JP4233121B2 - 希薄水性溶液からの発酵塩類の回収 - Google Patents

希薄水性溶液からの発酵塩類の回収 Download PDF

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Publication number
JP4233121B2
JP4233121B2 JP50557499A JP50557499A JP4233121B2 JP 4233121 B2 JP4233121 B2 JP 4233121B2 JP 50557499 A JP50557499 A JP 50557499A JP 50557499 A JP50557499 A JP 50557499A JP 4233121 B2 JP4233121 B2 JP 4233121B2
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water
extractant
amine
mixture
carboxylate
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Expired - Fee Related
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Japanese (ja)
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JP2002510972A5 (https=
JP2002510972A (ja
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ホルトザップル,マーク・ティー
デイヴィソン,リチャード・アール
ルエティッヒ,トルステン
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Texas A&M University System
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D17/00Separation of liquids, not provided for elsewhere, e.g. by thermal diffusion
    • B01D17/02Separation of non-miscible liquids
    • B01D17/04Breaking emulsions
    • B01D17/042Breaking emulsions by changing the temperature
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D11/00Solvent extraction
    • B01D11/04Solvent extraction of solutions which are liquid
    • B01D11/0446Juxtaposition of mixers-settlers
    • B01D11/0457Juxtaposition of mixers-settlers comprising rotating mechanisms, e.g. mixers, mixing pumps
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D17/00Separation of liquids, not provided for elsewhere, e.g. by thermal diffusion
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D17/00Separation of liquids, not provided for elsewhere, e.g. by thermal diffusion
    • B01D17/02Separation of non-miscible liquids
    • B01D17/0208Separation of non-miscible liquids by sedimentation
    • B01D17/0211Separation of non-miscible liquids by sedimentation with baffles
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D17/00Separation of liquids, not provided for elsewhere, e.g. by thermal diffusion
    • B01D17/02Separation of non-miscible liquids
    • B01D17/0208Separation of non-miscible liquids by sedimentation
    • B01D17/0214Separation of non-miscible liquids by sedimentation with removal of one of the phases
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D17/00Separation of liquids, not provided for elsewhere, e.g. by thermal diffusion
    • B01D17/02Separation of non-miscible liquids
    • B01D17/04Breaking emulsions
    • B01D17/041Breaking emulsions with moving devices
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D17/00Separation of liquids, not provided for elsewhere, e.g. by thermal diffusion
    • B01D17/02Separation of non-miscible liquids
    • B01D17/04Breaking emulsions
    • B01D17/044Breaking emulsions by changing the pressure
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D17/00Separation of liquids, not provided for elsewhere, e.g. by thermal diffusion
    • B01D17/02Separation of non-miscible liquids
    • B01D17/04Breaking emulsions
    • B01D17/045Breaking emulsions with coalescers
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D17/00Separation of liquids, not provided for elsewhere, e.g. by thermal diffusion
    • B01D17/02Separation of non-miscible liquids
    • B01D17/04Breaking emulsions
    • B01D17/047Breaking emulsions with separation aids
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D17/00Separation of liquids, not provided for elsewhere, e.g. by thermal diffusion
    • B01D17/02Separation of non-miscible liquids
    • B01D17/04Breaking emulsions
    • B01D17/048Breaking emulsions by changing the state of aggregation
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42Separation; Purification; Stabilisation; Use of additives
    • C07C51/48Separation; Purification; Stabilisation; Use of additives by liquid-liquid treatment

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  • Chemical & Material Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Extraction Or Liquid Replacement (AREA)
  • Preparation Of Compounds By Using Micro-Organisms (AREA)
  • Apparatus Associated With Microorganisms And Enzymes (AREA)
JP50557499A 1997-06-30 1998-06-12 希薄水性溶液からの発酵塩類の回収 Expired - Fee Related JP4233121B2 (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US08/885,841 US5986133A (en) 1997-06-30 1997-06-30 Recovery of fermentation salts from dilute aqueous solutions
US08/885,841 1997-06-30
PCT/US1998/012202 WO1999000352A1 (en) 1997-06-30 1998-06-12 Recovery of fermentation salts from dilute aqueous solutions

