JP2019522382A - Pv層シーケンスを作り出すための室温印刷方法およびこの方法を使用して得られるpv層シーケンス - Google Patents
Pv層シーケンスを作り出すための室温印刷方法およびこの方法を使用して得られるpv層シーケンス Download PDFInfo
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- JP2019522382A JP2019522382A JP2019523162A JP2019523162A JP2019522382A JP 2019522382 A JP2019522382 A JP 2019522382A JP 2019523162 A JP2019523162 A JP 2019523162A JP 2019523162 A JP2019523162 A JP 2019523162A JP 2019522382 A JP2019522382 A JP 2019522382A
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Abstract
Description
印刷方法によって、−室温で、−無機コア成分が水溶液および/または水分散液を使用して処理されて、電極を介して接触が形成され得る完全なPV層シーケンスを得る、方法において、この方法が以下のステップを含むこと、すなわち、ステップa)で、少なくとも2つの要素からなる、サイズ0.5〜100マイクロメートルの半導電粒子100が水性反応溶液200中に分散され、酸化または還元によって部分的に溶かされ、キャリア300の領域にわたって塗布され、ステップb)で、反応溶液200は、体積収縮で硬化反応溶液層201に変換され、ここで粒子100は、硬化反応溶液層201を越えて突出し、反応溶液層201中に固定された底部側と反応溶液層201を越えて突出する上側とを有し、ステップc)で、粒子の上側は、少なくとも部分的に上側接触部400を設けられることを特徴とする方法を提供する。
PV層シーケンスの生産のための本発明の方法は、すでに開発されたものを踏まえて、最初は、印刷方法によって水溶液および/または水分散液を使用して室温で無機PV活性コア成分を処理して、アクセプタ電極を介して接触接続可能な完全なPV層シーケンスを与えることを想定する。
有利な実施形態で、方法が案内され、この方法において、ステップa)で、技術等級純度の、最大サイズ30±15マイクロメートルの半導電SiC粒子100が、緩やかなガスの発生を伴って、水酸化ナトリウムでアルカリ化されたシリカ溶液からなる水性反応溶液200中に分散され、酸化によって部分的に溶かされ、予め塗布されたキャリア電極301を有し好ましくは追加の印刷された境界302を有するフィルムキャリアおよび/または紙キャリア300のセクションの領域にわたって塗布され、
− ステップb)で、反応溶液200は、体積収縮で硬化反応溶液層201に変換され、ここで粒子100は、硬化反応溶液層201を越えて突出し、反応溶液層201中に固定された底部側と反応溶液層201を越えて突出する上側とを有し、
− 上側領域セクションは、酸化的または還元的に調整され、それによって還元処理された粒子102の領域または酸化処理された粒子103の領域が定められ、次に、
− 鎖状、網状、網状管からなる群から選択される少なくとも1つの構造を含むナノスケール構造、好ましくはCNT鎖および/またはハロゲン鎖が、少なくとも1つの領域セクション中の粒子100と直接接触して形成され、
− 粒子100の相互に隣接する領域セクションは、異なる溶液で調整されて、還元処理された粒子102のセクションおよび酸化処理された粒子103のセクションとして交互シーケンスで粒子100の相互に隣接する領域セクションを形成し、
− ステップc)で、粒子の上側は、少なくとも部分的に上側接触部400を設けられ、粒子100の交互に調整された領域セクションは、直列に接続され、最終的な接触電極に接着される。
100 粒子
101 上側
102 還元処理されたセクション
103 酸化処理されたセクション
200 反応溶液
201 硬化反応溶液
300 キャリア
301 キャリア電極
302 境界(例えば凸版印刷)
400 上側接触部
100 粒子
101 上側
102 還元処理されたセクション
103 酸化処理されたセクション
200 反応溶液
201 硬化反応溶液
300 キャリア
301 キャリア電極
302 境界(例えば凸版印刷)
400 上側接触部
500 PV測定アセンブリ
601 裏側電極
602 断面図における裏側電極
603 TCO層
604 TCO外層およびAR外層を有するPV活性Si層
605 ガラスキャリアおよび上側
606 5マイクロメートルスケール
701 反応溶液で調整された粒子
702 硬化した、ガラス状非晶質反応溶液
703 20マイクロメートルスケール
801 2つの相互貫入相から構成されるマトリクスの相1
802 2つの相互貫入相から構成されるマトリクスの相2
803 マトリクス中に固定された粒子
804 5マイクロメートルスケール
Claims (10)
- PV層シーケンスを作り出すための方法であって、印刷方法によって
