JP3927121B2 - 染色されたプラスチック又はポリマー染料粒子の製造 - Google Patents
染色されたプラスチック又はポリマー染料粒子の製造 Download PDFInfo
- Publication number
- JP3927121B2 JP3927121B2 JP2002553409A JP2002553409A JP3927121B2 JP 3927121 B2 JP3927121 B2 JP 3927121B2 JP 2002553409 A JP2002553409 A JP 2002553409A JP 2002553409 A JP2002553409 A JP 2002553409A JP 3927121 B2 JP3927121 B2 JP 3927121B2
- Authority
- JP
- Japan
- Prior art keywords
- dye
- formula
- plastic
- polymer dye
- production
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B5/00—Dyes with an anthracene nucleus condensed with one or more heterocyclic rings with or without carbocyclic rings
- C09B5/24—Dyes with an anthracene nucleus condensed with one or more heterocyclic rings with or without carbocyclic rings the heterocyclic rings being only condensed with an anthraquinone nucleus in 1-2 or 2-3 position
- C09B5/34—Anthraquinone acridones or thioxanthrones
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B5/00—Dyes with an anthracene nucleus condensed with one or more heterocyclic rings with or without carbocyclic rings
- C09B5/24—Dyes with an anthracene nucleus condensed with one or more heterocyclic rings with or without carbocyclic rings the heterocyclic rings being only condensed with an anthraquinone nucleus in 1-2 or 2-3 position
- C09B5/34—Anthraquinone acridones or thioxanthrones
- C09B5/347—Anthraquinone acridones
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/16—Nitrogen-containing compounds
- C08K5/34—Heterocyclic compounds having nitrogen in the ring
- C08K5/3412—Heterocyclic compounds having nitrogen in the ring having one nitrogen atom in the ring
- C08K5/3432—Six-membered rings
- C08K5/3437—Six-membered rings condensed with carbocyclic rings
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Processes Of Treating Macromolecular Substances (AREA)
- Paints Or Removers (AREA)
- Other In-Based Heterocyclic Compounds (AREA)
Description
R1は、水素、ヒドロキシル又は基−NHCO−R6であり、R6は、C1〜C6アルキル又は非置換であるか、C1〜C4アルキルもしくはハロゲンで置換されているフェニルであり、
R2は、水素、ヒドロキシル又は基W−R7であり、Wは−NHCO−又は−S−であり、R7は、C1〜C6アルキル又は非置換であるか、C1〜C4アルキルもしくはハロゲンで置換されているフェニルであり、
R3は水素であり、
R4は水素又はヒドロキシルであり
R5は水素であり、あるいは、
R3とR4とが合わさって式
の少なくとも一つの染料の着色有効量と混合することを含むことを特徴とする方法を提供する。
の化合物をクロロスルホン酸中で閉環して式
反応容器に濃硫酸145.0重量部及びクロロスルホン酸70.0重量部を充填した。式
ポリエステルチップ(PET Arnite DO4-300、DSM)1200.00gを130℃で4時間予備乾燥させたのち、ローララック中、毎分60回転で式
ポリエステルチップ(PET Arnite DO4-300、DSM)1200.00gを130℃で4時間予備乾燥させたのち、ローララック中、毎分60回転で
式(2)の染料0.64g、
式(7)の染料0.30g及び
式(26)の染料1.46g
と均質になるまで15分間混合した。均質な混合物を、最高温度220℃の6個の加熱帯を含むCollin(D-85560 Ebersberg)製の二軸スクリュー25mm押出し機で押出しし、水で急冷し、MAPAG社(CH-3001 Bern)製のTurb Etuve TE25ペレタイザでペレット成形したのち、75℃で4時間乾燥させた。これが、良好な万能の堅ロウ性、特に非常に良好な耐光堅ロウ性及び高温耐光堅ロウ性を有する灰色のポリエステルチップを与えた。
ポリエステルチップ(PET Arnite DO4-300、DSM)1200.00gを130℃で4時間予備乾燥させたのち、ローララック中、毎分60回転で、式(2)の染料2.40gと均質になるまで15分間混合した。均質な混合物を、最高温度220℃の6個の加熱帯を含む二軸スクリュー25mm押出し機(Collin, D-85560 Ebersberg)で押出しし、水で急冷し、Turb Etuve TE25グラニュレータ(MAPAG社、CH-3001 Bern)で粗砕したのち、75℃で4時間乾燥させた。これが、良好な万能の堅ロウ性、特に非常に良好な耐光堅ロウ性及び高温耐光堅ロウ性を有する青いポリエステルチップを与えた。
Claims (3)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CH25092000 | 2000-12-22 | ||
PCT/EP2001/014691 WO2002051924A1 (en) | 2000-12-22 | 2001-12-13 | Preparation of dyed plastics or polymeric dye particles |
Publications (3)
Publication Number | Publication Date |
---|---|
JP2004522825A JP2004522825A (ja) | 2004-07-29 |
JP2004522825A5 JP2004522825A5 (ja) | 2005-12-22 |
JP3927121B2 true JP3927121B2 (ja) | 2007-06-06 |
Family
ID=4569743
