JP2018522554A - 薬味ソースの殺菌方法 - Google Patents
薬味ソースの殺菌方法 Download PDFInfo
- Publication number
- JP2018522554A JP2018522554A JP2018501209A JP2018501209A JP2018522554A JP 2018522554 A JP2018522554 A JP 2018522554A JP 2018501209 A JP2018501209 A JP 2018501209A JP 2018501209 A JP2018501209 A JP 2018501209A JP 2018522554 A JP2018522554 A JP 2018522554A
- Authority
- JP
- Japan
- Prior art keywords
- sauce
- antibacterial agent
- spicy
- sterilizing
- solution containing
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 235000015067 sauces Nutrition 0.000 title claims abstract description 54
- 235000013409 condiments Nutrition 0.000 title claims abstract description 34
- 230000001954 sterilising effect Effects 0.000 claims abstract description 62
- 238000000034 method Methods 0.000 claims abstract description 59
- 235000013311 vegetables Nutrition 0.000 claims description 35
- 235000011194 food seasoning agent Nutrition 0.000 claims description 30
- 239000003242 anti bacterial agent Substances 0.000 claims description 29
- 235000006886 Zingiber officinale Nutrition 0.000 claims description 20
- 235000008397 ginger Nutrition 0.000 claims description 20
- 240000002234 Allium sativum Species 0.000 claims description 18
- 235000004611 garlic Nutrition 0.000 claims description 18
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 16
- 239000004615 ingredient Substances 0.000 claims description 11
- 238000004806 packaging method and process Methods 0.000 claims description 11
- 239000002562 thickening agent Substances 0.000 claims description 8
- 238000002156 mixing Methods 0.000 claims description 7
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 claims description 6
- OSVXSBDYLRYLIG-UHFFFAOYSA-N dioxidochlorine(.) Chemical compound O=Cl=O OSVXSBDYLRYLIG-UHFFFAOYSA-N 0.000 claims description 6
- 150000007524 organic acids Chemical class 0.000 claims description 6
- 108010062877 Bacteriocins Proteins 0.000 claims description 5
- 235000002566 Capsicum Nutrition 0.000 claims description 5
- 239000006002 Pepper Substances 0.000 claims description 5
- 235000016761 Piper aduncum Nutrition 0.000 claims description 5
- 235000017804 Piper guineense Nutrition 0.000 claims description 5
- 244000203593 Piper nigrum Species 0.000 claims description 5
- 235000008184 Piper nigrum Nutrition 0.000 claims description 5
- 235000013555 soy sauce Nutrition 0.000 claims description 5
- 241000234282 Allium Species 0.000 claims description 4
- 235000002732 Allium cepa var. cepa Nutrition 0.000 claims description 4
- 235000002568 Capsicum frutescens Nutrition 0.000 claims description 4
- 238000009835 boiling Methods 0.000 claims description 4
- QWPPOHNGKGFGJK-UHFFFAOYSA-N hypochlorous acid Chemical compound ClO QWPPOHNGKGFGJK-UHFFFAOYSA-N 0.000 claims description 4
- 235000005985 organic acids Nutrition 0.000 claims description 4
- 239000005022 packaging material Substances 0.000 claims description 4
- 235000000346 sugar Nutrition 0.000 claims description 4
- FHSWKZUNNVWBSG-UHFFFAOYSA-M 2-[3-[(4-amino-2-methylpyrimidin-5-yl)methyl]-4-methyl-1,3-thiazol-3-ium-5-yl]ethanol;dodecyl hydrogen sulfate;dodecyl sulfate Chemical compound CCCCCCCCCCCCOS(O)(=O)=O.CCCCCCCCCCCCOS([O-])(=O)=O.CC1=C(CCO)SC=[N+]1CC1=CN=C(C)N=C1N FHSWKZUNNVWBSG-UHFFFAOYSA-M 0.000 claims description 3
- 235000005254 Allium ampeloprasum Nutrition 0.000 claims description 3
- 240000006108 Allium ampeloprasum Species 0.000 claims description 3
- 241000512259 Ascophyllum nodosum Species 0.000 claims description 3
