JP2018521060A - 日焼け止め用化粧料組成物 - Google Patents
日焼け止め用化粧料組成物 Download PDFInfo
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- JP2018521060A JP2018521060A JP2017568171A JP2017568171A JP2018521060A JP 2018521060 A JP2018521060 A JP 2018521060A JP 2017568171 A JP2017568171 A JP 2017568171A JP 2017568171 A JP2017568171 A JP 2017568171A JP 2018521060 A JP2018521060 A JP 2018521060A
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- 239000002537 cosmetic Substances 0.000 title claims abstract description 90
- 239000000516 sunscreening agent Substances 0.000 title claims abstract description 84
- 230000000475 sunscreen effect Effects 0.000 title claims abstract description 70
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims abstract description 85
- 239000004408 titanium dioxide Substances 0.000 claims abstract description 42
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- XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 claims description 16
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- HEOCBCNFKCOKBX-RELGSGGGSA-N (1s,2e,4r)-4,7,7-trimethyl-2-[(4-methylphenyl)methylidene]bicyclo[2.2.1]heptan-3-one Chemical compound C1=CC(C)=CC=C1\C=C/1C(=O)[C@]2(C)CC[C@H]\1C2(C)C HEOCBCNFKCOKBX-RELGSGGGSA-N 0.000 claims description 2
- TYYHDKOVFSVWON-UHFFFAOYSA-N 2-butyl-2-methoxy-1,3-diphenylpropane-1,3-dione Chemical compound C=1C=CC=CC=1C(=O)C(OC)(CCCC)C(=O)C1=CC=CC=C1 TYYHDKOVFSVWON-UHFFFAOYSA-N 0.000 claims description 2
- JGUMTYWKIBJSTN-UHFFFAOYSA-N 2-ethylhexyl 4-[[4,6-bis[4-(2-ethylhexoxycarbonyl)anilino]-1,3,5-triazin-2-yl]amino]benzoate Chemical compound C1=CC(C(=O)OCC(CC)CCCC)=CC=C1NC1=NC(NC=2C=CC(=CC=2)C(=O)OCC(CC)CCCC)=NC(NC=2C=CC(=CC=2)C(=O)OCC(CC)CCCC)=N1 JGUMTYWKIBJSTN-UHFFFAOYSA-N 0.000 claims description 2
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- SOXAGEOHPCXXIO-DVOMOZLQSA-N menthyl anthranilate Chemical compound CC(C)[C@@H]1CC[C@@H](C)C[C@H]1OC(=O)C1=CC=CC=C1N SOXAGEOHPCXXIO-DVOMOZLQSA-N 0.000 claims description 2
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- FMJSMJQBSVNSBF-UHFFFAOYSA-N octocrylene Chemical group C=1C=CC=CC=1C(=C(C#N)C(=O)OCC(CC)CCCC)C1=CC=CC=C1 FMJSMJQBSVNSBF-UHFFFAOYSA-N 0.000 claims description 2
- 229960000601 octocrylene Drugs 0.000 claims description 2
- DXGLGDHPHMLXJC-UHFFFAOYSA-N oxybenzone Chemical compound OC1=CC(OC)=CC=C1C(=O)C1=CC=CC=C1 DXGLGDHPHMLXJC-UHFFFAOYSA-N 0.000 claims description 2
- 229960001173 oxybenzone Drugs 0.000 claims description 2
- 239000000725 suspension Substances 0.000 claims description 2
- AKUPYGILGNUOIG-UHFFFAOYSA-N 5-methoxy-4-phenyltriazine Chemical compound COC1=CN=NN=C1C1=CC=CC=C1 AKUPYGILGNUOIG-UHFFFAOYSA-N 0.000 claims 1
- VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 claims 1
- 239000005977 Ethylene Substances 0.000 claims 1
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- 150000001993 dienes Chemical class 0.000 claims 1
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- 239000004814 polyurethane Substances 0.000 claims 1
- 239000002552 dosage form Substances 0.000 abstract description 6
- 235000010215 titanium dioxide Nutrition 0.000 description 38
