JP2020516724A - 耐熱性が改善された水性乾燥積層体結合剤 - Google Patents
耐熱性が改善された水性乾燥積層体結合剤 Download PDFInfo
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- JP2020516724A JP2020516724A JP2019555483A JP2019555483A JP2020516724A JP 2020516724 A JP2020516724 A JP 2020516724A JP 2019555483 A JP2019555483 A JP 2019555483A JP 2019555483 A JP2019555483 A JP 2019555483A JP 2020516724 A JP2020516724 A JP 2020516724A
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Abstract
Description
フィルム:実施例において使用される基材として、二軸延伸ポリプロピレンフィルム(BOPP、厚さ18μm)、真空蒸着ポリエチレンテレフタレートポリエステルフィルム(VMPET、厚さ12μm)フィルム、および広東ナンチェンカンパニー(Guangdong Nan Cheng Company)から市販されているポリエチレンフィルム(PE、厚さ60μm)が挙げられる。
水性の接着剤およびBOPP、VMPET、PEフィルムが、前処理なしで使用される。接着剤をBOPPフィルムにコーティングし、VMPETフィルムと組み合わせて、乾燥重量で2.0g/m2の量のBOPP/VMPET 2層積層体を得て、乾燥させる。次いで、2層積層体に、乾燥重量で2.0g/m2の量で水性接着剤をコーティングし、PEフィルムと組み合わせて、BOPP/VMPET/PE3層積層体を得る。BOPP/VMPET/PE3層積層体を50℃で2日間硬化させた後、試験を行った。
本開示の積層体を、Instron社から入手可能な5943 Series Single Column Table Top Systemを用いる250mm/分のクロスヘッド速度下でのT−剥離試験のために金属ステンシルを用いて、25mm幅×10cm長さのストリップに切断する。試験中、各ストリップのテールを指で僅かに引っ張り、テールが剥離方向に対して90度のままであることを確認する。各サンプルについて3つのストリップを試験し、その平均値を計算する。結果はN/15mm単位である。値が高いほど、結合強度は高くなる。
積層体を、140℃のシール温度および300Nの圧力下で1秒間(または220℃のシール温度および300Nの圧力下で0.5秒間)、Brugger Companyから入手可能なHSG−Cヒートシール機中でヒートシールし、その後冷却され、Instron社から入手可能な5943 Series Single Column Table Top Systemを用いる250mm/分のクロスヘッド速度下でのヒートシール強度試験のために、25mm幅×10cm長さのストリップに切断する。各サンプルについて3つのストリップを試験し、その平均値を計算する。結果はN/15mm単位である。値が高いほど、ヒートシール強度が向上する。
470.25gのアクリル共重合体エマルジョン(固形分44%のBA−スチレン共重合体)を、マグネチックスターラー付きの1リットルボトルに入れ、次に、4.75gのポリオール(ポリエーテルジオール)と25gのSUPER ESTER(登録商標)E−865NTロジン樹脂をボトルに注ぎ、20分間攪拌した。混合組成物が分配されたら、10gのCOREACTANT CR 3Aポリイソシアネートを混合エマルジョン中に滴下し、混合物をさらに20分間攪拌する。
表3に示すように、例示的な接着剤の例IE1およびIE2は、比較例の接着剤の例1のヒートシール強度に比し、140℃および220℃で有意に改善されたヒートシール強度を有する。
Claims (16)
- 二成分結合剤組成物であって、
(a)(i)少なくとも2つのヒドロキシル基を含み、水分散性ポリエーテルポリオール、ポリエステルポリオール、ポリエーテルポリエステルポリオールおよびそれらの混合物からなる群より選択される0.1%〜10%のポリオール、(ii)3%〜32%のロジン樹脂、および(iii)20%〜60%の少なくとも1つのスチレンモノマーの残基、0℃未満のTgを有する40〜80%の少なくとも1つのアクリルモノマーの残基、1〜4%の(メタ)アクリル酸の残基、および0.5%未満のヒドロキシル含有モノマーの残基を有する58%〜96%のポリマーを含む固体部分を有する水性混合物である第1の成分と、
(b)水分散性ポリイソシアネートを含む第2の成分と、を含み、
前記第2の成分は、前記第1の成分に対して、1:1〜8:1のNCO/NCO反応性基モル比で存在する、二成分結合剤組成物。 - 前記ポリマーが5,000〜2,000,000の重量平均分子量を有する、請求項1に記載の組成物。
- 前記ポリオールが、ポリプロピレングリコールである、請求項1に記載の組成物。
- 前記ポリオールが、100〜7,500の数平均分子量を有する、請求項1に記載の組成物。
- 前記ロジン樹脂が、原料ロジンを変性、水素化、不均化および重合することによりそれぞれ得られる変性ロジン、水素化ロジン、不均化ロジンおよび重合ロジン、ならびに原料ロジンをアルコールまたはエポキシ化合物でエステル化することにより得られるロジンエステルから選択される、請求項1に記載の組成物。
- 前記変性ロジン樹脂が、原料ロジンを不飽和酸で変性することにより得られる不飽和変性ロジン、および原料ロジンをフェノールで変性することにより得られるフェノール変性ロジンから選択される、請求項5に記載の組成物。
- 前記不飽和酸がアクリル酸、メタクリル酸、フマル酸、およびマレイン酸である、請求項6に記載の組成物。
- 前記フェノールが、フェノールおよびアルキルフェノールである、請求項6に記載の組成物。
- 前記アルコールがグリセリンである、請求項5に記載の組成物。
- 前記アルコールがペンタエリスリトールである、請求項5に記載の組成物。
- 前記ロジン樹脂が、1,000〜50,000の分子量を有する、請求項1に記載の組成物。
- 前記ロジン樹脂が、1〜50KOHmg/gの酸価を有する、請求項1に記載の組成物。
- 前記ロジン樹脂が25℃〜200℃の軟化点を有する、請求項1に記載の組成物。
- 前記ポリイソシアネートが、トルエンジイソシアネート、イソホロンジイソシアネート、ヘキサメチレンジイソシアネート、ジフェニルメタンジイソシアネート、ジシクロヘキシルメタンジイソシアネート、それらの異性体、およびそれらの混合物に基づくポリイソシアネートから選択される、請求項1に記載の組成物。
- 少なくとも2つの基材層が結合剤の層によって互いに結合される積層物品の作製方法であって、前記少なくとも2つの基材層を請求項1に記載の結合剤組成物で結合することを含む、方法。
- 請求項1に記載の結合剤組成物により少なくとも2つの基材層を結合する積層体。
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EP3609969B1 (en) | 2023-11-01 |
RU2768501C2 (ru) | 2022-03-24 |
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