- 239000004155 Chlorine dioxide Substances 0.000 claims description 3
- 241000238557 Decapoda Species 0.000 claims description 3
- 240000000599 Lentinula edodes Species 0.000 claims description 3
- 244000294411 Mirabilis expansa Species 0.000 claims description 3
- 235000015429 Mirabilis expansa Nutrition 0.000 claims description 3
- CBENFWSGALASAD-UHFFFAOYSA-N Ozone Chemical compound [O-][O+]=O CBENFWSGALASAD-UHFFFAOYSA-N 0.000 claims description 3
- 108010039918 Polylysine Proteins 0.000 claims description 3
- 239000005708 Sodium hypochlorite Substances 0.000 claims description 3
- 235000019398 chlorine dioxide Nutrition 0.000 claims description 3
- 239000011521 glass Substances 0.000 claims description 3
- 239000000463 material Substances 0.000 claims description 3
- 235000013536 miso Nutrition 0.000 claims description 3
- 239000004033 plastic Substances 0.000 claims description 3
- 229920000656 polylysine Polymers 0.000 claims description 3
- 150000003839 salts Chemical class 0.000 claims description 3
- 238000002791 soaking Methods 0.000 claims description 3
- SUKJFIGYRHOWBL-UHFFFAOYSA-N sodium hypochlorite Chemical compound [Na+].Cl[O-] SUKJFIGYRHOWBL-UHFFFAOYSA-N 0.000 claims description 3
- 239000000052 vinegar Substances 0.000 claims description 3
- 235000021419 vinegar Nutrition 0.000 claims description 3
- 244000273928 Zingiber officinale Species 0.000 claims 1
- 238000004659 sterilization and disinfection Methods 0.000 abstract description 43
- 230000000694 effects Effects 0.000 abstract description 8
- 239000000796 flavoring agent Substances 0.000 abstract description 3
- 235000019634 flavors Nutrition 0.000 abstract description 3
- 235000013599 spices Nutrition 0.000 abstract 2
- 230000000844 anti-bacterial effect Effects 0.000 description 20
- 241000234314 Zingiber Species 0.000 description 19
- 238000010438 heat treatment Methods 0.000 description 15
- 241000894006 Bacteria Species 0.000 description 13
- 241000233866 Fungi Species 0.000 description 9
- 244000005700 microbiome Species 0.000 description 8
- 206010033546 Pallor Diseases 0.000 description 7
- 230000001953 sensory effect Effects 0.000 description 7
- 241000193830 Bacillus <bacterium> Species 0.000 description 5
- 238000005406 washing Methods 0.000 description 5
- 238000011156 evaluation Methods 0.000 description 4
- 235000021067 refined food Nutrition 0.000 description 4
- YLZOPXRUQYQQID-UHFFFAOYSA-N 3-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)-1-[4-[2-[[3-(trifluoromethoxy)phenyl]methylamino]pyrimidin-5-yl]piperazin-1-yl]propan-1-one Chemical compound N1N=NC=2CN(CCC=21)CCC(=O)N1CCN(CC1)C=1C=NC(=NC=1)NCC1=CC(=CC=C1)OC(F)(F)F YLZOPXRUQYQQID-UHFFFAOYSA-N 0.000 description 3
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 3
- 108010053775 Nisin Proteins 0.000 description 3
- NVNLLIYOARQCIX-MSHCCFNRSA-N Nisin Chemical compound N1C(=O)[C@@H](CC(C)C)NC(=O)C(=C)NC(=O)[C@@H]([C@H](C)CC)NC(=O)[C@@H](NC(=O)C(=C/C)/NC(=O)[C@H](N)[C@H](C)CC)CSC[C@@H]1C(=O)N[C@@H]1C(=O)N2CCC[C@@H]2C(=O)NCC(=O)N[C@@H](C(=O)N[C@H](CCCCN)C(=O)N[C@@H]2C(NCC(=O)N[C@H](C)C(=O)N[C@H](CC(C)C)C(=O)N[C@H](CCSC)C(=O)NCC(=O)N[C@H](CS[C@@H]2C)C(=O)N[C@H](CC(N)=O)C(=O)N[C@H](CCSC)C(=O)N[C@H](CCCCN)C(=O)N[C@@H]2C(N[C@H](C)C(=O)N[C@@H]3C(=O)N[C@@H](C(N[C@H](CC=4NC=NC=4)C(=O)N[C@H](CS[C@@H]3C)C(=O)N[C@H](CO)C(=O)N[C@H]([C@H](C)CC)C(=O)N[C@H](CC=3NC=NC=3)C(=O)N[C@H](C(C)C)C(=O)NC(=C)C(=O)N[C@H](CCCCN)C(O)=O)=O)CS[C@@H]2C)=O)=O)CS[C@@H]1C NVNLLIYOARQCIX-MSHCCFNRSA-N 0.000 description 3
