JP4121602B2 - 二種金属シアン化物触媒の製造方法 - Google Patents

二種金属シアン化物触媒の製造方法 Download PDF

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Publication number
JP4121602B2
JP4121602B2 JP04805698A JP4805698A JP4121602B2 JP 4121602 B2 JP4121602 B2 JP 4121602B2 JP 04805698 A JP04805698 A JP 04805698A JP 4805698 A JP4805698 A JP 4805698A JP 4121602 B2 JP4121602 B2 JP 4121602B2
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iii
ligand
catalyst
water
suspension
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Expired - Fee Related
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JP04805698A
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Japanese (ja)
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JPH10277398A5 (https=
JPH10277398A (ja
Inventor
ゲオルク、ハインリヒ、グロシュ
ハーラルト、ラルビッヒ
ディーター、ユンゲ
ダニーラ、ゲーレン
ペーター、デ、フォクト
ゲルト、ヘプナー
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BASF SE
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BASF SE
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    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/40—High-molecular-weight compounds
    • C08G18/48—Polyethers
    • C08G18/4866—Polyethers having a low unsaturation value
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J27/00—Catalysts comprising the elements or compounds of halogens, sulfur, selenium, tellurium, phosphorus or nitrogen; Catalysts comprising carbon compounds
    • B01J27/24—Nitrogen compounds
    • B01J27/26—Cyanides
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
    • C08G65/2642—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds characterised by the catalyst used
    • C08G65/2645—Metals or compounds thereof, e.g. salts
    • C08G65/2663—Metal cyanide catalysts, i.e. DMC's

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  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Toxicology (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • General Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Polyethers (AREA)
  • Catalysts (AREA)
JP04805698A 1997-03-06 1998-02-27 二種金属シアン化物触媒の製造方法 Expired - Fee Related JP4121602B2 (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
DE19709031.1 1997-03-06
DE19709031A DE19709031A1 (de) 1997-03-06 1997-03-06 Verfahren zur Herstellung von Doppelmetallcyanidkatalysatoren
US09/035,601 US6303533B1 (en) 1997-03-06 1998-03-05 Process for preparing two-metal cyanide catalysts

Publications (3)

Publication Number Publication Date
JPH10277398A JPH10277398A (ja) 1998-10-20
JPH10277398A5 JPH10277398A5 (https=) 2005-09-02
JP4121602B2 true JP4121602B2 (ja) 2008-07-23

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ID=26034540

Family Applications (1)

Application Number Title Priority Date Filing Date
JP04805698A Expired - Fee Related JP4121602B2 (ja) 1997-03-06 1998-02-27 二種金属シアン化物触媒の製造方法

Country Status (6)

Country Link
US (1) US6303533B1 (https=)
EP (1) EP0862947B2 (https=)
JP (1) JP4121602B2 (https=)
CA (1) CA2228651A1 (https=)
DE (2) DE19709031A1 (https=)
ES (1) ES2198610T5 (https=)