Related Child Applications (1)

Application Number Title Priority Date Filing Date
JP2008240071A Division JP2009000686A (ja) 1997-06-30 2008-09-18 希薄水性溶液からの発酵塩類の回収

Publications (3)

Publication Number Publication Date
JP2002510972A JP2002510972A (ja) 2002-04-09
JP2002510972A5 JP2002510972A5 (https=) 2005-12-22
JP4233121B2 true JP4233121B2 (ja) 2009-03-04

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Family Applications (2)

Application Number Title Priority Date Filing Date
JP50557499A Expired - Fee Related JP4233121B2 (ja) 1997-06-30 1998-06-12 希薄水性溶液からの発酵塩類の回収
JP2008240071A Pending JP2009000686A (ja) 1997-06-30 2008-09-18 希薄水性溶液からの発酵塩類の回収

Family Applications After (1)

Application Number Title Priority Date Filing Date
JP2008240071A Pending JP2009000686A (ja) 1997-06-30 2008-09-18 希薄水性溶液からの発酵塩類の回収

Country Status (6)

Country Link
US (2) US5986133A (https=)
EP (1) EP0994842A1 (https=)
JP (2) JP4233121B2 (https=)
AU (1) AU756707B2 (https=)
CA (1) CA2294615C (https=)
WO (1) WO1999000352A1 (https=)