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 3
- 238000007598 dipping method Methods 0.000 description 3
- 235000013305 food Nutrition 0.000 description 3
- 238000007654 immersion Methods 0.000 description 3
- 238000005259 measurement Methods 0.000 description 3
- 230000000813 microbial effect Effects 0.000 description 3
- 239000004309 nisin Substances 0.000 description 3
- 235000010297 nisin Nutrition 0.000 description 3
- VZSRBBMJRBPUNF-UHFFFAOYSA-N 2-(2,3-dihydro-1H-inden-2-ylamino)-N-[3-oxo-3-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)propyl]pyrimidine-5-carboxamide Chemical compound C1C(CC2=CC=CC=C12)NC1=NC=C(C=N1)C(=O)NCCC(N1CC2=C(CC1)NN=N2)=O VZSRBBMJRBPUNF-UHFFFAOYSA-N 0.000 description 2
- NIPNSKYNPDTRPC-UHFFFAOYSA-N N-[2-oxo-2-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)ethyl]-2-[[3-(trifluoromethoxy)phenyl]methylamino]pyrimidine-5-carboxamide Chemical compound O=C(CNC(=O)C=1C=NC(=NC=1)NCC1=CC(=CC=C1)OC(F)(F)F)N1CC2=C(CC1)NN=N2 NIPNSKYNPDTRPC-UHFFFAOYSA-N 0.000 description 2
- AFCARXCZXQIEQB-UHFFFAOYSA-N N-[3-oxo-3-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)propyl]-2-[[3-(trifluoromethoxy)phenyl]methylamino]pyrimidine-5-carboxamide Chemical compound O=C(CCNC(=O)C=1C=NC(=NC=1)NCC1=CC(=CC=C1)OC(F)(F)F)N1CC2=C(CC1)NN=N2 AFCARXCZXQIEQB-UHFFFAOYSA-N 0.000 description 2
- 230000001580 bacterial effect Effects 0.000 description 2
- 239000000356 contaminant Substances 0.000 description 2
- 238000010411 cooking Methods 0.000 description 2
- 230000018044 dehydration Effects 0.000 description 2
- 238000006297 dehydration reaction Methods 0.000 description 2
- 239000003205 fragrance Substances 0.000 description 2
- JVTAAEKCZFNVCJ-UHFFFAOYSA-N lactic acid Chemical compound CC(O)C(O)=O JVTAAEKCZFNVCJ-UHFFFAOYSA-N 0.000 description 2
- 239000002075 main ingredient Substances 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 238000005057 refrigeration Methods 0.000 description 2
- HMUNWXXNJPVALC-UHFFFAOYSA-N 1-[4-[2-(2,3-dihydro-1H-inden-2-ylamino)pyrimidin-5-yl]piperazin-1-yl]-2-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)ethanone Chemical compound C1C(CC2=CC=CC=C12)NC1=NC=C(C=N1)N1CCN(CC1)C(CN1CC2=C(CC1)NN=N2)=O HMUNWXXNJPVALC-UHFFFAOYSA-N 0.000 description 1
- LDXJRKWFNNFDSA-UHFFFAOYSA-N 2-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)-1-[4-[2-[[3-(trifluoromethoxy)phenyl]methylamino]pyrimidin-5-yl]piperazin-1-yl]ethanone Chemical compound C1CN(CC2=NNN=C21)CC(=O)N3CCN(CC3)C4=CN=C(N=C4)NCC5=CC(=CC=C5)OC(F)(F)F LDXJRKWFNNFDSA-UHFFFAOYSA-N 0.000 description 1
- MSWZFWKMSRAUBD-IVMDWMLBSA-N 2-amino-2-deoxy-D-glucopyranose Chemical compound N[C@H]1C(O)O[C@H](CO)[C@@H](O)[C@@H]1O MSWZFWKMSRAUBD-IVMDWMLBSA-N 0.000 description 1
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
- 229920002134 Carboxymethyl cellulose Polymers 0.000 description 1
- 239000004278 EU approved seasoning Substances 0.000 description 1
- 102000004190 Enzymes Human genes 0.000 description 1
- 108090000790 Enzymes Proteins 0.000 description 1
- 229920002907 Guar gum Polymers 0.000 description 1
- 235000001715 Lentinula edodes Nutrition 0.000 description 1
- 239000004368 Modified starch Substances 0.000 description 1
- 229920000881 Modified starch Polymers 0.000 description 1
- MKYBYDHXWVHEJW-UHFFFAOYSA-N N-[1-oxo-1-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)propan-2-yl]-2-[[3-(trifluoromethoxy)phenyl]methylamino]pyrimidine-5-carboxamide Chemical compound O=C(C(C)NC(=O)C=1C=NC(=NC=1)NCC1=CC(=CC=C1)OC(F)(F)F)N1CC2=C(CC1)NN=N2 MKYBYDHXWVHEJW-UHFFFAOYSA-N 0.000 description 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 1