- JOYRKODLDBILNP-UHFFFAOYSA-N Ethyl urethane Chemical compound CCOC(N)=O JOYRKODLDBILNP-UHFFFAOYSA-N 0.000 description 22
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- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- XPSXNFUPMKXMLB-UHFFFAOYSA-N 3-ethyl-2-hexoxyphenol;5-methoxy-4-phenyltriazine Chemical compound COC1=CN=NN=C1C1=CC=CC=C1.CCCCCCOC1=C(O)C=CC=C1CC XPSXNFUPMKXMLB-UHFFFAOYSA-N 0.000 description 1
- 239000004606 Fillers/Extenders Substances 0.000 description 1
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- XVAMCHGMPYWHNL-UHFFFAOYSA-N bemotrizinol Chemical compound OC1=CC(OCC(CC)CCCC)=CC=C1C1=NC(C=2C=CC(OC)=CC=2)=NC(C=2C(=CC(OCC(CC)CCCC)=CC=2)O)=N1 XVAMCHGMPYWHNL-UHFFFAOYSA-N 0.000 description 1
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- 239000000686 essence Substances 0.000 description 1
- RTZKZFJDLAIYFH-UHFFFAOYSA-N ether Substances CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
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- 210000004709 eyebrow Anatomy 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
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- 238000012812 general test Methods 0.000 description 1
- 238000005470 impregnation Methods 0.000 description 1
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- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- WWZKQHOCKIZLMA-UHFFFAOYSA-N octanoic acid Chemical compound CCCCCCCC(O)=O WWZKQHOCKIZLMA-UHFFFAOYSA-N 0.000 description 1
- 239000004533 oil dispersion Substances 0.000 description 1
- 230000008520 organization Effects 0.000 description 1
- SOQBVABWOPYFQZ-UHFFFAOYSA-N oxygen(2-);titanium(4+) Chemical class [O-2].[O-2].[Ti+4] SOQBVABWOPYFQZ-UHFFFAOYSA-N 0.000 description 1
- 239000006072 paste Substances 0.000 description 1
- 229920003023 plastic Polymers 0.000 description 1
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- 239000000243 solution Substances 0.000 description 1
- 239000013589 supplement Substances 0.000 description 1
- LADGBHLMCUINGV-UHFFFAOYSA-N tricaprin Chemical compound CCCCCCCCCC(=O)OCC(OC(=O)CCCCCCCCC)COC(=O)CCCCCCCCC LADGBHLMCUINGV-UHFFFAOYSA-N 0.000 description 1
- 125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 description 1
- 229920002554 vinyl polymer Polymers 0.000 description 1
- 238000005303 weighing Methods 0.000 description 1
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Classifications
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/29—Titanium; Compounds thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0241—Containing particulates characterized by their shape and/or structure
- A61K8/025—Explicitly spheroidal or spherical shape
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/04—Dispersions; Emulsions
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/04—Dispersions; Emulsions
- A61K8/042—Gels
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
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- A61K8/044—Suspensions
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
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- A—HUMAN NECESSITIES
