JP2018506504A - 液状化粧料担持用発泡フォームの製造方法、及びその発泡フォーム - Google Patents
液状化粧料担持用発泡フォームの製造方法、及びその発泡フォーム Download PDFInfo
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- 239000002537 cosmetic Substances 0.000 title claims abstract description 107
- 239000006260 foam Substances 0.000 title claims abstract description 101
- 239000007788 liquid Substances 0.000 title claims abstract description 92
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 29
- 239000004721 Polyphenylene oxide Substances 0.000 claims abstract description 42
- 229920005906 polyester polyol Polymers 0.000 claims abstract description 42
- 229920000570 polyether Polymers 0.000 claims abstract description 42
- 229920005862 polyol Polymers 0.000 claims abstract description 42
- 150000003077 polyols Chemical class 0.000 claims abstract description 42
- 239000000203 mixture Substances 0.000 claims abstract description 36
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 34
- 238000002156 mixing Methods 0.000 claims abstract description 33
- 239000003054 catalyst Substances 0.000 claims abstract description 32
- 239000004094 surface-active agent Substances 0.000 claims abstract description 32
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims abstract description 28
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- 238000005187 foaming Methods 0.000 claims abstract description 24
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- IMNIMPAHZVJRPE-UHFFFAOYSA-N triethylenediamine Chemical compound C1CN2CCN1CC2 IMNIMPAHZVJRPE-UHFFFAOYSA-N 0.000 claims description 14
- 230000006835 compression Effects 0.000 claims description 11
- 238000007906 compression Methods 0.000 claims description 11
- FRCHKSNAZZFGCA-UHFFFAOYSA-N 1,1-dichloro-1-fluoroethane Chemical compound CC(F)(Cl)Cl FRCHKSNAZZFGCA-UHFFFAOYSA-N 0.000 claims description 7
- BHNZEZWIUMJCGF-UHFFFAOYSA-N 1-chloro-1,1-difluoroethane Chemical compound CC(F)(F)Cl BHNZEZWIUMJCGF-UHFFFAOYSA-N 0.000 claims description 5
- HGXVKAPCSIXGAK-UHFFFAOYSA-N 2,4-diethyl-6-methylbenzene-1,3-diamine;4,6-diethyl-2-methylbenzene-1,3-diamine Chemical compound CCC1=CC(CC)=C(N)C(C)=C1N.CCC1=CC(C)=C(N)C(CC)=C1N HGXVKAPCSIXGAK-UHFFFAOYSA-N 0.000 claims description 5
- -1 33 lv Chemical compound 0.000 claims description 5
- GSEJCLTVZPLZKY-UHFFFAOYSA-N Triethanolamine Chemical compound OCCN(CCO)CCO GSEJCLTVZPLZKY-UHFFFAOYSA-N 0.000 claims description 5
- 239000003581 cosmetic carrier Substances 0.000 claims description 3
- 239000004604 Blowing Agent Substances 0.000 abstract description 10
- 239000000243 solution Substances 0.000 abstract description 9
- 239000006071 cream Substances 0.000 abstract description 5