- HDSBZMRLPLPFLQ-UHFFFAOYSA-N Propylene glycol alginate Chemical compound OC1C(O)C(OC)OC(C(O)=O)C1OC1C(O)C(O)C(C)C(C(=O)OCC(C)O)O1 HDSBZMRLPLPFLQ-UHFFFAOYSA-N 0.000 description 1
- 240000004808 Saccharomyces cerevisiae Species 0.000 description 1
- KDYFGRWQOYBRFD-UHFFFAOYSA-N Succinic acid Natural products OC(=O)CCC(O)=O KDYFGRWQOYBRFD-UHFFFAOYSA-N 0.000 description 1
- 241000607479 Yersinia pestis Species 0.000 description 1
- 150000001298 alcohols Chemical class 0.000 description 1
- 235000010407 ammonium alginate Nutrition 0.000 description 1
- 239000000728 ammonium alginate Substances 0.000 description 1
- KPGABFJTMYCRHJ-YZOKENDUSA-N ammonium alginate Chemical compound [NH4+].[NH4+].O1[C@@H](C([O-])=O)[C@@H](OC)[C@H](O)[C@H](O)[C@@H]1O[C@@H]1[C@@H](C([O-])=O)O[C@@H](O)[C@@H](O)[C@H]1O KPGABFJTMYCRHJ-YZOKENDUSA-N 0.000 description 1
- MSWZFWKMSRAUBD-UHFFFAOYSA-N beta-D-galactosamine Natural products NC1C(O)OC(CO)C(O)C1O MSWZFWKMSRAUBD-UHFFFAOYSA-N 0.000 description 1
- KDYFGRWQOYBRFD-NUQCWPJISA-N butanedioic acid Chemical compound O[14C](=O)CC[14C](O)=O KDYFGRWQOYBRFD-NUQCWPJISA-N 0.000 description 1
- 239000011575 calcium Substances 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- 239000001768 carboxy methyl cellulose Substances 0.000 description 1
- 235000010948 carboxy methyl cellulose Nutrition 0.000 description 1
- 239000008112 carboxymethyl-cellulose Substances 0.000 description 1
- 230000015556 catabolic process Effects 0.000 description 1
- 238000012258 culturing Methods 0.000 description 1
- 238000006731 degradation reaction Methods 0.000 description 1
- 230000006866 deterioration Effects 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 239000000428 dust Substances 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 235000013373 food additive Nutrition 0.000 description 1
- 239000002778 food additive Substances 0.000 description 1
- 229960002442 glucosamine Drugs 0.000 description 1
- 239000000665 guar gum Substances 0.000 description 1
- 235000010417 guar gum Nutrition 0.000 description 1
- 229960002154 guar gum Drugs 0.000 description 1
- 230000002779 inactivation Effects 0.000 description 1
- 230000002401 inhibitory effect Effects 0.000 description 1
- 239000004310 lactic acid Substances 0.000 description 1
- 235000014655 lactic acid Nutrition 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 235000019426 modified starch Nutrition 0.000 description 1
- 238000005457 optimization Methods 0.000 description 1
- 239000001814 pectin Substances 0.000 description 1
- 235000010987 pectin Nutrition 0.000 description 1
- 229920001277 pectin Polymers 0.000 description 1
- 229960000292 pectin Drugs 0.000 description 1
- 239000011591 potassium Substances 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- 238000002203 pretreatment Methods 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 235000010409 propane-1,2-diol alginate Nutrition 0.000 description 1
- 239000000770 propane-1,2-diol alginate Substances 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000004094 surface-active agent Substances 0.000 description 1
Images
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L3/00—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs
- A23L3/015—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with pressure variation, shock, acceleration or shear stress or cavitation