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP2002553409A Expired - Fee Related JP3927121B2 (ja) | 2000-12-22 | 2001-12-13 | 染色されたプラスチック又はポリマー染料粒子の製造 |
Country Status (9)
Country | Link |
---|---|
US (1) | US6923836B2 (ja) |
EP (1) | EP1343840A1 (ja) |
JP (1) | JP3927121B2 (ja) |
KR (1) | KR20040010577A (ja) |
CN (1) | CN1481416A (ja) |
BR (1) | BR0116321A (ja) |
CA (1) | CA2430604A1 (ja) |
MX (1) | MXPA03005623A (ja) |
WO (1) | WO2002051924A1 (ja) |
Families Citing this family (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2003080735A1 (en) * | 2002-03-22 | 2003-10-02 | Ciba Specialty Chemicals Holding Inc. | Anthraquinone dyes |
MXPA04009115A (es) * | 2002-03-22 | 2004-12-07 | Ciba Sc Holding Ag | Tintes de antraquinona. |
ES2315655T3 (es) * | 2003-04-22 | 2009-04-01 | Huntsman Advanced Materials (Switzerland) Gmbh | Mezclas de pigmento/colorante. |
KR100692787B1 (ko) * | 2006-04-17 | 2007-03-12 | (주)엑셀코리아 | 기능성 화장품 용기 뚜껑 제조 방법 |
CN105801887B (zh) * | 2016-04-11 | 2019-01-08 | 浙江纳美新材料股份有限公司 | 一种制备聚合物连续色卡的方法 |
Family Cites Families (11)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US1002066A (en) * | 1911-02-18 | 1911-08-29 | Basf Ag | Vat dye. |
US1690913A (en) * | 1925-10-29 | 1928-11-06 | Grasselli Dyestuff Corp | Manufacture of vat dyestuffs of the anthraquinone-acridone series |
US2031406A (en) * | 1932-01-19 | 1936-02-18 | Gen Aniline Works Inc | Vat dyestuffs of the anthraquinone-2.1(n) benzacridone series |
BE627049A (ja) * | 1962-01-12 | |||
CH401311A (de) * | 1962-03-13 | 1965-10-31 | Ciba Geigy | Verfahren zur Herstellung von wasserunlöslichen, carbonsäureamidgruppenhaltigen Farbstoffen |
DE1278634B (de) * | 1964-02-25 | 1968-09-26 | Basf Ag | Verfahren zur Herstellung von Farbstoffen der Anthrachinonreihe |
GB1111895A (en) * | 1966-03-17 | 1968-05-01 | Ici Ltd | Process for the mass coloration of polyesters |
FR1493903A (fr) * | 1965-09-15 | 1967-09-01 | Sandoz Sa | Colorants anthraquinoniques, leur procédé de fabrication et leurs applications |
GB1127704A (en) * | 1966-03-08 | 1968-09-18 | Ici Ltd | Polycyclic dyestuffs containing a 3:4-phthaloylacridone residue |
GB1073367A (en) * | 1966-03-24 | 1967-06-28 | Ici Ltd | Polycyclic dyestuffs |
CH570436A5 (ja) * | 1972-07-07 | 1975-12-15 | Ciba Geigy Ag |
-
2001
- 2001-12-13 WO PCT/EP2001/014691 patent/WO2002051924A1/en active Application Filing
- 2001-12-13 KR KR10-2003-7008128A patent/KR20040010577A/ko not_active Application Discontinuation
- 2001-12-13 MX MXPA03005623A patent/MXPA03005623A/es unknown
- 2001-12-13 CN CNA018209726A patent/CN1481416A/zh active Pending
- 2001-12-13 JP JP2002553409A patent/JP3927121B2/ja not_active Expired - Fee Related
- 2001-12-13 US US10/451,172 patent/US6923836B2/en not_active Expired - Fee Related
- 2001-12-13 BR BR0116321-3A patent/BR0116321A/pt not_active IP Right Cessation
- 2001-12-13 EP EP01272009A patent/EP1343840A1/en not_active Withdrawn
- 2001-12-13 CA CA002430604A patent/CA2430604A1/en not_active Abandoned
Also Published As
Publication number | Publication date |
---|---|
EP1343840A1 (en) | 2003-09-17 |
US20040045102A1 (en) | 2004-03-11 |
CN1481416A (zh) | 2004-03-10 |
MXPA03005623A (es) | 2003-10-06 |
KR20040010577A (ko) | 2004-01-31 |
WO2002051924A1 (en) | 2002-07-04 |
US6923836B2 (en) | 2005-08-02 |
BR0116321A (pt) | 2003-10-14 |
JP2004522825A (ja) | 2004-07-29 |
CA2430604A1 (en) | 2002-07-04 |
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