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- 239000000499 gel Substances 0.000 abstract description 5
- 239000000725 suspension Substances 0.000 abstract description 5
- 239000007787 solid Substances 0.000 abstract description 3
- 238000010521 absorption reaction Methods 0.000 description 14
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 12
- 238000011049 filling Methods 0.000 description 12
- 230000000704 physical effect Effects 0.000 description 12
- 230000000052 comparative effect Effects 0.000 description 8
- 238000007599 discharging Methods 0.000 description 8
- 238000000034 method Methods 0.000 description 8
- 230000007062 hydrolysis Effects 0.000 description 6
- 238000006460 hydrolysis reaction Methods 0.000 description 6
- 238000002360 preparation method Methods 0.000 description 6
- 238000005260 corrosion Methods 0.000 description 4
- 230000007797 corrosion Effects 0.000 description 4
- 150000002148 esters Chemical class 0.000 description 4
- 238000011068 loading method Methods 0.000 description 4
- 229920003002 synthetic resin Polymers 0.000 description 4
- 239000000057 synthetic resin Substances 0.000 description 4
- 238000010998 test method Methods 0.000 description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
- 238000002835 absorbance Methods 0.000 description 2
- 239000000654 additive Substances 0.000 description 2
- 230000001914 calming effect Effects 0.000 description 2
- 238000012937 correction Methods 0.000 description 2
- 230000002950 deficient Effects 0.000 description 2
- 239000012153 distilled water Substances 0.000 description 2
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- C08J9/14—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof using blowing gases generated by a previously added blowing agent by a physical blowing agent organic
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- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
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- B—PERFORMING OPERATIONS; TRANSPORTING
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- B29K—INDEXING SCHEME ASSOCIATED WITH SUBCLASSES B29B, B29C OR B29D, RELATING TO MOULDING MATERIALS OR TO MATERIALS FOR MOULDS, REINFORCEMENTS, FILLERS OR PREFORMED PARTS, e.g. INSERTS
- B29K2071/00—Use of polyethers, e.g. PEEK, i.e. polyether-etherketone or PEK, i.e. polyetherketone or derivatives thereof, as moulding material
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29K—INDEXING SCHEME ASSOCIATED WITH SUBCLASSES B29B, B29C OR B29D, RELATING TO MOULDING MATERIALS OR TO MATERIALS FOR MOULDS, REINFORCEMENTS, FILLERS OR PREFORMED PARTS, e.g. INSERTS