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23B—PRESERVING, e.g. BY CANNING, MEAT, FISH, EGGS, FRUIT, VEGETABLES, EDIBLE SEEDS; CHEMICAL RIPENING OF FRUIT OR VEGETABLES; THE PRESERVED, RIPENED, OR CANNED PRODUCTS
- A23B7/00—Preservation or chemical ripening of fruit or vegetables
- A23B7/06—Blanching
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23B—PRESERVING, e.g. BY CANNING, MEAT, FISH, EGGS, FRUIT, VEGETABLES, EDIBLE SEEDS; CHEMICAL RIPENING OF FRUIT OR VEGETABLES; THE PRESERVED, RIPENED, OR CANNED PRODUCTS
- A23B7/00—Preservation or chemical ripening of fruit or vegetables
- A23B7/14—Preserving or ripening with chemicals not covered by groups A23B7/08 or A23B7/10
- A23B7/153—Preserving or ripening with chemicals not covered by groups A23B7/08 or A23B7/10 in the form of liquids or solids
- A23B7/157—Inorganic compounds
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L23/00—Soups; Sauces; Preparation or treatment thereof
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L27/00—Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
- A23L27/10—Natural spices, flavouring agents or condiments; Extracts thereof
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L3/00—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs
- A23L3/015—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with pressure variation, shock, acceleration or shear stress or cavitation
- A23L3/0155—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with pressure variation, shock, acceleration or shear stress or cavitation using sub- or super-atmospheric pressures, or pressure variations transmitted by a liquid or gas
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L3/00—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs
- A23L3/02—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by heating materials in packages which are progressively transported, continuously or stepwise, through the apparatus
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L3/00—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs
- A23L3/10—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by heating materials in packages which are not progressively transported through the apparatus
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L3/00—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs
- A23L3/16—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by heating loose unpacked materials
- A23L3/165—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by heating loose unpacked materials in solid state
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L3/00—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs
- A23L3/34—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L3/00—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs
- A23L3/34—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals
- A23L3/3454—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals in the form of liquids or solids
- A23L3/3463—Organic compounds; Microorganisms; Enzymes
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L3/00—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs
- A23L3/34—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals
- A23L3/3454—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals in the form of liquids or solids
- A23L3/358—Inorganic compounds
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A40/00—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production
- Y02A40/90—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production in food processing or handling, e.g. food conservation
