JP2017530126A5 - - Google Patents
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- Publication number
- JP2017530126A5 JP2017530126A5 JP2017516116A JP2017516116A JP2017530126A5 JP 2017530126 A5 JP2017530126 A5 JP 2017530126A5 JP 2017516116 A JP2017516116 A JP 2017516116A JP 2017516116 A JP2017516116 A JP 2017516116A JP 2017530126 A5 JP2017530126 A5 JP 2017530126A5
- Authority
- JP
- Japan
- Prior art keywords
- acetate
- isobutyl
- methyltetrahydropyran
- cis
- trans
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000000203 mixture Substances 0.000 claims description 42
- 239000003205 fragrance Substances 0.000 claims description 20
- -1 Tetrahydropyran-4-yl Chemical group 0.000 claims description 18
- 150000001875 compounds Chemical class 0.000 claims description 13
- UWKAYLJWKGQEPM-LBPRGKRZSA-N linalyl acetate Chemical compound CC(C)=CCC[C@](C)(C=C)OC(C)=O UWKAYLJWKGQEPM-LBPRGKRZSA-N 0.000 claims description 12
- QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 claims description 9
- 239000000796 flavoring agent Substances 0.000 claims description 7
- UWKAYLJWKGQEPM-UHFFFAOYSA-N linalool acetate Natural products CC(C)=CCCC(C)(C=C)OC(C)=O UWKAYLJWKGQEPM-UHFFFAOYSA-N 0.000 claims description 6
- 238000000034 method Methods 0.000 claims description 6
- 235000019634 flavors Nutrition 0.000 claims description 5
- SYSQUGFVNFXIIT-UHFFFAOYSA-N n-[4-(1,3-benzoxazol-2-yl)phenyl]-4-nitrobenzenesulfonamide Chemical class C1=CC([N+](=O)[O-])=CC=C1S(=O)(=O)NC1=CC=C(C=2OC3=CC=CC=C3N=2)C=C1 SYSQUGFVNFXIIT-UHFFFAOYSA-N 0.000 claims description 5
- 239000002304 perfume Substances 0.000 claims description 4
- 235000002566 Capsicum Nutrition 0.000 claims description 3
- 239000006002 Pepper Substances 0.000 claims description 3
- 235000016761 Piper aduncum Nutrition 0.000 claims description 3
- 235000017804 Piper guineense Nutrition 0.000 claims description 3
- 235000008184 Piper nigrum Nutrition 0.000 claims description 3
- 239000003085 diluting agent Substances 0.000 claims description 3
- 230000002708 enhancing effect Effects 0.000 claims description 3
- 241000722363 Piper Species 0.000 claims 2
- 239000002537 cosmetic Substances 0.000 claims 2
- 239000003599 detergent Substances 0.000 claims 2
- 239000000463 material Substances 0.000 claims 2
- GBBKVBKUYQKEFL-UHFFFAOYSA-N [4-methyl-2-(2-methylpropyl)oxan-4-yl] acetate Chemical compound C(C)(C)CC1CC(C)(OC(=O)C)CCO1 GBBKVBKUYQKEFL-UHFFFAOYSA-N 0.000 claims 1
- 239000012459 cleaning agent Substances 0.000 claims 1
- 239000008194 pharmaceutical composition Substances 0.000 claims 1
- 239000011541 reaction mixture Substances 0.000 claims 1
- 238000000926 separation method Methods 0.000 claims 1
- 230000032050 esterification Effects 0.000 description 2
- 238000005886 esterification reaction Methods 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
- YVSNOTITPICPTB-UHFFFAOYSA-N 4-methyl-2-(2-methylpropyl)oxan-4-ol Chemical compound CC(C)CC1CC(C)(O)CCO1 YVSNOTITPICPTB-UHFFFAOYSA-N 0.000 description 1
- LETLQGKRPMMKKC-UHFFFAOYSA-N 4-methyl-2-(2-methylpropyl)oxane Chemical compound CC(C)CC1CC(C)CCO1 LETLQGKRPMMKKC-UHFFFAOYSA-N 0.000 description 1