− 室温で、
− 無機コア成分が
− 水溶液および/または水分散液を使用して処理されて、
電極を介して接触が形成され得る完全なPV層シーケンスを得る、方法において、前記方法が以下のステップを含むこと、すなわち
− ステップa)で、少なくとも2つの要素からなる、サイズ0.5〜100マイクロメートルの半導電粒子(100)が水性反応溶液(200)中に分散され、酸化または還元によって部分的に溶かされ、キャリア(300)の領域にわたって塗布され、
− ステップb)で、前記反応溶液(200)は、体積収縮で硬化反応溶液層(201)に変換され、前記粒子(100)は、前記硬化反応溶液層(201)を越えて突出し、前記反応溶液層(201)中に固定された底部側と前記反応溶液層(201)を越えて突出する上側とを有し、
− ステップc)で、前記粒子の前記上側は、少なくとも部分的に上側接触部(400)を設けられる
ことを特徴とする方法。 - 請求項1に記載の方法において、前記粒子(100)は、少なくとも1つの追加のステップで、少なくとも1つの表面セクションにおいて酸化または還元調整され、それによって還元処理された粒子(102)の領域または酸化処理された粒子(103)の領域が定められることを特徴とする方法。
- 請求項1または2に記載の方法において、さらなる方法ステップで、鎖状、網状、網状管からなる群から選択される少なくとも1つの構造を含むナノスケール構造が、好ましくは前記上側の領域セクションである、少なくとも1つの領域セクションの粒子(100)と直接接触して形成されることを特徴とする方法。
- 請求項1乃至3の何れか一項に記載の方法において、前記粒子(100)の相互に隣接する領域セクションは、異なる溶液で調整されて、次に還元処理された粒子(102)のセクションおよび酸化処理された粒子(103)のセクションとして交互シーケンスで前記粒子(100)の前記相互に隣接する領域セクションを形成することを特徴とする方法。
- 請求項1乃至4の何れか一項に記載の方法において、少なくとも1つのさらなる方法ステップで、少なくとも1つのキャリア電極(301)および/または上側接触層(400)を含む電極は、2次元材料に準備的に塗布され、最終的に前記2次元材料を通して前記PV層シーケンスに接着されることを特徴とする方法。
- 請求項1乃至5の何れか一項に記載の方法において、前記PV層シーケンスのために使用される前記キャリアは、連続的な、平らな材料のシート、好ましくはフィルムのシートおよび/または紙のシート、より好ましくは麻紙のシートを含むことを特徴とする方法。
- 請求項1乃至6の何れか一項に記載の方法において、粉砕された、好ましくは機械的に粉砕された、50マイクロメートル以下の粒径を有し、好ましくは30±15マイクロメートルの粒径を有し、より好ましくは0.5〜10マイクロメートルの粒径を有する粒子(100)が使用されることを特徴とする方法。
- 請求項1乃至7の何れか一項に記載の方法において、ステップa)で、最大サイズ30±15マイクロメートルの半導電SiC粒子(100)が、緩やかなガスの発生を伴って、水酸化ナトリウムでアルカリ化されたシリカ溶液からなる水性反応溶液(200)中に分散され、酸化によって部分的に溶かされ、予め塗布されたキャリア電極(301)を有し好ましくは追加の印刷された境界(302)を有するフィルムキャリアおよび/または紙キャリア(300)のセクションの前記領域にわたって塗布され、
− ステップb)で、前記反応溶液(200)は、体積収縮で硬化反応溶液層(201)に変換され、前記粒子(100)は、前記硬化反応溶液層(201)を越えて突出し、前記反応溶液層(201)中に固定された底部側と前記反応溶液層(201)を越えて突出する上側とを有し、
− 上側領域セクションは、酸化的または還元的に調整され、それによって還元処理された粒子(102)の領域または酸化処理された粒子(103)の領域が定められ、次に、
− 鎖状、網状、網状管からなる群から選択される少なくとも1つの構造を含むナノスケール構造、好ましくはCNT鎖および/またはハロゲン鎖が、少なくとも1つの領域セクション中の粒子(100)と直接接触して形成され、
− 前記粒子(100)の相互に隣接する領域セクションは、異なる溶液で調整されて、還元処理された粒子(102)のセクションおよび酸化処理された粒子(103)のセクションとして交互シーケンスで前記粒子(100)の前記相互に隣接する領域セクションを形成し、
− ステップc)で、前記粒子の前記上側は、少なくとも部分的に上側接触部(400)を設けられ、前記粒子(100)の前記交互に調整された領域セクションは、直列に接続され、最終的な接触電極に接着される
ことを特徴とする方法。 - 請求項1乃至8の何れか一項に記載の方法において、前記接触電極は、埋込みフィルムの内側に印刷および/または配置され、前記方法によって得られた前記PV層シーケンスは、前記埋込みフィルム中に積層されて、前記埋込み材料から導かれる電気的接触を作り出すことを特徴とする方法。
- 請求項1乃至9の何れか一項に記載の方法に従って得られるPV層シーケンス。
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