JP2018171908A - 熱線透過抑制透光性基材、透光性基材ユニット - Google Patents
熱線透過抑制透光性基材、透光性基材ユニット Download PDFInfo
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Abstract
【解決手段】可視光及び近赤外光の波長領域のうちの少なくとも一部の波長領域の光の透過を抑制する透光性日射カットユニットと、
前記透光性日射カットユニット上に配置された、透明導電性酸化物を含有する透明導電性酸化物層とを有する熱線透過抑制透光性基材を提供する。
【選択図】図1
Description
前記透光性日射カットユニット上に配置された、透明導電性酸化物を含有する透明導電性酸化物層とを有する熱線透過抑制透光性基材を提供する。
[熱線透過抑制透光性基材]
本実施形態の熱線透過抑制透光性基材の一構成例について以下に説明する。
[透光性基材ユニット]
次に、本実施形態の透光性基材ユニットの一構成例について説明する。図4に示すように、本実施形態の透光性基材ユニット40は、窓用透光性基材41と、窓用透光性基材41の一方の面41a上に配置した既述の熱線透過抑制透光性基材42とを有することができる。
(評価方法)
(1)可視光透過率
可視光透過率は、分光光度計(日立ハイテク製 製品名「U−4100」)を用いて、JIS A5759−2008(建築窓ガラスフィルム)に準じて求めた。
(2)室内反射率
室内反射率は、絶対反射率として測定した。
(3)放射率
放射率は、角度可変反射アクセサリを備えるフーリエ変換型赤外分光(FT−IR)装置(Varian製)を用いて、光学干渉層側から波長5μm以上25μm以下の範囲の赤外線を照射した場合の正反射率を測定し、JIS R3106−2008(板ガラス類の透過率・反射率・放射率・日射熱取得率の試験方法)に準じて求めた。
(4)遮蔽係数
分光光度計(日立ハイテク製 製品名「U−4100」)を用いて、日射透過率τeおよび日射反射率ρeを測定し、JIS A5759−2008(建築窓ガラスフィルム)A法により、遮蔽係数を算出した。
(5)耐久性
直径3mmのステンレス製の金属棒に対して、4cm×4cmの熱線透過抑制透光性基材の透光性日射カットユニット側の面を内側にして、すなわち金属棒の表面と対向するようにして巻付けた。そして、熱線透過抑制透光性基材の金属棒の外周方向と平行な方向の両端をクリップで挟み30号(112.5g)の重りで荷重を5秒間かけた。
[実施例1]
表1に示した構成を有する熱線透過抑制透光性基材を作製し、評価を行った。
[実施例2、3]
透明導電性酸化物層が、表1に示した厚みとなるようにした点を除いて、実施例1と同様にして熱線透過抑制透光性基材、および透光性基材ユニットを作製し、評価を行った。なお、透明導電性酸化物層の厚みは、表1中断熱機能層の欄に開示している。
[実施例4]
透光性基材、およびハードコート層の構成について、以下のように変更した点以外は実施例1と同様にして熱線透過抑制透光性基材、および透光性基材ユニットを作製し、評価を行った。
[実施例5、6]
透明導電性酸化物層が、表1に示した厚みとなるようにした点を除いて、実施例4と同様にして熱線透過抑制透光性基材、および透光性基材ユニットを作製し、評価を行った。結果を表1に示す。
[実施例7]
粘着剤層、およびハードコート層、透明導電性酸化物層の構成について、以下のように変更した点以外は実施例1と同様にして熱線透過抑制透光性基材、および透光性基材ユニットを作製し、評価を行った。
[実施例8]
透光性基材、ハードコート層、透明導電性酸化物層の構成について、以下のように変更した点以外は実施例1と同様にして熱線透過抑制透光性基材、および透光性基材ユニットを作製し、評価を行った。
[実施例9]
粘着剤層、およびハードコート層を設けなかった点、透光性基材、および透明導電性酸化物層の構成を変更した点以外は実施例1と同様にして熱線透過抑制透光性基材の作製を行った。
[実施例10]
透光性基材として、厚みが19μmの着色され、内部透過率が50%のポリエチレンテレフタレート(PET)フィルム(三菱樹脂株式会社製 商品名:Z750E19)を用いた点、及び透明導電性酸化物層の厚みを表1に示した値とした点以外は実施例4と同様にして熱線透過抑制透光性基材、および透光性基材ユニットを作製し、評価を行った。
[実施例11]
表1に示した構成を有する熱線透過抑制透光性基材を作製し、評価を行った。
[実施例12]
表1に示した構成を有する熱線透過抑制透光性基材を作製し、評価を行った。
[実施例13]
透光性基材として、グリーンに着色され近赤外線を吸収する遮熱機能を有する、厚みが6mm+6mmの合わせグリーンガラス(旭硝子株式会社製 商品名クールベール)を用いた点以外は、実施例9と同様にして熱線透過抑制透光性基材、および透光性基材ユニットを作製し、評価を行った。