Families Citing this family (53)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
RU2133385C1 (ru) * 1998-01-27 1999-07-20 Попов Сергей Анатольевич Насосно-эжекторная установка
ES2312337T3 (es) 1999-03-11 2009-03-01 Zeachem Inc. Proceso para producir etanol.
US7074603B2 (en) 1999-03-11 2006-07-11 Zeachem, Inc. Process for producing ethanol from corn dry milling
US7684786B2 (en) * 2003-08-26 2010-03-23 Nokia Corporation Method and system for establishing a connection between network elements
EP1470099A4 (en) * 2002-01-03 2006-04-12 Staley Mfg Co A E PROCESS FOR PURIFYING AN ORGANIC ACID
US6641734B2 (en) * 2002-01-03 2003-11-04 A. E. Staley Manufacturing Co. Process for purifying an organic acid
DE10251191A1 (de) * 2002-11-04 2004-05-13 Bayer Ag Verfahren zur Trennung von m- und p-Dichlorbenzol enthaltenden Gemischen
AU2005207970B2 (en) * 2004-01-29 2011-04-28 Zeachem Inc. Recovery of organic acids
BRPI0509886B1 (pt) 2004-04-13 2018-01-30 Iogen Energy Corporation Método para o processamento de uma matéria-prima lignocelulósica e obtenção de um sal inorgânico
CN101061229B (zh) * 2004-06-16 2012-06-13 得克萨斯A&M大学系统 将生物质转化为羧酸和醇类的方法和系统
US7682811B2 (en) * 2006-01-27 2010-03-23 University Of Massachusetts Systems and methods for producing biofuels and related materials
US9499635B2 (en) 2006-10-13 2016-11-22 Sweetwater Energy, Inc. Integrated wood processing and sugar production
US8323923B1 (en) 2006-10-13 2012-12-04 Sweetwater Energy, Inc. Method and system for producing ethanol
US7670813B2 (en) * 2006-10-25 2010-03-02 Iogen Energy Corporation Inorganic salt recovery during processing of lignocellulosic feedstocks
EP2121946A4 (en) 2007-02-09 2012-08-29 Zeachem Inc ENERGY-EFFICIENT METHOD FOR MANUFACTURING PRODUCTS
US8153850B2 (en) * 2007-05-11 2012-04-10 The Texas A&M University System Integrated biofuel production system
DE102007059389A1 (de) * 2007-07-21 2009-06-10 Universität Dortmund Verfahren zur Aufarbeitung von koaleszenzgehemmten Emulsionen aus Ganzzell-Biotransformationen mit komprimierten oder überkritischen Gasen
WO2009085324A1 (en) * 2007-12-31 2009-07-09 University Of North Dakota Method for production of short chain carboxylic acids and esters from biomass and product of same
US8076504B2 (en) * 2007-12-31 2011-12-13 The University Of North Dakota Method for production of short chain carboxylic acids and esters from biomass and product of same
BRPI0905949A2 (pt) * 2008-02-07 2015-06-30 Zeachem Inc Produção indireta de butanol e hexanol
NZ587605A (en) * 2008-02-27 2012-10-26 Qteros Inc Methods for the conversion of plant materials into fuels and chemicals by sequential action of two microorganisms
AU2009244135A1 (en) * 2008-05-07 2009-11-12 Zeachem Inc. Recovery of organic acids
MX2011004912A (es) * 2008-11-26 2011-05-30 Univ North Dakota Metodo para producir compuestos organicos ciclicos a partir de aceites de cultivo.
MX2011005690A (es) 2008-12-02 2011-10-28 Texas A & M Univ Sys Vias alternas a los alcoholes e hidrocarbonos de biomasa.
CA2781862C (en) * 2008-12-09 2018-02-13 Sweetwater Energy, Inc. Ensiling biomass for biofuels production and multiple phase apparatus for hydrolyzation of ensiled biomass
JP5536341B2 (ja) 2009-01-06 2014-07-02 住友重機械工業株式会社 減速装置