- 244000179970 Monarda didyma Species 0.000 description 1
- 235000010672 Monarda didyma Nutrition 0.000 description 1
- 244000270834 Myristica fragrans Species 0.000 description 1
- 235000009421 Myristica fragrans Nutrition 0.000 description 1
- 244000203593 Piper nigrum Species 0.000 description 1
- 239000001926 citrus aurantium l. subsp. bergamia wright et arn. oil Substances 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 235000013355 food flavoring agent Nutrition 0.000 description 1
- 238000004508 fractional distillation Methods 0.000 description 1
- 239000000171 lavandula angustifolia l. flower oil Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000001702 nutmeg Substances 0.000 description 1
- 230000001953 sensory effect Effects 0.000 description 1
- 230000002195 synergetic effect Effects 0.000 description 1
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP14186627.7 | 2014-09-26 | ||
| EP14186627 | 2014-09-26 | ||
| PCT/EP2015/072083 WO2016046360A1 (de) | 2014-09-26 | 2015-09-25 | Verwendung von isomerenreinem oder hoch isomerenangereichertem cis- oder trans-(2-isobutyl-4-methyl-tetrahydropyran-4-yl)acetat |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2017530126A JP2017530126A (ja) | 2017-10-12 |
| JP2017530126A5 true JP2017530126A5 (https=) | 2018-11-01 |
| JP6822948B2 JP6822948B2 (ja) | 2021-01-27 |
Family
ID=51752982
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2017516116A Active JP6822948B2 (ja) | 2014-09-26 | 2015-09-25 | 異性体として純粋な又は高度に異性体濃縮されたcis−又はtrans−(2−イソブチル−4−メチルテトラヒドロピラン−4−イル)アセテートの使用 |
Country Status (9)
| Country | Link |
|---|---|
| US (1) | US10160931B2 (https=) |
| EP (1) | EP3197987B1 (https=) |
| JP (1) | JP6822948B2 (https=) |
| CN (1) | CN106715408B (https=) |
| ES (1) | ES2721530T3 (https=) |
| MX (1) | MX375962B (https=) |
| PL (1) | PL3197987T3 (https=) |
| TR (1) | TR201904599T4 (https=) |
| WO (1) | WO2016046360A1 (https=) |
Families Citing this family (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP6741687B2 (ja) | 2015-05-04 | 2020-08-19 | ビーエーエスエフ ソシエタス・ヨーロピアBasf Se | メロナールの調製方法 |
| BR112018000481B1 (pt) | 2015-07-10 | 2022-01-11 | Basf Se | Processos para preparação de compostos e de (-)- ambrox (v) |
| CN107848929A (zh) | 2015-07-15 | 2018-03-27 | 巴斯夫欧洲公司 | 制备芳基丙烯的方法 |
| US10202323B2 (en) | 2015-07-15 | 2019-02-12 | Basf Se | Process for preparing an arylpropene |
| EP3170828A1 (de) | 2015-11-23 | 2017-05-24 | Basf Se | Verfahren zur herstellung von verbindungen mit 16-oxabicyclo[10.3.1]pentadecengerüst und deren folgeprodukten |
| ES2899827T3 (es) | 2015-12-08 | 2022-03-14 | Basf Se | Material zeolítico que contiene estaño y que tiene una estructura de marco BEA |
| EP3816297A1 (de) | 2016-02-19 | 2021-05-05 | Basf Se | Biokatalytische zyklisierung von mehrfach ungesättigten carbonsäuren-verbindungen |
| US10981885B2 (en) | 2016-05-31 | 2021-04-20 | Basf Se | Tetrahydropyranyl lower alkyl esters and the production of same using a ketene compound |
| WO2017211784A1 (en) | 2016-06-07 | 2017-12-14 | Basf Se | Process for preparing 2,3-unsaturated alcohols |
| JP7039551B2 (ja) | 2016-07-15 | 2022-03-22 | ビーエーエスエフ ソシエタス・ヨーロピア | 3-メチル-1,5-シクロペンタデカンジオンからの14-メチル-16-オキサビシクロ[10.3.1]ペンタデセンの調製 |
