en) | 2007-09-20 | 2008-09-15 | Mitigation of secondary phase formation during waste vitrification |
CN200880108138.6A CN101801861B (zh) | 2007-09-20 | 2008-09-15 | 减轻废料玻璃化期间的二次相形成 |
KR1020107008631A KR101512285B1 (ko) | 2007-09-20 | 2008-09-15 | 폐기물 유리화 동안의 이차 상 형성의 완화 |
EP08832539.4A EP2195277B1 (en) | 2007-09-20 | 2008-09-15 | Mitigation of secondary phase formation during waste vitrification |
US14/021,739 US8951182B2 (en) | 2007-09-20 | 2013-09-09 | Mitigation of secondary phase formation during waste vitrification |
Applications Claiming Priority (1)
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JP2007244041A JP4406451B2 (ja) | 2007-09-20 | 2007-09-20 | 高レベル放射性廃液のガラス溶融方法 |
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JP2009074919A JP2009074919A (ja) | 2009-04-09 |
JP4406451B2 true JP4406451B2 (ja) | 2010-01-27 |
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JP2007244041A Active JP4406451B2 (ja) | 2007-09-20 | 2007-09-20 | 高レベル放射性廃液のガラス溶融方法 |
Country Status (7)
Country | Link |
---|---|
US (2) | US8530718B2 (ja) |
EP (1) | EP2195277B1 (ja) |
JP (1) | JP4406451B2 (ja) |
KR (1) | KR101512285B1 (ja) |
CN (1) | CN101801861B (ja) |
CA (1) | CA2699304C (ja) |
WO (1) | WO2009039059A1 (ja) |
Families Citing this family (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP4406451B2 (ja) * | 2007-09-20 | 2010-01-27 | 株式会社Ihi | 高レベル放射性廃液のガラス溶融方法 |
US9245655B2 (en) * | 2012-05-14 | 2016-01-26 | Energysolutions, Llc | Method for vitrification of waste |
CN103366847A (zh) * | 2013-07-23 | 2013-10-23 | 南京大学 | 废玻璃在固化放射性核素中的应用及固化Sr2+废物的方法 |
KR101507148B1 (ko) | 2013-11-19 | 2015-04-01 | 서울대학교산학협력단 | 방사성 희토류 폐기물 유리화 방법 |
KR101524588B1 (ko) | 2013-12-04 | 2015-06-01 | 한국수력원자력 주식회사 | 저방사성 폐수지를 유리화하기 위한 유리조성물 및 이를 이용한 저방사성 폐수지의 유리화 방법 |
JP2015190892A (ja) * | 2014-03-28 | 2015-11-02 | 株式会社Ihi | 高レベル放射性廃液ガラス固化設備のルテニウム処理方法及び装置 |
US11508490B2 (en) | 2020-03-11 | 2022-11-22 | Henry Crichlow | Managing volatiles in nuclear waste vitrification |
Family Cites Families (12)
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JPS61132898A (ja) * | 1984-11-30 | 1986-06-20 | 株式会社東芝 | 放射性廃棄物の固化処理方法 |
FR2596910A1 (fr) | 1986-04-08 | 1987-10-09 | Tech Nles Ste Gle | Procede pour la preparation d'un verre borosilicate contenant des dechets nucleaires |
JP2536778B2 (ja) * | 1988-08-11 | 1996-09-18 | 動力炉・核燃料開発事業団 | 放射性廃液処理用カ―トリッジの製造法 |
US5120342A (en) | 1991-03-07 | 1992-06-09 | Glasstech, Inc. | High shear mixer and glass melting apparatus |
US5340372A (en) * | 1991-08-07 | 1994-08-23 | Pedro Buarque de Macedo | Process for vitrifying asbestos containing waste, infectious waste, toxic materials and radioactive waste |
US5891011A (en) * | 1992-04-01 | 1999-04-06 | The United States Of America As Represented By The United States Department Of Energy | Vitrification of waste |
JP2989508B2 (ja) * | 1995-02-28 | 1999-12-13 | 核燃料サイクル開発機構 | 高レベル放射性廃液のガラス固化方法 |
US5662579A (en) * | 1995-03-21 | 1997-09-02 | The United States Of America As Represented By The United States Department Of Energy | Vitrification of organics-containing wastes |
US5678236A (en) * | 1996-01-23 | 1997-10-14 | Pedro Buarque De Macedo | Method and apparatus for eliminating volatiles or airborne entrainments when vitrifying radioactive and/or hazardous waste |
JP4283402B2 (ja) | 1999-12-22 | 2009-06-24 | 日本無機株式会社 | 放射性廃液処理用カートリッジの製造法 |
GB2367419A (en) * | 2000-08-19 | 2002-04-03 | British Nuclear Fuels Plc | Encapsulation of waste |
JP4406451B2 (ja) * | 2007-09-20 | 2010-01-27 | 株式会社Ihi | 高レベル放射性廃液のガラス溶融方法 |
-
2007
- 2007-09-20 JP JP2007244041A patent/JP4406451B2/ja active Active
-
2008
- 2008-09-15 CN CN200880108138.6A patent/CN101801861B/zh not_active Expired - Fee Related
- 2008-09-15 EP EP08832539.4A patent/EP2195277B1/en active Active
- 2008-09-15 CA CA2699304A patent/CA2699304C/en active Active
- 2008-09-15 KR KR1020107008631A patent/KR101512285B1/ko active IP Right Grant
- 2008-09-15 WO PCT/US2008/076381 patent/WO2009039059A1/en active Application Filing
- 2008-09-15 US US12/677,490 patent/US8530718B2/en active Active
-
2013
- 2013-09-09 US US14/021,739 patent/US8951182B2/en active Active
Also Published As
Publication number | Publication date |
---|---|
US8951182B2 (en) | 2015-02-10 |
CA2699304C (en) | 2015-05-12 |
US8530718B2 (en) | 2013-09-10 |
EP2195277A4 (en) | 2013-11-27 |
JP2009074919A (ja) | 2009-04-09 |
US20100285945A1 (en) | 2010-11-11 |
EP2195277B1 (en) | 2019-05-08 |
KR101512285B1 (ko) | 2015-04-15 |
EP2195277A1 (en) | 2010-06-16 |
CN101801861A (zh) | 2010-08-11 |
WO2009039059A1 (en) | 2009-03-26 |
KR20100092427A (ko) | 2010-08-20 |
US20140066684A1 (en) | 2014-03-06 |
CN101801861B (zh) | 2014-02-19 |
CA2699304A1 (en) | 2009-03-26 |
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