[実施例14]
TiO2層で挟まれたAg層にかえて、Ni−Cr層を用いた点以外は、実施例12と同様にして熱線透過抑制透光性基材、および透光性基材ユニットを作製し、評価を行った。
[実施例15]
光学干渉層として、アクリレート樹脂層にかえてSiO2層を成膜した点以外は、実施例2と同様にして熱線透過抑制透光性基材、および透光性基材ユニットを作製し、評価を行った。
[実施例16]
本実施例では、光学干渉層側から順に積層し、熱線透過抑制透光性基材を製造した。
[実施例17]
透明導電性酸化物層として、ITO膜に替えて、IZO膜(Indium Zinc Oxide膜、酸化インジウム亜鉛膜)を厚みが400nmとなるように成膜した点以外は、実施例1と同様にして熱線透過抑制透光性基材、および透光性基材ユニットを作製し、評価を行った。
[実施例18]
透明導電性酸化物層であるITO膜の厚みを30nmとした点以外は、実施例1と同様にして熱線透過抑制透光性基材、および透光性基材ユニットを作製し、評価を行った。
[実施例19]
遮熱ハードコート層と透明導電性酸化物層の間に以下の層を成膜した点以外は、実施例2と同様にして熱線透過抑制透光性基材、および透光性基材ユニットを作製し、評価を行った。
[比較例1]
表1に示した構成を有する熱線透過抑制透光性基材を作製し、評価を行った。
[比較例2、3]
APC層が、表1に示した厚みとなるようにした点を除いて、比較例1と同様にして熱線透過抑制透光性基材、および透光性基材ユニットを作製し、評価を行った。結果を表1に示す。
[比較例4]
透光性基材として、厚みが19μmであり、着色され、内部透過率が50%のポリエチレンテレフタレート(PET)フィルム(三菱樹脂株式会社製 商品名:Z750E19)を用いた点以外は、比較例3と同様にして熱線透過抑制透光性基材、および透光性基材ユニットを作製し、評価を行った。結果を表1に示す。
[比較例5]
ハードコート層を設けなかった点以外は実施例2と同様にして熱線透過抑制透光性基材、および透光性基材ユニットを作製し、評価を行った。なお、遮熱機能層を有していない。
断熱機能層である透明導電性酸化物層の厚さのみが異なる実施例1〜実施例3の結果と、実施例4〜6の結果と、比較例1〜3の結果をそれぞれ表2〜表4に分けて示す。
11 透光性日射カットユニット
111 ハードコート層
112 透光性基材
113 粘着剤層
12 透明導電性酸化物層
31 光学干渉層
40 透光性基材ユニット
41 窓用透光性基材
Claims (9)
- 可視光及び近赤外光の波長領域のうちの少なくとも一部の波長領域の光の透過を抑制する透光性日射カットユニットと、
前記透光性日射カットユニット上に配置された、透明導電性酸化物を含有する透明導電性酸化物層とを有する熱線透過抑制透光性基材。 - 前記透明導電性酸化物層の厚みが、30nm以上500nm以下である請求項1に記載の熱線透過抑制透光性基材。
- 前記透明導電性酸化物層が、前記透明導電性酸化物として、
スズ、チタン、タングステン、モリブデン、亜鉛、および水素から選択される1種類以上がドープされた酸化インジウムと、
アンチモン、インジウム、タンタル、塩素、およびフッ素から選択される1種類以上がドープされた酸化スズと、
インジウム、アルミニウム、スズ、ガリウム、フッ素、およびホウ素から選択される1種類以上がドープされた酸化亜鉛と、から選択される1種類以上を含有する請求項1または2に記載の熱線透過抑制透光性基材。 - 前記透明導電性酸化物層上にさらに光学干渉層を有する請求項1〜請求項3のいずれか1項に記載の熱線透過抑制透光性基材。
- 前記透光性日射カットユニットは、透光性基材と、前記透光性基材以外の部材とを含む請求項1〜請求項4のいずれか1項に記載の熱線透過抑制透光性基材。
- 前記透光性日射カットユニットは、前記透明導電性酸化物層と対向する面側から順に、ハードコート層、透光性基材、および粘着剤層を有しており、
前記ハードコート層、前記透光性基材、前記粘着剤層から選択された1以上の層が可視光及び近赤外光の波長領域のうちの少なくとも一部の波長領域の光の透過を抑制する機能を有する請求項1〜請求項5のいずれか1項に記載の熱線透過抑制透光性基材。 - 前記透明導電性酸化物層の側から測定した放射率が0.60以下である請求項1〜請求項6のいずれか1項に記載の熱線透過抑制透光性基材。
- 窓用透光性基材と、
前記窓用透光性基材の一方の面上に配置した請求項1〜請求項7のいずれか1項に記載の熱線透過抑制透光性基材とを有する透光性基材ユニット。 - 遮蔽係数が0.90以下である請求項8に記載の透光性基材ユニット。
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