JP2021527730A - 密封材組成物 - Google Patents
密封材組成物 Download PDFInfo
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- JP2021527730A JP2021527730A JP2020569022A JP2020569022A JP2021527730A JP 2021527730 A JP2021527730 A JP 2021527730A JP 2020569022 A JP2020569022 A JP 2020569022A JP 2020569022 A JP2020569022 A JP 2020569022A JP 2021527730 A JP2021527730 A JP 2021527730A
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- C08G65/04—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers only
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Abstract
Description
本出願は、2018年6月12日に出願された大韓民国特許出願第10−2018−0067307号に基づく優先権の利益を主張し、当該大韓民国特許出願の文献に開示されたすべての内容は本明細書の一部として組み込まれる。
本発明は、密封材組成物、それを含む有機電子装置及び前記有機電子装置の製造方法に関する。
常温でエポキシ化合物として脂環式エポキシ化合物(Daicel社のCelloxide 2021P)及び脂肪族エポキシ化合物(HAJIN CHEM TECH社、DE203)、オキセタン基含有化合物(TOAGOSEI社のOXT−221)、光開始剤(BASF社のIrgacure PAG 290、以下、I290という)及びフッ素系界面活性剤(DIC社のF552)をそれぞれ22.2:18.8:49.0:5.0:1.0(Celloxide2021P:DE203:OXT−221:I290:F552)の重量割合で混合容器に投入した。前記エポキシ化合物に100重量部に対して、水分吸着剤が15重量部になるようにCaO(Aldrich社、平均粒径約150nm)を投入した。
常温でエポキシ化合物として脂環式エポキシ化合物(Daicel社のCelloxide 2021P)、オキセタン基含有化合物(TOAGOSEI社のOXT−221)、スルホニウム塩を含む光開始剤(I290)及びフッ素系界面活性剤(DIC社のF552)をそれぞれ37.5:52.5:5.0:1.0(Celloxide2021P:OXT−221:I290:F552)の重量割合で混合容器に投入したこと以外は、実施例1と同じ方法で密封材組成物を製造した。
常温でエポキシ化合物として脂環式エポキシ化合物(Daicel社のCelloxide 2021P)及び脂肪族エポキシ化合物(HAJIN CHEM TECH社、DE203)、オキセタン基含有化合物(TOAGOSEI社のOXT−221)、光開始剤(I290)及びフッ素系界面活性剤(DIC社のF552)をそれぞれ37.5:7.0:45.5:5.0:1.0(Celloxide2021P:DE203:OXT−221:I290:F552)の重量割合で混合容器に投入したこと以外は、実施例1と同じ方法で密封材組成物を製造した。
光開始剤としてI290の代わりに、BASF社のヨードニウム(Iodonium)光開始剤であるIrgacure 250(active contents 75wt%、溶媒(プロピレンカーボネート)25wt%)を用いたこと以外は、実施例1と同じ方法で密封材組成物を製造した。
常温でエポキシ化合物として脂環式エポキシ化合物(Daicel社のCelloxide 2021P)及び脂肪族エポキシ化合物(HAJIN CHEM TECH社、DE203)、オキセタン基含有化合物(TOAGOSEI社のOXT−221)、光開始剤(BASF社のIrgacure PAG 290、以下、I290という)、フッ素系界面活性剤(DIC社のF552)及びジエチレングリコールモノブチルエーテルアセテート(Diethylene glycol monobutyl ether acetate)をそれぞれ17.2:18.8:44.0:5.0:1.0:10.0(Celloxide2021P:DE203:OXT−221:I290:F552:ジエチレングリコールモノブチルエーテルアセテート)の重量割合で混合容器に投入したこと以外は、実施例1と同じ方法で密封材組成物を製造した。
常温でエポキシ化合物として脂環式エポキシ化合物(Daicel社のCelloxide 2021P)及び脂肪族エポキシ化合物(HAJIN CHEM TECH社、DE203)、オキセタン基含有化合物(TOAGOSEI社のOXT−221)、光開始剤(BASF社のIrgacure PAG 290、以下、I290という)及びフッ素系界面活性剤(DIC社のF552)をそれぞれ5:26:48:5:1(Celloxide2021P:DE203:OXT−221:I290:F552)の重量割合で混合容器に投入したこと以外は、実施例1と同じ方法で密封材組成物を製造した。
常温でエポキシ化合物として脂環式エポキシ化合物(Daicel社のCelloxide 2021P)及び脂肪族エポキシ化合物(HAJIN CHEM TECH社、DE203)、オキセタン基含有化合物(TOAGOSEI社のOXT−221)、光開始剤(I290)及びフッ素系界面活性剤(DIC社のF552)をそれぞれ2.3:23.4:64.3:5.0:1.0(Celloxide2021P:DE203:OXT−221:I290:F552)の重量割合で混合容器に投入したこと以外は、実施例1と同じ方法で密封材組成物を製造した。