US20120329116A1 (en) * 2009-04-20 2012-12-27 Greenfield Ethanol Inc. Pretreatment of lignocellulosic biomass through removal of inhibitory compounds
ES2499490T3 (es) * 2009-04-20 2014-09-29 Greenfield Ethanol Inc. Pretratamiento de biomasa lignocelulósica para eliminación de compuestos inhibidores
BRPI1013829A2 (pt) * 2009-04-20 2019-09-24 Qteros Inc composições e métodos para fermentação de biomassa
JP5662424B2 (ja) * 2009-05-14 2015-01-28 ユニヴァーシティー オブ ノースダコタ バイオマス油から高炭素含量生成物を生成するための方法
LT2438036T (lt) * 2009-06-04 2017-06-26 Genomatica, Inc. Fermentacijos sultinio komponentų išskyrimo būdas
US9662594B2 (en) * 2009-06-22 2017-05-30 Ng Innovations, Inc. Systems and methods for treating fractionated water
US8409442B2 (en) * 2009-08-20 2013-04-02 Ng Innovations, Inc. Water separation method and apparatus
US8470139B2 (en) * 2009-12-11 2013-06-25 Nginnovations, Inc. Systems and method for low temperature recovery of fractionated water
WO2012021956A1 (pt) * 2010-08-19 2012-02-23 Companhia Refinadora Da Amazônia Processo de obtenção de ácido lático com elevado grau de pureza a partir de licor fermentativo
US8859808B2 (en) 2010-08-19 2014-10-14 Paulo Yoshida Method for obtaining lactic acid with a high degree of purity from fermentative liquor
CA2831485A1 (en) 2011-04-22 2012-10-26 University Of North Dakota Production of aromatics from noncatalytically cracked fatty acid based oils
GB2496599A (en) * 2011-08-26 2013-05-22 Tha Ni Ind E Gmbh Two tank fermentation system and method of operation
KR20150035479A (ko) * 2011-12-21 2015-04-06 인비스타 테크놀러지스 에스.에이 알.엘. 안정한 에멀젼을 감소시키기 위한 추출 용매 제어
EP2794047B1 (en) 2011-12-21 2021-04-14 INVISTA Textiles (U.K.) Limited Extraction solvent control for reducing stable emulsions
US9133223B2 (en) 2011-12-21 2015-09-15 Invista North America S.A.R.L. Extraction solvent control for reducing stable emulsions
JP2015512862A (ja) * 2011-12-21 2015-04-30 インヴィスタ テクノロジーズ エスアエルエル 安定なエマルジョンを減じるための抽出溶媒制御
US8765430B2 (en) 2012-02-10 2014-07-01 Sweetwater Energy, Inc. Enhancing fermentation of starch- and sugar-based feedstocks
PL2836602T3 (pl) 2012-04-13 2019-07-31 Sweetwater Energy, Inc. Sposoby i układy do sacharyfikacji biomasy
US8563277B1 (en) 2012-04-13 2013-10-22 Sweetwater Energy, Inc. Methods and systems for saccharification of biomass
WO2014152665A1 (en) 2013-03-15 2014-09-25 Genomatica, Inc. Process and systems for obtaining 1,4-butanediol from fermentation broths
CA2906917A1 (en) 2013-03-15 2014-09-18 Sweetwater Energy, Inc. Carbon purification of concentrated sugar streams derived from pretreated biomass
BR112016002948B1 (pt) 2013-08-15 2020-12-01 Hatch Ltd método para controlar o tempo de retenção de uma mistura de reação aquosa em um reator e reator com controle de tempo de retenção
WO2016094594A1 (en) 2014-12-09 2016-06-16 Sweetwater Energy, Inc. Rapid pretreatment
US11821047B2 (en) 2017-02-16 2023-11-21 Apalta Patent OÜ High pressure zone formation for pretreatment
CN109384666B (zh) 2018-11-26 2021-06-22 广州楹鼎生物科技有限公司 一种联动回收有机酸水溶液中有机酸的方法
BR112022012348A2 (pt) 2019-12-22 2022-09-13 Sweetwater Energy Inc Métodos de fazer lignina especializada e produtos de lignina da biomassa
CN116062829B (zh) * 2022-12-12 2024-10-08 内蒙古鄂尔多斯电力冶金集团股份有限公司 一种非变温的萃取结晶脱盐方法