Families Citing this family (46)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE19742978A1 (de) 1997-09-29 1999-04-01 Basf Ag Multimetallcyanidkomplexe als Katalysatoren
US6051680A (en) * 1998-06-08 2000-04-18 Arco Chemical Technology, L.P. Silylated double metal cyanide complex catalysts
DE19917897A1 (de) † 1999-04-20 2000-10-26 Basf Ag Verfahren zur Herstellung von Polyurethanen
DE19919267A1 (de) 1999-04-28 2000-11-02 Bayer Ag Kristallisierende Polyetherpolyole, ein Verfahren zu deren Herstellung sowie deren Verwendung
DE50010642D1 (de) * 1999-06-02 2005-08-04 Basf Ag Verfahren zur herstellung von polyetherpolyole unter verwendung von kristallinen multimetallcyanid-katalysatoren
US6800583B2 (en) 1999-06-02 2004-10-05 Basf Aktiengesellschaft Suspension of multimetal cyanide compounds, their preparation and their use
US6613714B2 (en) * 1999-06-02 2003-09-02 Basf Aktiengesellschaft Multimetal cyanide compounds, their preparation and their use
US6376645B1 (en) * 1999-07-09 2002-04-23 The Dow Chemical Company Complexing agent-modified hexacyanometallate hexanitrometallate catalysts
JP2003504461A (ja) * 1999-07-09 2003-02-04 ザ ダウ ケミカル カンパニー スルホン化合物またはスルホキシド化合物で錯化された金属触媒
US6358877B1 (en) 1999-09-10 2002-03-19 The Dow Chemical Company Metal catalysts complexed with sulfone or sulfoxide compounds
DE19949091A1 (de) 1999-10-12 2001-04-26 Basf Ag Polyester-Polyetherblockcopolymere
US6429166B1 (en) * 2000-05-19 2002-08-06 Dow Global Technologies Inc. Method for preparing metal cyanide catalyst/polyol initiator slurries
US6436867B1 (en) * 2000-08-01 2002-08-20 Basf Corporation One-step synthesis of double metal cyanides
DE10137628A1 (de) * 2001-08-03 2003-02-27 Basf Ag Verfahren zur Herstellung von Polyurethan-Weichschaumstoffen
DE10141122A1 (de) * 2001-08-22 2003-03-13 Basf Ag Verfahren zur Erhöhung der katalytischen Aktivität von Multimetallcyanidverbindungen
US6696383B1 (en) * 2002-09-20 2004-02-24 Bayer Polymers Llc Double-metal cyanide catalysts which can be used to prepare polyols and the processes related thereto
US6806348B2 (en) * 2003-02-11 2004-10-19 Basf Corporation Process for removing and regenerating a double metal cyanide (DMC) catalyst from a polymer polyol
US7378559B2 (en) * 2003-03-07 2008-05-27 Dow Global Technologies Inc. Continuous process and system of producing polyether polyols
US6855658B1 (en) * 2003-08-26 2005-02-15 Bayer Antwerp, N.V. Hydroxide containing double metal cyanide (DMC) catalysts
DE102004013408A1 (de) 2004-03-18 2005-10-06 Basf Ag Polyetheralkohole und Verfahren zur Herstellung von Polyetheralkoholen zur Polyurethansynthese
EP2003156A1 (de) 2007-04-19 2008-12-17 Basf Se Urethangruppen und Isocyanatgruppen enthaltende Prepolymere
EP1983010A3 (de) 2007-04-19 2009-07-29 Basf Se Verfahren zur Herstellung von Polyurethanen
DE102008042715A1 (de) 2007-10-12 2009-04-16 Basf Se Polyetherpolyole
EP2238195B1 (de) 2008-01-29 2015-03-18 Basf Se Verfahren zur herstellung von polyetheralkoholen
CN101684184A (zh) 2008-09-27 2010-03-31 巴斯夫欧洲公司 可通过使用可再生的原料获得的聚氨酯鞋底
DE102009045651A1 (de) 2008-10-17 2010-04-29 Basf Se Textilien und Verfahren zu ihrer Herstellung
CN102498145B (zh) 2009-07-10 2013-10-23 巴斯夫欧洲公司 基于可再生资源生产多元醇的方法
SG181448A1 (en) 2010-01-15 2012-08-30 Basf Se "process for the dmc-catalyzed preparation of polyols"
DE102010039090A1 (de) 2010-08-09 2012-02-09 Basf Se Verfahren zur Herstellung von Polyetheralkoholen
WO2014139935A1 (en) 2013-03-11 2014-09-18 Basf Se The use of polyalkoxylates in lubricant compositions
US9938484B2 (en) 2013-05-17 2018-04-10 Basf Se Use of polytetrahydrofuranes in lubricating oil compositions
KR102220786B1 (ko) * 2013-07-18 2021-03-02 에스케이이노베이션 주식회사 이중금속 시아나이드(ｄｍｃ) 촉매 및 이를 통해 제조된 에폭사이드/이산화탄소 공중합체
US20150113867A1 (en) 2013-10-24 2015-04-30 Basf Se Use of an alkoxylated polytetrahydrofuran to reduce fuel consumption
WO2015113850A1 (en) 2014-01-28 2015-08-06 Basf Se The use of alkoxylated polyethylene glycols in lubricating oil compositions
EP3146028B1 (en) 2014-05-22 2018-07-11 Basf Se Lubricant compositions containing beta-glucans
EP3029087A1 (de) 2014-12-05 2016-06-08 Evonik Degussa GmbH Verfahren zur Herstellung von niedrigviskosen Polyethersiloxanen
US9562135B1 (en) 2015-12-21 2017-02-07 Covestro Llc Polyether carbonates by DMC catalysis
EP3315591A1 (en) 2016-10-28 2018-05-02 Basf Se Energy efficient lubricant compositions
CA3075364A1 (en) 2017-10-27 2019-05-02 Huntsman International Llc Catalysts for making oxazolidinone materials
US10479862B2 (en) 2017-12-07 2019-11-19 Covestro Llc Amine based polymer polyol stabilizers
US10526484B2 (en) 2017-12-20 2020-01-07 Covestro Llc Dithiocarbonate containing polyols as polymer polyol stabilizers
JP7573529B2 (ja) * 2018-12-21 2024-10-25 ダウ グローバル テクノロジーズ エルエルシー ポリエーテル重合プロセス
US10544158B1 (en) 2019-03-14 2020-01-28 Covestro Llc Process for producing polycyclic polyether polyols
US11566145B2 (en) 2019-03-14 2023-01-31 Covestro Llc Polyurethane coating compositions and their use as gel coats
KR102717144B1 (ko) * 2021-07-15 2024-10-11 아주대학교산학협력단 하이드로젠 헥사시아노코발테이트와 아연 카복실레이트의 조합으로 제조된 더블메탈시아나이드 촉매 및 이를 이용한 프로필렌 옥사이드 중합
CN116376001B (zh) * 2023-04-10 2026-03-24 浙江皇马科技股份有限公司 一种改性双金属氰化物合成宽分子量分布脂肪醇聚醚的方法

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DD148957A1 (de) * 1980-01-31 1981-06-17 Gerhard Behrendt Verfahren zur herstellung von hochmolekularen polyetheralkoholen
US4764567A (en) 1986-11-20 1988-08-16 Basf Corporation Process for the preparation of polyoxyalkylene block polyethers having enhanced properties
CA2138063C (en) * 1993-12-23 2007-02-20 Bi Le-Khac Polyurethane foam-supported double metal cyanide catalysts for polyol synthesis
US5482908A (en) * 1994-09-08 1996-01-09 Arco Chemical Technology, L.P. Highly active double metal cyanide catalysts
US5627122A (en) * 1995-07-24 1997-05-06 Arco Chemical Technology, L.P. Highly active double metal cyanide complex catalysts
US5639705A (en) * 1996-01-19 1997-06-17 Arco Chemical Technology, L.P. Double metal cyanide catalysts and methods for making them

Also Published As

Publication number Publication date
CA2228651A1 (en) 1998-09-06
EP0862947B2 (de) 2007-09-05
DE59808009D1 (de) 2003-05-28
US6303533B1 (en) 2001-10-16
ES2198610T5 (es) 2008-02-16
EP0862947A1 (de) 1998-09-09
DE19709031A1 (de) 1998-09-10
ES2198610T3 (es) 2004-02-01
EP0862947B1 (de) 2003-04-23
JPH10277398A (ja) 1998-10-20

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