| EP3572487A1 (en) * | 2018-05-25 | 2019-11-27 | Basf Se | 2-furyl- and 2-thienyl-substituted di- and tetrahydropyrans for use as aroma chemicals |
| EP3880777B1 (en) * | 2018-11-13 | 2025-06-25 | Symrise AG | Perfuming ingredients with lily of the valley note |
| EP3838895A1 (en) * | 2019-12-16 | 2021-06-23 | Basf Se | Substituted 4-methylene-tetrahydropyrans, 4-methyl-dihydropyrans and 4-methyl-tetrahydropyrans and use thereof as aroma chemicals |
| CN119790128A (zh) * | 2022-09-06 | 2025-04-08 | 西姆莱斯股份公司 | 香料混合物(iii) |
Family Cites Families (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4963285A (en) * | 1989-02-09 | 1990-10-16 | International Flavors & Fragrances Inc. | 2,4,4-irisubstituted tetrahydro pyranyl esters and organoleptic uses thereof |
| EP2432773B1 (de) | 2009-05-19 | 2013-08-28 | Basf Se | Verfahren zur Herstellung von 2-substituierten Tetrahydropyranolen |
| MX2012013509A (es) | 2010-05-27 | 2013-01-24 | Basf Se | Procedimiento para la preparacion de tetrahidropiranoles 2-sustituidos. |
| ES2511143T3 (es) | 2010-06-10 | 2014-10-22 | Basf Se | Procedimiento para la preparación y aislamiento de tetrahidropiranoles sustituidos en la posición 2 |
| ES2498942T3 (es) * | 2010-11-10 | 2014-09-26 | Basf Se | Composiciones de perfume que comprenden mezclas especiales de diastereómeros de 2-isobutil-4-metil-tetrahidro-2H-piran-4-ol |
| US9340754B2 (en) | 2012-11-27 | 2016-05-17 | Basf Se | Process for the preparation of cyclohexyl-substituted tertiary alkanols |
| ES2676411T3 (es) | 2013-04-29 | 2018-07-19 | Basf Se | Procedimiento para la preparación de 4-hidroxi-4-metil-tetrahidropiranos 2-sustituidos, con recirculación |
| CN106103398A (zh) | 2014-01-17 | 2016-11-09 | 巴斯夫欧洲公司 | 用于生产芳基丙烯的方法 |
| EP3131888B1 (de) | 2014-04-14 | 2022-08-03 | Basf Se | Herstellung von 2-substituierten 4-hydroxy-4-methyl-tetrahydropyranen aus 2-alkyl-4,4-dimethyl-1,3-dioxan-haltigen ausgangsstoffen |
| EP2865676A1 (de) | 2014-04-14 | 2015-04-29 | Basf Se | Herstellung von 2-substituierten 4-Methyl-tetrahydropyranen aus 2-Alkyl-4,4-dimethyl-1,3-dioxan-haltigen Ausgangsstoffen |
| MX386539B (es) | 2014-04-14 | 2025-03-18 | Basf Se | Producción de 4-hidroxi-4-metiltetrahidropiranos 2-sustituidos que tienen calidad odorífera estable. |
| US20170275225A1 (en) | 2014-09-09 | 2017-09-28 | Basf Se | Method for the preparation of 2-alkoxy cyclohexanol |
| CN106660916A (zh) | 2014-09-09 | 2017-05-10 | 巴斯夫欧洲公司 | 生产芳香物质的方法 |
-
2015
- 2015-09-25 JP JP2017516116A patent/JP6822948B2/ja active Active
- 2015-09-25 PL PL15767522T patent/PL3197987T3/pl unknown
- 2015-09-25 TR TR2019/04599T patent/TR201904599T4/tr unknown
- 2015-09-25 US US15/514,101 patent/US10160931B2/en active Active
- 2015-09-25 EP EP15767522.4A patent/EP3197987B1/de active Active
- 2015-09-25 WO PCT/EP2015/072083 patent/WO2016046360A1/de not_active Ceased
- 2015-09-25 CN CN201580051668.1A patent/CN106715408B/zh active Active
- 2015-09-25 MX MX2017003923A patent/MX375962B/es active IP Right Grant
- 2015-09-25 ES ES15767522T patent/ES2721530T3/es active Active
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