Family Cites Families (40)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US1442306A (en) * 1923-01-16 Oil-elotation apparatus
GB277975A (en) 1926-09-23 1929-01-21 Fernand Germain Process for the production of butyrone
FR642698A (fr) 1927-03-23 1928-09-01 H Gouthiere Et Cie Soc Procédé de fabrication des cétones
CH132022A (fr) 1928-03-07 1929-03-31 Ketol Sa L Procédé pour la décomposition continue de substances par la chaleur.
GB445108A (en) 1934-10-02 1936-04-02 British Celanese Improvements in the recovery of acidic and basic reagents
FR1064614A (fr) 1949-06-21 1954-05-17 Procédé et dispositif pour la production de gaz méthane, dane les installations septiques rurales en particulier
US2845936A (en) * 1955-05-09 1958-08-05 Hercules Powder Co Ltd Countercurrent contacting apparatus
US3079705A (en) 1959-01-20 1963-03-05 Bauer Bros Co Peanut cooler
US3088909A (en) * 1961-02-09 1963-05-07 Richard R Davison Mixed solvents for saline water extraction
US3424675A (en) * 1965-08-25 1969-01-28 Us Interior Vapor compression solvent extractor desalination
GB1140224A (en) 1966-02-16 1969-01-15 Inst Gornogo Dela Sibirskogo O Vibration magnetometer
NL6801614A (https=) * 1968-02-05 1969-08-07
DE7138603U (de) * 1971-10-12 1972-06-15 Passavant Werke Vorrichtung zur mechanisch-chemischen Wasseraufbereitung und Abwasserbehandlung
BE793060A (fr) * 1971-12-24 1973-04-16 Metallgesellschaft Ag Dispositif pour separer des liquides
FR2227830A1 (en) 1973-05-04 1974-11-29 Guttridge Ltd David Portable pellet processing appts - with air drying columns and screens for farm animal feed
US4132651A (en) * 1976-02-19 1979-01-02 Dejong Leendert W C Separating device to separate two liquids of different specific gravity
DE2710241A1 (de) * 1976-03-11 1977-09-22 Krebs & Co Ag Verfahren zum vermengen und trennen von zwei nicht mischbaren fluessigkeiten
US4131651A (en) * 1977-10-25 1978-12-26 Barnes-Hind Pharmaceuticals, Inc. Treatment of dry eye
FI57059C (fi) * 1978-06-28 1980-06-10 Outokumpu Oy Extraktionsenhet foer vaetske-vaetske-extraktion
JPS6027441Y2 (ja) * 1980-03-17 1985-08-19 住友金属鉱山株式会社 液々抽出装置
AU7279981A (en) 1980-08-21 1982-02-25 Koppers Company, Inc. Method + apparatus for cooling pellets
US4444881A (en) 1981-10-26 1984-04-24 Cpc International Inc. Recovery of organic acids from a fermentation broth
US4469582A (en) * 1982-03-22 1984-09-04 Combustion Engineering, Inc. Electrically enhanced inclined plate separator
JPS597131A (ja) * 1982-07-06 1984-01-14 Daicel Chem Ind Ltd 酢酸の回収法
JPS5912706A (ja) * 1982-07-13 1984-01-23 Daicel Chem Ind Ltd ミキサ−セトラ−の運転方法
DE3312579A1 (de) 1983-04-08 1984-10-11 Bayer Ag, 5090 Leverkusen Verfahren zur durchfuehrung von mikrobiologischen umsetzungen bei enger verweilzeitverteilung
SE445710B (sv) * 1984-11-01 1986-07-14 Hyosong M Lee Anordning for kontinuerlig separering av en vetskeblandning, innehallande en lettare och en tyngre fas
US4978616A (en) 1985-02-28 1990-12-18 Verax Corporation Fluidized cell cultivation process
US5050997A (en) * 1987-12-23 1991-09-24 Sklokin Leonid I Mixer-settler for liquid-liquid extraction
US5046856A (en) * 1989-09-12 1991-09-10 Dowell Schlumberger Incorporated Apparatus and method for mixing fluids
DE69001804T2 (de) 1990-03-01 1993-09-09 Cominco Ltd Methode und vorrichtung zur kuehlung von festen teilchen.
US5132456A (en) 1991-05-07 1992-07-21 The Regents Of The University Of California Sorption of carboxylic acid from carboxylic salt solutions at PHS close to or above the pKa of the acid, with regeneration with an aqueous solution of ammonia or low-molecular-weight alkylamine
US5326474A (en) * 1992-11-13 1994-07-05 The United States Of America As Represented By The Secretary Of The Navy Low flow fluid separator
US5264623A (en) * 1993-01-04 1993-11-23 Energy Mines & Resources Canada Method of producing calcium salts from biomass
TW360636B (en) * 1993-07-12 1999-06-11 Glitsch Method and apparatus for recovering acetic acid from aqueous streams
US5554301A (en) * 1995-05-08 1996-09-10 Universal Environmental Technologies, Inc. Water clarification system
DE19624268C2 (de) 1995-09-30 2001-09-27 Herhof Umwelttechnik Gmbh Verfahren und Vorrichtung zur Verwertung organischer Abfälle
US5874263A (en) 1996-07-31 1999-02-23 The Texas A&M University System Method and apparatus for producing organic acids
US5795478A (en) * 1997-01-15 1998-08-18 Hirs; Gene Oil extraction system
US6043392A (en) * 1997-06-30 2000-03-28 Texas A&M University System Method for conversion of biomass to chemicals and fuels

Also Published As

Publication number Publication date
EP0994842A1 (en) 2000-04-26
JP2009000686A (ja) 2009-01-08
AU756707B2 (en) 2003-01-23
WO1999000352A1 (en) 1999-01-07
CA2294615C (en) 2009-07-14
AU7961898A (en) 1999-01-19
US6478965B1 (en) 2002-11-12
JP2002510972A (ja) 2002-04-09
CA2294615A1 (en) 1999-01-07
US5986133A (en) 1999-11-16

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