常温でエポキシ化合物として脂環式エポキシ化合物(Daicel社のCelloxide 2021P)及び脂肪族エポキシ化合物(HAJIN CHEM TECH社、DE203)、オキセタン基含有化合物(TOAGOSEI社のOXT−221)、光開始剤(BASF社のIrgacure PAG 290、以下、I290という)及びフッ素系界面活性剤(DIC社のF552)をそれぞれ10:10:59:5:1(Celloxide2021P:DE203:OXT−221:I290:F552)の重量割合で混合容器に投入したこと以外は、実施例1と同じ方法で密封材組成物を製造した。
常温でエポキシ化合物として脂環式エポキシ化合物(Daicel社のCelloxide 2021P)、オキセタン基含有化合物(TCI社の3−allyloxy oxetane)、トリ(エチレングリコール)ジビニルエーテル(TEGDVE)、光開始剤(BASF社のIrgacure PAG 290、以下、I290という)及びフッ素系界面活性剤(DIC社のF552)をそれぞれ20:50:30:5:1(Celloxide2021P:3−アリルオキシオキセタン(3−allyloxy oxetane):TEGDVE:I290:F552)の重量割合で混合容器に投入したこと以外は、実施例1と同じ方法で密封材組成物を製造した。
SiNx蒸着膜が形成されたガラス基材上に、実施例及び比較例で製造した密封材組成物をインクジェットコーティングして5μm厚さの有機層を形成した。
実施例及び比較例で製造した密封材組成物をUnijet UJ−200(Inkjet head−Dimatix 10Pl 256)を用いてインクジェッティングを試みた。5分おきに吐出テストを行い、吐出可能持続時間が3時間以上であると、O、1時間以上3時間未満であると、△、1時間未満であると、Xに分類した。
31:基板
32:有機電子素子
33:有機層
34:無機層
35:保護膜
36:封止構造
37:封止フィルム
38:カバー基板
Claims (21)
- エポキシ化合物、前記エポキシ化合物100重量部に対して45重量部〜145重量部の範囲内であり、オキセタン基を有する化合物及び水分吸着剤を含むことを特徴とする、密封材組成物。
- 前記エポキシ化合物は、少なくとも2官能以上であることを特徴とする、請求項1に記載の密封材組成物。
- 前記エポキシ化合物は、分子構造内に環形構造を有する化合物及び/又は直鎖又は分枝鎖の脂肪族化合物を含むことを特徴とする、請求項1または2に記載の密封材組成物。
- 前記分子構造内に環形構造を有する化合物は、分子構造内の環構成原子が3〜10の範囲内であることを特徴とする、請求項3に記載の密封材組成物。
- 前記直鎖又は分枝鎖の脂肪族化合物は、前記環形構造を有する化合物100重量部に対して、20重量部以上、205重量部未満の範囲内に含まれることを特徴とする、請求項3または4に記載の密封材組成物。
- 前記オキセタン基を有する化合物は、沸点が90〜300℃の範囲内にあることを特徴とする、請求項1から5のいずれか一項に記載の密封材組成物。
- 前記オキセタン基を有する化合物は、重量平均分子量が150〜1,000g/molの範囲内にあることを特徴とする、請求項1から6のいずれか一項に記載の密封材組成物。
- イオン性光開始剤をさらに含むことを特徴とする、請求項1から7のいずれか一項に記載の密封材組成物。
- 前記光開始剤は、スルホ二ウム塩を含む光開始剤であることを特徴とする、請求項8に記載の密封材組成物。
- 前記光開始剤は、前記エポキシ化合物100重量部に対して1〜15重量部で含まれることを特徴とする、請求項8または9に記載の密封材組成物。
- 界面活性剤をさらに含むことを特徴とする、請求項1から10のいずれか一項に記載の密封材組成物。
- 前記界面活性剤は、極性作用基を含むことを特徴とする、請求項11に記載の密封材組成物。
- 前記界面活性剤は、フッ素系化合物を含むことを特徴とする、請求項11または12に記載の密封材組成物。
- 前記界面活性剤は、前記エポキシ化合物100重量部に対して0.01重量部〜10重量部で含まれることを特徴とする、請求項11から13のいずれか一項に記載の密封材組成物。
- 無溶剤形態のインク組成物であることを特徴とする、請求項1から14のいずれか一項に記載の密封材組成物。
- 25℃の温度、90%のトルク及び100rpmのせん断速度で、ブルックフィールド社のDV−3で測定した粘度が50cPs以下であることを特徴とする、請求項1から15のいずれか一項に記載の密封材組成物。
- 前記水分吸着剤は、化学反応性吸着剤であることを特徴とする、請求項1から16のいずれか一項に記載の密封材組成物。
- 前記水分吸着剤は、前記エポキシ化合物100重量部に対して5〜150重量部で含まれることを特徴とする、請求項1から17のいずれか一項に記載の密封材組成物。
- 基板;前記基板上に形成された有機電子素子;及び前記有機電子素子の全面を密封し、請求項1から18のいずれか一項に記載の密封材組成物を含む有機層を含むことを特徴とする、有機電子装置。
- 上部に有機電子素子が形成された基板上に、請求項1から18のいずれか一項に記載の密封材組成物が前記有機電子素子の全面を密封するように有機層を形成するステップを含むことを特徴とする、有機電子装置の製造方法。
- 前記有機層を形成するステップは、インクジェット印刷、グラビアコーティング、スピンコーティング、スクリーンプリンティング又はリバースオフセットコーティングを含むことを特徴とする、請求項20に記載の有機電子装置の製造方法。
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EP3800228A4 (en) | 2021-04-21 |
US20210230445A1 (en) | 2021-07-29 |
KR20190140861A (ko) | 2019-12-20 |
CN112218931B (zh) | 2024-02-13 |
WO2019240484A1 (ko) | 2019-12-19 |
CN112218931A (zh) | 2021-01-12 |
KR102383537B1 (ko) | 2022-04-06 |
EP3800228A1 (en) | 2021-04-07 |
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