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Microbiology (AREA)
- Seasonings (AREA)
- Seeds, Soups, And Other Foods (AREA)
- Preparation Of Fruits And Vegetables (AREA)
- Food Preservation Except Freezing, Refrigeration, And Drying (AREA)
- Packging For Living Organisms, Food Or Medicinal Products That Are Sensitive To Environmental Conditiond (AREA)
Abstract
Description
上記抗菌剤を含む溶液に浸漬した香辛野菜をゆでる段階と、
上記ゆでた香辛野菜を調味原料及び増粘剤と混合して薬味ソースを得る段階と、
上記薬味ソースを包装して超高圧で殺菌する段階と、を含む薬味ソースの殺菌方法を提供することである。
上記抗菌剤を含む溶液に浸漬した香辛野菜をゆでる段階(S102)と、
上記ゆでた香辛野菜を調味原料及び増粘剤と混合して薬味ソースを得る段階(S103)と、
上記薬味ソースを包装して超高圧で殺菌する段階(S104)と、を含む薬味ソースの殺菌方法を提供する。
上記抗菌剤を含む溶液に浸漬した香辛野菜をゆでる段階と、
上記ゆでた香辛野菜を調味原料及び増粘剤と混合して薬味ソースを得る段階と、
上記薬味ソースを包装して超高圧で殺菌する段階と、を含む薬味ソースの殺菌方法を提供する。
本発明の一実施例に係る殺菌方法を用いて滅菌した薬味ソースを製造し、そのフローチャートを図1に示した。香辛野菜としてはニンニクとショウガを使用した。
ニンニクとショウガの表面についているホコリ、異物などの汚染物質を除去するために、きれいな水で3回洗浄した後、脱水機で700rpm、1分間回転脱水した。脱水後に、損傷したり病害虫にやられたニンニク、ショウガは選別して除去した。
洗浄及び選別を終えたニンニク及びショウガは、常温の100ppm次亜塩素酸(hypochlorous acid)溶液で1時間浸漬した後(以下、「抗菌溶液浸漬法」と称する。)、きれいな水で洗浄した後、95℃の水で30秒間ブランチング加熱(以下、「ブランチング加熱法」と称する。)を実施した。
上記実施例1−2の前処理殺菌工程を経たニンニク、ショウガは細かく切った後、砂糖、醤油、調味料などの調味原料及び増粘剤と混合し、85℃、20分内外の加熱を行って薬味ソースを製造した。
上記実施例1−1〜実施例1−3の過程を経て製造された薬味ソースは、透明な耐熱性パウチに200g単位で包装した後、25℃〜100℃の温度で500MPaの圧力で3分〜10分間処理し、冷蔵又は常温流通が可能な加工食品として製造した。
ニンニク、ショウガの前処理殺菌処理を恒温循環水槽を用いて行い、総細菌、バチルス系の耐熱性細菌、酵母及びかびのような真菌類に対する殺菌効果をそれぞれ確認した。
ニンニク及びショウガの試料に対して様々な殺菌方法における殺菌効果を確認した。実験の結果、表1に示すように、みじん切りしたニンニク、ショウガ自体の抗菌成分は、真菌類において殺菌効果があるが、耐熱性細菌であるバチルスが約103CFU/gで自生しており、総細菌数においては殺菌効果がほとんどなかった。また、抗菌溶液浸漬法の場合、丸ごとのショウガ内の真菌の殺菌には多少効果があると確認されたが、総細菌数にはほとんど変化がないことから、バチルス系の耐熱性細菌には殺菌効果がないことが確認された。これに対し、90℃、40秒間実施するブランチング加熱法では、ニンニクもショウガも、総細菌数及び真菌数が約103CFU/gであって、最も効果的な方法であることが確認された。
表2に示すように、90℃〜95℃、30秒〜40秒間ブランチング加熱時に、丸ごとのニンニクでは細菌、真菌の両方とも死滅したことが確認され、丸ごとのショウガでは、バチルス系の耐熱性細菌がニンニクに比べて多く自生しているため、ブランチング後にも約102CFU/gの細菌が残存したことが確認された。
超高圧殺菌工程は、実験室規模の超高圧機(High pressure processor)(Hiperbaric社製)を用いて、パウチで包装された試料にそれぞれ、0、5、10、15、20分間100、300、500MPaの圧力を加えた。この時、温度は、実験群の条件によって25℃〜100℃に設定し、超高圧上昇時間(Come−up times)は100〜500MPaで26秒〜2分30秒がかかった。殺菌を終えた後、細菌及び真菌の測定は、該当の微生物別に適正な培地を使用して37℃、48時間培養し、コロニー計数方法を用いて分析した。
実施例2−2によって前処理殺菌工程(抗菌溶液浸漬法及びブランチング加熱法)を経たニンニクとショウガを使って薬味ソースを製造し、製造した薬味ソースを、25℃の常温で3分間500MPaの超高圧で加圧した後、それぞれ冷蔵及び常温で保存した結果、表4に示すように、いずれも微生物増殖が観察されず、微生物に対する安全性を確保できたことが分かる。
実施例2−2によって前処理殺菌工程を経たニンニクとショウガを使用して薬味ソースを製造し、製造した薬味ソースを90℃〜100℃の温度で3分間500MPaの超高圧で加圧した後、それぞれ冷蔵及び常温で保存した結果、表4に示すように、いずれも微生物増殖が観察されず、微生物に対する安全性を確保できたことが分かる。
Claims (9)
- 香辛野菜を、抗菌剤を含む溶液に浸漬する段階と、
上記抗菌剤を含む溶液に浸漬した香辛野菜をゆでる段階と、
上記ゆでた香辛野菜を調味原料及び増粘剤と混合して薬味ソースを得る段階と、
上記薬味ソースを包装して超高圧で殺菌する段階と、
を含む薬味ソースの殺菌方法。 - 上記香辛野菜は、ニンニク、ショウガ、唐辛子、コショウ、玉ネギ及びネギからなる群から選ばれる一つ以上である、請求項1に記載の方法。
- 上記抗菌剤は、次亜塩素酸ナトリウム、次亜塩素酸、二酸化塩素、オゾン、過酸化水素、有機酸、バクテリオシン、ポリリシン及びビタミンB1ラウリル硫酸塩からなる群から選ばれる、請求項1に記載の方法。
- 上記抗菌剤を含む溶液は、0.01%〜3%(w/w)の抗菌剤を含む、請求項1に記載の方法。
- 上記ゆでる段階は、上記抗菌剤を含む溶液に浸漬した香辛野菜を80℃〜100℃の温度の水でゆでることを含む、請求項1に記載の方法。
- 上記調味原料は、砂糖、塩、醤油、コチュジャン、味噌、酢、粉唐辛子、昆布、海老、煮干し及び椎茸からなる群から選ばれる一つ以上である、請求項1に記載の方法。
- 上記殺菌する段階は、200MPa〜900MPaの圧力を加えることを含む、請求項1に記載の方法。
- 上記殺菌する段階は、20℃〜100℃の温度でなされる、請求項1に記載の方法。
- 上記包装は、上記薬味ソースをパウチ、プラスチック容器、ガラス瓶、チューブ及び缶からなる群から選ばれる包装材料で包装する、請求項1に記載の方法。
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
KR10-2015-0099234 | 2015-07-13 | ||
KR1020150099234A KR101786182B1 (ko) | 2015-07-13 | 2015-07-13 | 양념 소스의 살균 방법 |
PCT/KR2016/005425 WO2017010675A1 (ko) | 2015-07-13 | 2016-05-23 | 양념 소스의 살균 방법 |
Publications (2)
Publication Number | Publication Date |
---|---|
JP2018522554A true JP2018522554A (ja) | 2018-08-16 |
JP6577129B2 JP6577129B2 (ja) | 2019-09-18 |
Family
ID=57758106