- B29K2075/00—Use of PU, i.e. polyureas or polyurethanes or derivatives thereof, as moulding material
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- B—PERFORMING OPERATIONS; TRANSPORTING
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- B29L2031/00—Other particular articles
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Abstract
Description
1)ポリエステルポリオールの準備:ポリエステルポリオールをチャンバに入れ、温度55〜65℃、空気を抜き取り、0.1〜0.2KPa気圧条件で60分間鎮静にした後、温度を25〜35℃に下げた後、窒素を供給し、2〜3KPa内部圧力条件で48時間鎮静にし、ポリエステルポリオールを準備した。
2)ポリエーテルポリオールの準備:ポリエーテルポリオールをチャンバに入れ、温度15〜25℃、0.1〜0.2KPa気圧条件で60分間鎮静にした後、窒素を供給し、2〜3KPa気圧条件で48時間鎮静にし、ポリエーテルポリオールを準備した。
3)その他添加剤の準備:容量の需要に応じて、発泡剤、触媒剤及び界面活性剤をそれぞれタンクに注入して準備した。
4)発泡及び成形:前述のところで準備したポリエステルポリオール、ポリエーテルポリオール、発泡剤、触媒剤及び界面活性剤を、適正配合条件によって、混合撹拌タンクに順次に投入した後、温度22〜24℃、タンク内部圧力3KPaの条件で、分当たり5,000rpmで撹拌しながら連続発泡させた後、形成される発泡フォームを48時間熟成させ、液状化粧料を担持して使用することができる大きさに、前記発泡フォームを裁断して製品化した。
従来のポリエステルポリオール単独で製造された発泡フォーム(比較例1)と、ポリエーテルポリオール単独で製造された発泡フォーム(比較例2)とを準備した。前述の実施例及び比較例によって準備された発泡フォームの物性を比較し、その結果を下記表1に示した。
吸収度(%)=(B−A)/A×100
T:60℃
R/H:98%
露光時間(日):15日
1)ポリエステルポリオールの準備:ポリエステルポリオールをチャンバに入れ、温度55〜65℃、空気を抜き取り、0.1〜0.2kPa気圧条件で60分間鎮静にした後、温度を25〜35℃に下げた後、窒素を供給し、2〜3kPa内部圧力条件で48時間鎮静にし、ポリエステルポリオールを準備した。
2)ポリエーテルポリオールの準備:ポリエーテルポリオールをチャンバに入れ、温度15〜25℃、0.1〜0.2kPa気圧条件で60分間鎮静にした後、窒素を供給し、2〜3kPa気圧条件で48時間鎮静にし、ポリエーテルポリオールを準備した。
3)その他添加剤の準備:容量の需要に応じて、発泡剤、触媒剤及び界面活性剤をそれぞれタンクに注入して準備した。
4)発泡及び成形:前述のところで準備したポリエステルポリオール、ポリエーテルポリオール、発泡剤、触媒剤及び界面活性剤を、適正配合条件によって、混合撹拌タンクに順次に投入した後、温度22〜24℃、タンク内部圧力3kPaの条件で、分当たり5,000rpmで撹拌しながら連続発泡させた後、形成される発泡フォームを48時間熟成させ、液状化粧料を担持して使用することができる大きさに、前記発泡フォームを裁断して製品化した。
従来のポリエステルポリオール単独で製造された発泡フォーム(比較例1)と、ポリエーテルポリオール単独で製造された発泡フォーム(比較例2)とを準備した。前述の実施例及び比較例によって準備された発泡フォームの物性を比較し、その結果を下記表1に示した。
吸収度(%)=(B−A)/A×100
T:60℃
R/H:98%
露光時間(日):15日
Claims (7)
- (a)ポリエステルポリオールをチャンバに入れ、温度55〜65℃、空気を抜き取り、0.1〜0.2KPa気圧条件で60分間鎮静にした後、温度を25〜35℃に下げた後、窒素を供給し、2〜3KPa気圧条件で48時間鎮静にし、ポリエステルポリオールを準備する段階と、
(b)ポリエーテルポリオールをチャンバに入れ、温度15〜25℃、0.1〜0.2KPa気圧条件で60分間鎮静にした後、窒素を供給し、2〜3KPa気圧条件で48時間鎮静にし、ポリエーテルポリオールを準備する段階と、
(c)容量の需要に応じて、発泡剤、触媒剤及び界面活性剤をそれぞれタンクに注入して準備する段階と、
(d)前記ポリエステルポリオール、ポリエーテルポリオール、発泡剤、触媒剤及び界面活性剤を、配合比率によって、混合撹拌タンクに順次に投入した後、温度22〜24℃、タンク内部圧力3KPaの条件で、分当たり5,000rpmで撹拌しながら連続発泡させる段階と、
(e)前記発泡段階(d)が完了した後、形成される発泡フォームを48時間熟成させる段階と、
(f)前記発泡フォームを裁断して製品化する段階と、を含んでなることを特徴とする液状化粧料担持用発泡フォームの製造方法。 - 前記(d)段階の配合は、前記ポリエステルポリオールとポリエーテルポリオールとを3:7〜4:6の重量比で混合した混合物100重量部に対して、発泡剤0.2〜0.4重量部、触媒剤0.2〜0.4重量部、界面活性剤2〜4重量部を含むように混合することを特徴とする請求項1に記載の液状化粧料担持用発泡フォームの製造方法。
- 前記発泡剤は、HCFC−141b、HCFC−142b、HCF−22からなる群のうちから選択されるいずれか一つであることを特徴とする請求項1に記載の液状化粧料担持用発泡フォームの製造方法。
- 前記触媒剤は、TEDA、DETDA、33lv、A−1、A−99、TEOAからなる群のうちから選択されるいずれか一つであることを特徴とする請求項1に記載の液状化粧料担持用発泡フォームの製造方法。