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/27—Zinc; Compounds thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/04—Topical preparations for affording protection against sunlight or other radiation; Topical sun tanning preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/41—Particular ingredients further characterized by their size
- A61K2800/412—Microsized, i.e. having sizes between 0.1 and 100 microns
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
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- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Veterinary Medicine (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Birds (AREA)
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- Chemical & Material Sciences (AREA)
- Dispersion Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Dermatology (AREA)
- Cosmetics (AREA)
Abstract
Description
下表1の組成に従い、当業界の通常的な方法にて日焼け止め化粧料組成物を製造した。具体的に、下記の日焼け止め剤、油性成分、及び界面活性剤を混合し、室温で撹拌して均一にした後、これに、下記増粘剤を混合して均一に撹拌した。次いで、ピグメントを混合し均一に撹拌した。別途のミキサーに下記水性成分を混合し、室温で撹拌して完全に溶解させた。均一に撹拌した前記水性成分を前記製造した油性成分を含む混合物にゆっくり投入し、ホモジナイザーを利用して乳化させた。次いで、皮膚保護成分及び香料などを投入してからこれを冷却して、W/O日焼け止め用化粧料組成物に係る実施例1、比較例1及び2をそれぞれ得た。
1)Petri dishを用いて粉末原料(日焼け止め剤)1.00gを測量する。
2)Syringe+CSA(Caprylic/Capric Triglyceride)の重さを測量する。
3)Syringeを用いて2)のCSAを1)の粉末原料に適正量投入する。
4)スパチュラを用いて3)の粉末とオイルとを混ぜ合わせる。
5)3)の粉末がオイルによって固まる時点まで2)〜3)の過程を繰り返す。
6)Syringe+CSAの重さ測量によって投入オイル量を測定する。
前記製造された実施例1及び比較例1、2の安定度、紫外線防止度及び使用性を下記の方法にてそれぞれ評価した。
下表5の組成にて、当業界の通常的な方法にて日焼け止め化粧料組成物を製造した。具体的に、下記の日焼け止め剤、油性成分、及び界面活性剤を混合し、室温で撹拌して均一にした後、これに、下記増粘剤を混合して均一に撹拌した。次いで、ピグメント及びパウダーを混合し均一に撹拌した。別途のミキサーに下記水性成分を混合し、室温で撹拌して完全に溶解させた。均一に撹拌した前記水性成分を前記製造した油性成分を含む混合物にゆっくり投入し、ホモジナイザーを利用して乳化させた。次いで、これを冷却して、W/O日焼け止め用化粧料組成物に係る実施例2、3、及び比較例3、4をそれぞれ得た。
充填能は、化粧料15gを手動で発泡ウレタンフォームに充填(容器に担体を入れてスパチュラを用いて充填)される時間で測定した。具体的に、円径44mm×高さ9.0mmの大きさの発泡ウレタンフォームに前記実施例2、3及び比較例3、4の各日焼け止め化粧料組成物15gを手動で充填するのに掛かる時間を測定した。
Claims (11)
- 70nm超過150nm以下の中央体積粒子径を有し且つ吸油量が0超過0.5以下の球状(sphere)の微粒子二酸化チタンを含む、日焼け止め用化粧料組成物;及び
前記日焼け止め用化粧料組成物が含浸されるスポンジを含む担体;を含む、化粧品。 - 前記日焼け止め用化粧料組成物は、前記球状の微粒子二酸化チタンを組成物の総質量に対して0.1〜25質量%で含む、請求項1に記載の化粧品。
- 前記日焼け止め用化粧料組成物は、前記球状の微粒子二酸化チタン以外の無機日焼け止め剤及び有機日焼け止め剤のうち一つ以上を更に含む、請求項1に記載の化粧品。
- 前記無機日焼け止め剤は、吸油量が0.5〜1.0である、非球状を有する微粒子二酸化チタン及び酸化亜鉛のうち一つ以上を含み、
前記有機日焼け止め剤は、オクチルメトキシシンナメート、エチルヘキシルメトキシシンナメート、オクトクリレン、アボベンゼン、ブチルメトキシジベンゾイルメタン、オキシベンゾン、オクチルトリアゾン、メンチルアントラニレート、3,4−メチルベンジリデンカンファー、及びビス−エチルヘキシルオキシフェノールメトキシフェニルトリアジンのうち一つ以上を含む、請求項3に記載の化粧品。 - 前記日焼け止め用化粧料組成物は、前記無機日焼け止め剤を組成物の総質量に対して0.1〜25質量%で更に含む、請求項3に記載の化粧品。
- 前記日焼け止め用化粧料組成物は、前記有機日焼け止め剤を組成物の総質量に対して0.1〜10質量%で更に含む、請求項3に記載の化粧品。
- 前記日焼け止め用化粧料組成物は、紫外線防止指数(Sun Protection Factor、SPF)が30以上であり、且つ紫外線A防止グレイド(Protection grade of UVA、PA)がダブルプラス(PA++)乃至トリプルプラス(PA+++)である、請求項1に記載の化粧品。
- 前記日焼け止め用化粧料組成物は、溶液、エマルジョン、ゲル、クリーム、及び懸濁液からなる群より選択されるものである、請求項1に記載の化粧品。
- 前記スポンジは、天然ゴム、合成樹脂、ポリウレタン、ラテックス、アクリロニトリル−ブタジエンゴム(NBR)、ブタジエンゴム(BR)、スチレン−ブタジエンゴム(SBR)、NR(Natural Rubber)、クロロプレンゴム(CR)、ブチルゴム(isoprene−isobutylene rubber:IIR)、イソプレンゴム(IR)、加硫エチレン−プロピレンゴム(EPR)、多硫化ゴム(Polysulfide rubber)、シリコーンゴム(silicone rubber)、フルオロゴム(fluororubber)、ウレタンゴム(urethane rubber)、アクリルゴム(Acrylic rubber)、EPDM(Ethylene propylene diene monomer)ゴム、ポリビニルアルコール(PVA)及びエチレンビニルアセテート(EVA)、及びNR(Nitrile Rubber)からなる群より選択された1種以上を含む、請求項1に記載の化粧品。
- 前記日焼け止め用化粧料組成物は、充填能が0.1〜5秒であり、且つ前記充填能は、前記担体のスポンジに手動で化粧料組成物15gが充填される時間である、請求項1に記載の化粧品。
- 当該化粧品は、日焼け止め用化粧料組成物が含浸された担体から化粧料組成物を取る塗布具を更に含む、請求項1に記載の化粧品。
Applications Claiming Priority (3)
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KR1020150093779A KR102083914B1 (ko) | 2015-06-30 | 2015-06-30 | 자외선 차단용 화장료 조성물 |
KR10-2015-0093779 | 2015-06-30 | ||
PCT/KR2016/006739 WO2017003135A1 (ko) | 2015-06-30 | 2016-06-24 | 자외선 차단용 화장료 조성물 |
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JP6862370B2 JP6862370B2 (ja) | 2021-04-21 |
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US (1) | US20180185254A1 (ja) |
EP (1) | EP3318245B1 (ja) |
JP (1) | JP6862370B2 (ja) |
KR (1) | KR102083914B1 (ja) |
CN (1) | CN107708656B (ja) |
CA (1) | CA2989289A1 (ja) |
MY (1) | MY188656A (ja) |
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Cited By (1)
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KR102525969B1 (ko) * | 2022-11-24 | 2023-04-26 | 주식회사 필킨 | 적외선 및 자외선 차단 화장 조성물 및 그 제조방법 |
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CN107864620A (zh) * | 2015-06-29 | 2018-03-30 | 高砂香料工业株式会社 | 麝香组合物和其使用方法 |
KR102591903B1 (ko) * | 2017-03-03 | 2023-10-19 | 가부시키가이샤 시세이도 | 화장품 |
KR102464015B1 (ko) | 2017-11-20 | 2022-11-08 | (주)아모레퍼시픽 | 폴리글리세릴계 유화제 및 소르비탄계 유화제를 포함하는 자외선 차단용 화장료 조성물 |
CN109568150A (zh) * | 2018-12-21 | 2019-04-05 | 上海昊海化工有限公司 | 一种防晒泡棉 |
KR20210127475A (ko) | 2020-04-14 | 2021-10-22 | 손희선 | 특수 히알루론산을 포함하여 보습 효과가 향상된 자외선 차단용 화장료 조성물 |
KR20200047465A (ko) | 2020-04-15 | 2020-05-07 | 손희선 | Spf 40 이상의 자외선 차단 효과 및 144시간 이상의 보습 효과를 나타내는 기능성 화장료 조성물 |
US20240122826A1 (en) | 2022-10-15 | 2024-04-18 | LCS Advanced Solutions, LLC | Structurally diverse, stable, and radiation-protective particle matrix sunscreen and cosmetic compositions and related methods |
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2016
- 2016-06-24 CA CA2989289A patent/CA2989289A1/en active Pending
- 2016-06-24 MY MYPI2017704997A patent/MY188656A/en unknown
- 2016-06-24 EP EP16818168.3A patent/EP3318245B1/en active Active
- 2016-06-24 US US15/740,150 patent/US20180185254A1/en not_active Abandoned
- 2016-06-24 CN CN201680038467.2A patent/CN107708656B/zh active Active
- 2016-06-24 WO PCT/KR2016/006739 patent/WO2017003135A1/ko active Application Filing
- 2016-06-24 JP JP2017568171A patent/JP6862370B2/ja active Active
- 2016-06-24 SG SG11201710212UA patent/SG11201710212UA/en unknown
- 2016-06-28 TW TW105120293A patent/TWI717362B/zh active
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Also Published As
Publication number | Publication date |
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SG11201710212UA (en) | 2018-01-30 |
JP6862370B2 (ja) | 2021-04-21 |
KR20170003295A (ko) | 2017-01-09 |
EP3318245A1 (en) | 2018-05-09 |
MY188656A (en) | 2021-12-22 |
WO2017003135A1 (ko) | 2017-01-05 |
TWI717362B (zh) | 2021-02-01 |
EP3318245B1 (en) | 2021-02-24 |
KR102083914B1 (ko) | 2020-03-03 |
EP3318245A4 (en) | 2019-01-16 |
CN107708656A (zh) | 2018-02-16 |
TW201701854A (zh) | 2017-01-16 |
US20180185254A1 (en) | 2018-07-05 |
CN107708656B (zh) | 2021-09-28 |
CA2989289A1 (en) | 2017-01-05 |
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