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP2018501209A Active JP6577129B2 (ja) | 2015-07-13 | 2016-05-23 | 薬味ソースの殺菌方法 |
Country Status (6)
Country | Link |
---|---|
US (1) | US20190116845A1 (ja) |
EP (1) | EP3323297A4 (ja) |
JP (1) | JP6577129B2 (ja) |
KR (1) | KR101786182B1 (ja) |
CN (1) | CN107835644A (ja) |
WO (1) | WO2017010675A1 (ja) |
Families Citing this family (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN110742083A (zh) * | 2019-10-12 | 2020-02-04 | 中粮屯河糖业股份有限公司 | 甜菜杀菌剂及其制备方法和应用 |
KR102413384B1 (ko) * | 2020-08-25 | 2022-06-24 | 백현아 | 차아염소산수 기반의 천연물 살균소독제 및 그 제조 방법 |
CN113317483A (zh) * | 2021-06-16 | 2021-08-31 | 北京工商大学 | 排骨风味的香精及其制备方法、食品 |
Citations (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS52136931A (en) * | 1976-05-11 | 1977-11-16 | Sanei Kagaku Kogyo Kk | Material for treated meat and vegetable food |
JPS58129934A (ja) * | 1982-01-27 | 1983-08-03 | Fujimasa Shokuhin Kk | 落花生餡の製造方法 |
JPS62236466A (ja) * | 1986-04-04 | 1987-10-16 | Lion Corp | 練りわさびの製造法 |
US20020028268A1 (en) * | 1999-08-31 | 2002-03-07 | Kraft Foods Holdings, Inc. | Stabilization of cooked meat and meat-vegetable compositions using whey from nisin-producing cultures |
JP2007104979A (ja) * | 2005-10-14 | 2007-04-26 | Miyagi Prefecture | 分離液状ドレッシングおよびその製造方法 |
KR20090108970A (ko) * | 2008-04-14 | 2009-10-19 | 황보람 | 과일 한방 소스 |
KR20120014665A (ko) * | 2010-08-10 | 2012-02-20 | (주)청룡수산 | 고등어 조림용 소스의 제조 방법 |
WO2015016458A2 (ko) * | 2013-07-31 | 2015-02-05 | 씨제이제일제당(주) | 초고압을 이용한 야채류 식품의 제조방법 |
Family Cites Families (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH07115925A (ja) * | 1993-10-22 | 1995-05-09 | Shokuhin Sangyo Chokoatsu Riyou Gijutsu Kenkyu Kumiai | ペースト状食品 |
KR960028848A (ko) * | 1995-01-10 | 1996-08-17 | 김정순 | 초고압을 이용한 페이스트상 식품의 새로운 살균방법 |
US7175870B2 (en) * | 2004-01-08 | 2007-02-13 | The Garlic Company | Processed garlic pieces |
KR20100046972A (ko) * | 2008-10-28 | 2010-05-07 | 한국식품연구원 | 식품의 살균 방법 |
US20110274766A1 (en) * | 2010-05-05 | 2011-11-10 | Allen Randall R | Synergy of Strong Acids and Peroxy Compounds |
CN102077858A (zh) * | 2010-11-22 | 2011-06-01 | 天津光辉食品有限公司 | 一种超高压蔬菜食品的加工方法 |
US20130078339A1 (en) * | 2011-09-27 | 2013-03-28 | Caitlin Elizabeth Trahan | High Pressure Processing of Pathogenostat-Treated Food Articles |
JP5909614B2 (ja) * | 2011-09-28 | 2016-04-27 | バイオジェニック株式会社 | 生姜を含むペーストの製造方法 |
US20130183420A1 (en) * | 2012-01-13 | 2013-07-18 | Justin Wade Shimek | Premium Quality Refrigerated Vegetable Products and Methods of Making Them |
US20150056359A1 (en) * | 2013-08-16 | 2015-02-26 | Robert Jensen | Integral sauteed peppers and onions condiment/sauce for flavor and aroma enhancement of foods |
-
2015
- 2015-07-13 KR KR1020150099234A patent/KR101786182B1/ko active IP Right Grant
-
2016
- 2016-05-23 EP EP16824592.6A patent/EP3323297A4/en active Pending
- 2016-05-23 CN CN201680041186.2A patent/CN107835644A/zh active Pending
- 2016-05-23 JP JP2018501209A patent/JP6577129B2/ja active Active
- 2016-05-23 WO PCT/KR2016/005425 patent/WO2017010675A1/ko active Application Filing
- 2016-05-23 US US15/743,084 patent/US20190116845A1/en not_active Abandoned
Patent Citations (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS52136931A (en) * | 1976-05-11 | 1977-11-16 | Sanei Kagaku Kogyo Kk | Material for treated meat and vegetable food |
JPS58129934A (ja) * | 1982-01-27 | 1983-08-03 | Fujimasa Shokuhin Kk | 落花生餡の製造方法 |
JPS62236466A (ja) * | 1986-04-04 | 1987-10-16 | Lion Corp | 練りわさびの製造法 |