- 前記界面活性剤は、AK8818、AK8803、AK8806からなる群のうちから選択されるいずれか一つであることを特徴とする請求項1に記載の液状化粧料担持用発泡フォームの製造方法。
- 液状化粧料担持用発泡フォームにおいて、
ポリエステルポリオールとポリエーテルポリオールとの混合比が、3:7または4:6のうちいずれか一つであることを特徴とする液状化粧料担持用発泡フォーム。 - 前記発泡フォームは、平均ポアサイズ900〜1,100μm、60〜80ppi(pore per inch)のポア数、密度40〜45kg/m2、反発弾性率40〜45%、圧縮変形率30〜40%、硬度75〜80°、引っ張り強度220〜230KPa、吸収率300〜400%であることを特徴とする請求項6に記載の液状化粧料担持用発泡フォーム。
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KR101881007B1 (ko) * | 2015-08-21 | 2018-07-24 | 주식회사 에이블씨엔씨 | 폴리에스테르 폴리에테르 중합 발포폼을 포함하는 화장품 |
KR101779571B1 (ko) * | 2017-01-06 | 2017-09-19 | 주식회사 세림티티시 | 화장용 발포폼의 제조방법 및 그 발포폼 |
US11525186B2 (en) | 2019-06-11 | 2022-12-13 | Ecolab Usa Inc. | Corrosion inhibitor formulation for geothermal reinjection well |
CN111186070A (zh) * | 2020-02-11 | 2020-05-22 | 刘林杰 | 一种基于三叶橡胶树的乳胶反洗发泡的橡胶加工系统 |
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US5552449A (en) * | 1991-04-22 | 1996-09-03 | Wm. T. Burnett & Co., Inc. | Polyurethane foam based on combination of polyester resin and polyether polyol |
WO2013154391A1 (ko) * | 2012-04-13 | 2013-10-17 | (주)아모레퍼시픽 | 발포 폼을 포함하는 화장료 조성물 담체 |
JP2014227426A (ja) * | 2013-05-17 | 2014-12-08 | 株式会社東洋クオリティワン | 化粧塗布用ポリウレタンフォームの製造方法および化粧塗布用ポリウレタンフォーム |
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DE19530388A1 (de) * | 1995-08-18 | 1997-02-20 | Bayer Ag | Geruchsarme, höhermolekulare Polyetherpolyole, ein Verfahren zu deren Herstellung sowie deren Verwendung für die Herstellung von auf Polyetherpolyolen aufbauenden Polymeren, Kosmetika und pharmazeutischen Produkten |
JP4731245B2 (ja) | 2005-08-12 | 2011-07-20 | 倉敷紡績株式会社 | 軟質ポリウレタンフォームおよび化粧用部材 |
CN101024684A (zh) * | 2007-01-29 | 2007-08-29 | 青岛科技大学 | 聚醚酯多元醇及其制备方法 |
KR101257628B1 (ko) * | 2011-03-24 | 2013-04-29 | (주)아모레퍼시픽 | 화장료 조성물이 함침된 발포 우레탄 폼을 포함하는 화장품 |
TWI617261B (zh) * | 2012-06-29 | 2018-03-11 | 愛茉莉太平洋股份有限公司 | 用於包含供於應用的海綿之化妝品組合物的容器 |
KR101791884B1 (ko) * | 2012-09-21 | 2017-10-31 | (주)아모레퍼시픽 | 화장료 조성물이 함침된 우레탄 폼 |
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Patent Citations (3)
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US5552449A (en) * | 1991-04-22 | 1996-09-03 | Wm. T. Burnett & Co., Inc. | Polyurethane foam based on combination of polyester resin and polyether polyol |
WO2013154391A1 (ko) * | 2012-04-13 | 2013-10-17 | (주)아모레퍼시픽 | 발포 폼을 포함하는 화장료 조성물 담체 |
JP2014227426A (ja) * | 2013-05-17 | 2014-12-08 | 株式会社東洋クオリティワン | 化粧塗布用ポリウレタンフォームの製造方法および化粧塗布用ポリウレタンフォーム |
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CN106572947B (zh) | 2019-05-03 |
WO2016133259A1 (ko) | 2016-08-25 |
US20170226304A1 (en) | 2017-08-10 |
JP6791841B2 (ja) | 2020-11-25 |
KR101574493B1 (ko) | 2015-12-11 |
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