US20020028268A1 (en) * | 1999-08-31 | 2002-03-07 | Kraft Foods Holdings, Inc. | Stabilization of cooked meat and meat-vegetable compositions using whey from nisin-producing cultures |
JP2007104979A (ja) * | 2005-10-14 | 2007-04-26 | Miyagi Prefecture | 分離液状ドレッシングおよびその製造方法 |
KR20090108970A (ko) * | 2008-04-14 | 2009-10-19 | 황보람 | 과일 한방 소스 |
KR20120014665A (ko) * | 2010-08-10 | 2012-02-20 | (주)청룡수산 | 고등어 조림용 소스의 제조 방법 |
WO2015016458A2 (ko) * | 2013-07-31 | 2015-02-05 | 씨제이제일제당(주) | 초고압을 이용한 야채류 식품의 제조방법 |
Also Published As
Publication number | Publication date |
---|---|
JP6577129B2 (ja) | 2019-09-18 |
EP3323297A4 (en) | 2019-01-16 |
CN107835644A (zh) | 2018-03-23 |
WO2017010675A1 (ko) | 2017-01-19 |
KR20170008028A (ko) | 2017-01-23 |
KR101786182B1 (ko) | 2017-10-17 |
US20190116845A1 (en) | 2019-04-25 |
EP3323297A1 (en) | 2018-05-23 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
Di Cagno et al. | Exploitation of vegetables and fruits through lactic acid fermentation | |
JP6532463B2 (ja) | 超高圧を用いた野菜類食品の製造方法 | |
Barth et al. | Microbiological spoilage of fruits and vegetables | |
KR101907743B1 (ko) | 마이크로파 가열 전처리를 포함하는 가공 식품의 살균방법 | |
Artes et al. | Minimal processing of fresh fruit, vegetables, and juices | |
WO2001056408A1 (fr) | Procedes de production d'aliments presentant de bonnes qualites de conservation et agents de conservation d'aliments | |
JP6577129B2 (ja) | 薬味ソースの殺菌方法 | |
CN106174266A (zh) | 酱腌菜加工工艺 | |
CN105995917B (zh) | 泡椒酱汁及其制备方法 | |
Wacher et al. | Fermented vegetable products | |
Jamaluddin et al. | A review of clean‐label approaches to chilli paste processing | |
CN107279670B (zh) | 一种即食臭鳜鱼的制备方法及其保鲜液 | |
JP4964076B2 (ja) | 容器詰め殺菌野菜の製造方法 | |
CN105995776A (zh) | 一种低亚硝酸盐倒坛腌制蔬菜及其制作方法 | |
CN105918427A (zh) | 一种酱卤肉制品的保鲜方法 | |
JP7036425B2 (ja) | 椎茸エキスの製造方法およびその椎茸エキスを含有する日持向上剤 | |
KR101105469B1 (ko) | 상온유통이 가능한 레토르트 게살스프 제품 및 그의 제조방법 | |
JP2011139648A (ja) | 長期間の保存が可能な加熱加工ジャガイモおよびその製造方法 | |
Xu et al. | Application of pulsed light (PL)-surfactant combination on inactivation of Salmonella and apparent quality of green onions | |
KR101870570B1 (ko) | 김치 양념 소스의 제조방법 | |
JP2004215544A (ja) | 生鮮野菜の鮮度保持方法および保存性のよい生鮮野菜 | |
Thakur et al. | Increased shelf life and safety of ketchup prepared from organically raised tomato (cv. Solan lalima) | |
Singh et al. | Effect of processing methods on physico-chemical properties, sensory evaluations and storage studies of cauliflower (Brassica oleracea L. var. botrytis) Pickle | |
Board | Modern Technology on Food Preservation | |
JP2017195792A (ja) | 野菜炒め用調味液及びその製造方法 |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
A621 | Written request for application examination |
Free format text: JAPANESE INTERMEDIATE CODE: A621 Effective date: 20180112 |
|
A131 | Notification of reasons for refusal |
Free format text: JAPANESE INTERMEDIATE CODE: A131 Effective date: 20181203 |
|
A521 | Request for written amendment filed |
Free format text: JAPANESE INTERMEDIATE CODE: A523 Effective date: 20190304 |
|
TRDD | Decision of grant or rejection written | ||
A01 | Written decision to grant a patent or to grant a registration (utility model) |
Free format text: JAPANESE INTERMEDIATE CODE: A01 Effective date: 20190722 |
|
A61 | First payment of annual fees (during grant procedure) |
Free format text: JAPANESE INTERMEDIATE CODE: A61 Effective date: 20190821 |
|
R150 | Certificate of patent or registration of utility model |
Ref document number: 6577129 Country of ref document: JP Free format text: JAPANESE INTERMEDIATE CODE: R150 |
|
R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |